A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure
Abstract A simple two step synthetic method for di‐doped crystalline mesoporous tin dioxide powder containing antimony and fluoride at ambient pressure and temperature has been developed. This approach produced materials with high surface areas and improved electrical and optoelectrical conductance....
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Wiley-VCH
2025-01-01
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Online Access: | https://doi.org/10.1002/open.202400096 |
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author | Tariq Aqeel Heather F. Greer |
author_facet | Tariq Aqeel Heather F. Greer |
author_sort | Tariq Aqeel |
collection | DOAJ |
description | Abstract A simple two step synthetic method for di‐doped crystalline mesoporous tin dioxide powder containing antimony and fluoride at ambient pressure and temperature has been developed. This approach produced materials with high surface areas and improved electrical and optoelectrical conductance. The two dopant elements; antimony and fluoride were introduced to tin dioxide by two approaches. Both approaches produced mesoporous tin dioxide with antimony and fluoride that are integrated in the framework. The structures of these materials are analyzed by powder X‐ray diffraction, N2 sorption analysis, transmission electron microscopy, energy dispersive X‐ray spectroscopy and X‐ray photoelectron spectroscopy. The conductance of the materials improved by factor of 13–34 compared to undoped mesoporous tin dioxide. The effect of the di‐doped elements on structure, conductance and optoelectronic properties of these materials are discussed in this paper. |
format | Article |
id | doaj-art-b68a460c937d46f3bafb5cb01d6f1479 |
institution | Kabale University |
issn | 2191-1363 |
language | English |
publishDate | 2025-01-01 |
publisher | Wiley-VCH |
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series | ChemistryOpen |
spelling | doaj-art-b68a460c937d46f3bafb5cb01d6f14792025-01-11T07:54:10ZengWiley-VCHChemistryOpen2191-13632025-01-01141n/an/a10.1002/open.202400096A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and PressureTariq Aqeel0Heather F. Greer1Department of Science College of basic education The Public Authority for Applied Education and Training (PAAET) P.O. Box 23167 Safat 13092 KuwaitYusuf Hamied Department of Chemistry University of Cambridge Cambridge CB2 1EW UKAbstract A simple two step synthetic method for di‐doped crystalline mesoporous tin dioxide powder containing antimony and fluoride at ambient pressure and temperature has been developed. This approach produced materials with high surface areas and improved electrical and optoelectrical conductance. The two dopant elements; antimony and fluoride were introduced to tin dioxide by two approaches. Both approaches produced mesoporous tin dioxide with antimony and fluoride that are integrated in the framework. The structures of these materials are analyzed by powder X‐ray diffraction, N2 sorption analysis, transmission electron microscopy, energy dispersive X‐ray spectroscopy and X‐ray photoelectron spectroscopy. The conductance of the materials improved by factor of 13–34 compared to undoped mesoporous tin dioxide. The effect of the di‐doped elements on structure, conductance and optoelectronic properties of these materials are discussed in this paper.https://doi.org/10.1002/open.202400096MesoporousTin dioxideFluorideAntimonyOptoelectronic conductance |
spellingShingle | Tariq Aqeel Heather F. Greer A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure ChemistryOpen Mesoporous Tin dioxide Fluoride Antimony Optoelectronic conductance |
title | A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure |
title_full | A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure |
title_fullStr | A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure |
title_full_unstemmed | A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure |
title_short | A Facile Method to Incorporate Di‐Dopant Elements (F and Sb) into Crystalline Mesoporous Tin Dioxide Nano Powder at Ambient Temperature and Pressure |
title_sort | facile method to incorporate di dopant elements f and sb into crystalline mesoporous tin dioxide nano powder at ambient temperature and pressure |
topic | Mesoporous Tin dioxide Fluoride Antimony Optoelectronic conductance |
url | https://doi.org/10.1002/open.202400096 |
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