In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel

Abstract The bainitic transformation behavior and microstructural evolution in C–Mn–Si steel were investigated using in-situ Laser Scanning Confocal Microscopy (LSCM) and dilatometry. The study focused on three distinct isothermal bainitic transformation (IBT) temperatures (400 °C, 350 °C, and 300 °...

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Main Authors: Soumyadarshi Saswat Mahapatra, Md. Basiruddin Sk, Prakash Srirangam, Soumitra Kumar Dinda
Format: Article
Language:English
Published: Springer 2025-07-01
Series:Discover Materials
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Online Access:https://doi.org/10.1007/s43939-025-00333-4
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author Soumyadarshi Saswat Mahapatra
Md. Basiruddin Sk
Prakash Srirangam
Soumitra Kumar Dinda
author_facet Soumyadarshi Saswat Mahapatra
Md. Basiruddin Sk
Prakash Srirangam
Soumitra Kumar Dinda
author_sort Soumyadarshi Saswat Mahapatra
collection DOAJ
description Abstract The bainitic transformation behavior and microstructural evolution in C–Mn–Si steel were investigated using in-situ Laser Scanning Confocal Microscopy (LSCM) and dilatometry. The study focused on three distinct isothermal bainitic transformation (IBT) temperatures (400 °C, 350 °C, and 300 °C), revealing morphological transitions from granular and upper bainite to refined lower bainite with decreasing IBT. During rapid cooling from the austenitization temperature, bainitic ferrite nucleation at the free surface commenced approximately 60 °C higher than the bainite start (Bs) temperature measured by dilatometry. This discrepancy was attributed to reduced strain energy requirements at the free surface, facilitating easier plastic relaxation of the surrounding austenite. The IBT300 sample exhibited the finest microstructure, characterized by a predominant lower bainite morphology and thin retained austenite films, significantly improving strength and impact toughness. Sympathetic nucleation of bainitic ferrite was frequently observed, especially in lower IBT-treated samples, contributing to microstructural refinement. Additionally, free energy calculations indicated a correlation between isothermal holding temperatures and carbon partitioning, influencing the extent of bainitic transformation. This work underscores the critical role of transformation kinetics and morphological evolution in achieving optimized bainitic microstructures, providing a pathway for enhancing the mechanical properties of high-strength steels.
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spelling doaj-art-b87e44c11e4e4cabb0f3d11085f7f50e2025-08-20T04:02:41ZengSpringerDiscover Materials2730-77272025-07-015111210.1007/s43939-025-00333-4In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steelSoumyadarshi Saswat Mahapatra0Md. Basiruddin Sk1Prakash Srirangam2Soumitra Kumar Dinda3Metallurgical and Materials Engineering Department, National Institute of TechnologyMetallurgical and Materials Engineering Department, Jadavpur UniversityWarwick Manufacturing Group (WMG), University of WarwickMetallurgical and Materials Engineering Department, National Institute of TechnologyAbstract The bainitic transformation behavior and microstructural evolution in C–Mn–Si steel were investigated using in-situ Laser Scanning Confocal Microscopy (LSCM) and dilatometry. The study focused on three distinct isothermal bainitic transformation (IBT) temperatures (400 °C, 350 °C, and 300 °C), revealing morphological transitions from granular and upper bainite to refined lower bainite with decreasing IBT. During rapid cooling from the austenitization temperature, bainitic ferrite nucleation at the free surface commenced approximately 60 °C higher than the bainite start (Bs) temperature measured by dilatometry. This discrepancy was attributed to reduced strain energy requirements at the free surface, facilitating easier plastic relaxation of the surrounding austenite. The IBT300 sample exhibited the finest microstructure, characterized by a predominant lower bainite morphology and thin retained austenite films, significantly improving strength and impact toughness. Sympathetic nucleation of bainitic ferrite was frequently observed, especially in lower IBT-treated samples, contributing to microstructural refinement. Additionally, free energy calculations indicated a correlation between isothermal holding temperatures and carbon partitioning, influencing the extent of bainitic transformation. This work underscores the critical role of transformation kinetics and morphological evolution in achieving optimized bainitic microstructures, providing a pathway for enhancing the mechanical properties of high-strength steels.https://doi.org/10.1007/s43939-025-00333-4C–Mn–Si steelBainitic transformationIn-situ confocal microscopyElectron backscattered diffraction analysisDilatometric study
spellingShingle Soumyadarshi Saswat Mahapatra
Md. Basiruddin Sk
Prakash Srirangam
Soumitra Kumar Dinda
In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
Discover Materials
C–Mn–Si steel
Bainitic transformation
In-situ confocal microscopy
Electron backscattered diffraction analysis
Dilatometric study
title In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
title_full In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
title_fullStr In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
title_full_unstemmed In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
title_short In-situ investigation on the morphological evaluation of bainitic microstructure of medium C-steel
title_sort in situ investigation on the morphological evaluation of bainitic microstructure of medium c steel
topic C–Mn–Si steel
Bainitic transformation
In-situ confocal microscopy
Electron backscattered diffraction analysis
Dilatometric study
url https://doi.org/10.1007/s43939-025-00333-4
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