Phase-interface-anchored cadmium single-atom catalysts for efficient methanol steam reforming

Abstract Employing interface engineering to design innovative single-atom catalysts (SACs) for effective methanol steam reforming (MSR) presents an attractive yet formidable challenge. Here, we report phase-interface confined Cd/P25 SACs, where Cd atoms are stably anchored at the phase interface bet...

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Bibliographic Details
Main Authors: Shunan Zhang, Haozhi Zhou, Zilong Shao, Baohuan Wei, Zhen Hu, Hao Liang, Ruonan Zhang, Xiaofang Liu, Hu Luo, Lin Xia, Yuhan Sun, Hui Wang
Format: Article
Language:English
Published: Nature Portfolio 2025-08-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-63060-7
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Summary:Abstract Employing interface engineering to design innovative single-atom catalysts (SACs) for effective methanol steam reforming (MSR) presents an attractive yet formidable challenge. Here, we report phase-interface confined Cd/P25 SACs, where Cd atoms are stably anchored at the phase interface between anatase (101) and rutile (110) facets. The Cd-O-Ti phase interface sites formed exhibit asymmetric geometric and electronic properties that enable 100% methanol conversion, a low CO concentration (~0.1 mol%) in the effluent gas, and sustained stability exceeding 150 h. The H2 production rate at these interface sites is approximately 15-fold and 8-fold higher than that of anatase and rutile surface sites, respectively. Enhancing the phase interface density through atmosphere pretreatment can further increase the H2 production rate by an additional 11%. Furthermore, these powder SACs can be 3D printed into kilogram-scale monolithic catalysts, advancing practical in-situ hydrogen generation applications.
ISSN:2041-1723