Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies

The present work has investigated the fracture toughness of a model DGEBA epoxy system subject to Hidro-Thermal aging. A Photoelastic Stress Analysis technique has been implemented, showing the evolution of stresses arising throughout the water uptake process due to the non-uniform swelling of the m...

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Main Authors: G. Pitarresi, A. Toscano, M. Scafidi, M. Di Filippo, S. Alessi, G. Spadaro
Format: Article
Language:English
Published: Gruppo Italiano Frattura 2014-09-01
Series:Fracture and Structural Integrity
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Online Access:https://www.fracturae.com/index.php/fis/article/view/1313
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author G. Pitarresi
A. Toscano
M. Scafidi
M. Di Filippo
S. Alessi
G. Spadaro
author_facet G. Pitarresi
A. Toscano
M. Scafidi
M. Di Filippo
S. Alessi
G. Spadaro
author_sort G. Pitarresi
collection DOAJ
description The present work has investigated the fracture toughness of a model DGEBA epoxy system subject to Hidro-Thermal aging. A Photoelastic Stress Analysis technique has been implemented, showing the evolution of stresses arising throughout the water uptake process due to the non-uniform swelling of the material. Gravimetric and Dynamic Mechanical Thermal Analyses have further complemented the characterization, showing the onset of plasticization effects with aging. The correlation of all previous characterizations has allowed to conclude that an increase of KIC fracture toughness is obtained at the fully saturated condition. In particular Photoelasticity has also revealed the onset of relevant swelling induced stresses during the first stages of water absorption, leading to an increase of fracture toughness due to compressive stresses settling near the crack tip. A stress free condition is instead reestablished at the later stages of absorption, suggesting that the increased toughness of the saturated material is an effect of the modifications induced by aging on the polymer structure.
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institution Kabale University
issn 1971-8993
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publishDate 2014-09-01
publisher Gruppo Italiano Frattura
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series Fracture and Structural Integrity
spelling doaj-art-4df61c64a3804199b9496c2a2a4fe06d2025-01-03T00:40:23ZengGruppo Italiano FratturaFracture and Structural Integrity1971-89932014-09-01830Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxiesG. Pitarresi0A. Toscano1M. Scafidi2M. Di Filippo3S. Alessi4G. Spadaro5University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)University of Palermo, Dipartimento di Ingegneria Chimica, Gestionale, Informatica, Meccanica (DICGIM) – Viale delle Scienze, 90128 Palermo (Italy)The present work has investigated the fracture toughness of a model DGEBA epoxy system subject to Hidro-Thermal aging. A Photoelastic Stress Analysis technique has been implemented, showing the evolution of stresses arising throughout the water uptake process due to the non-uniform swelling of the material. Gravimetric and Dynamic Mechanical Thermal Analyses have further complemented the characterization, showing the onset of plasticization effects with aging. The correlation of all previous characterizations has allowed to conclude that an increase of KIC fracture toughness is obtained at the fully saturated condition. In particular Photoelasticity has also revealed the onset of relevant swelling induced stresses during the first stages of water absorption, leading to an increase of fracture toughness due to compressive stresses settling near the crack tip. A stress free condition is instead reestablished at the later stages of absorption, suggesting that the increased toughness of the saturated material is an effect of the modifications induced by aging on the polymer structure.https://www.fracturae.com/index.php/fis/article/view/1313Fracture Toughness
spellingShingle G. Pitarresi
A. Toscano
M. Scafidi
M. Di Filippo
S. Alessi
G. Spadaro
Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
Fracture and Structural Integrity
Fracture Toughness
title Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
title_full Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
title_fullStr Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
title_full_unstemmed Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
title_short Photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
title_sort photoelastic stress analysis assisted evaluation of fracture toughness in hydrothermally aged epoxies
topic Fracture Toughness
url https://www.fracturae.com/index.php/fis/article/view/1313
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AT atoscano photoelasticstressanalysisassistedevaluationoffracturetoughnessinhydrothermallyagedepoxies
AT mscafidi photoelasticstressanalysisassistedevaluationoffracturetoughnessinhydrothermallyagedepoxies
AT mdifilippo photoelasticstressanalysisassistedevaluationoffracturetoughnessinhydrothermallyagedepoxies
AT salessi photoelasticstressanalysisassistedevaluationoffracturetoughnessinhydrothermallyagedepoxies
AT gspadaro photoelasticstressanalysisassistedevaluationoffracturetoughnessinhydrothermallyagedepoxies