Synthesis and characterization of new hybrid microspheres with amide functionalization
In this article, synthesis and characterization of new crosslinked hybrid microspheres are presented. This material was obtained by the emulsion-suspension polymerization of 1,4-divinylbenzene and trimethoxyvinylsilane. In the case of introducing biologically active functional groups on the surface...
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| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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SAGE Publishing
2017-06-01
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| Series: | Adsorption Science & Technology |
| Online Access: | https://doi.org/10.1177/0263617417694364 |
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| _version_ | 1841564078989901824 |
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| author | Beata Podkościelna Karolina Fila Małgorzata Gil Janina Nowak |
| author_facet | Beata Podkościelna Karolina Fila Małgorzata Gil Janina Nowak |
| author_sort | Beata Podkościelna |
| collection | DOAJ |
| description | In this article, synthesis and characterization of new crosslinked hybrid microspheres are presented. This material was obtained by the emulsion-suspension polymerization of 1,4-divinylbenzene and trimethoxyvinylsilane. In the case of introducing biologically active functional groups on the surface of microspheres, methacrylamide as a third monomer was added. Chemical structures of all new materials were confirmed by the spectroscopic method (attenuated total reflectance-Fourier transform infrared spectroscopy) and elemental analysis. The influence of comonomer structure on the physico-chemical properties of the hybrid microspheres was investigated. Porous structures in a dry state were studied by means of nitrogen adsorption–desorption measurements. Thermal stabilities and degradation behavior of the obtained copolymers were characterized by the use of thermogravimetric/derivative thermo-gravimetric analysis. |
| format | Article |
| id | doaj-art-20e31df0cacb4898961b5d95b47bbdf2 |
| institution | Kabale University |
| issn | 0263-6174 2048-4038 |
| language | English |
| publishDate | 2017-06-01 |
| publisher | SAGE Publishing |
| record_format | Article |
| series | Adsorption Science & Technology |
| spelling | doaj-art-20e31df0cacb4898961b5d95b47bbdf22025-01-02T23:11:48ZengSAGE PublishingAdsorption Science & Technology0263-61742048-40382017-06-013510.1177/0263617417694364Synthesis and characterization of new hybrid microspheres with amide functionalizationBeata PodkościelnaKarolina FilaMałgorzata GilJanina NowakIn this article, synthesis and characterization of new crosslinked hybrid microspheres are presented. This material was obtained by the emulsion-suspension polymerization of 1,4-divinylbenzene and trimethoxyvinylsilane. In the case of introducing biologically active functional groups on the surface of microspheres, methacrylamide as a third monomer was added. Chemical structures of all new materials were confirmed by the spectroscopic method (attenuated total reflectance-Fourier transform infrared spectroscopy) and elemental analysis. The influence of comonomer structure on the physico-chemical properties of the hybrid microspheres was investigated. Porous structures in a dry state were studied by means of nitrogen adsorption–desorption measurements. Thermal stabilities and degradation behavior of the obtained copolymers were characterized by the use of thermogravimetric/derivative thermo-gravimetric analysis.https://doi.org/10.1177/0263617417694364 |
| spellingShingle | Beata Podkościelna Karolina Fila Małgorzata Gil Janina Nowak Synthesis and characterization of new hybrid microspheres with amide functionalization Adsorption Science & Technology |
| title | Synthesis and characterization of new hybrid microspheres with amide functionalization |
| title_full | Synthesis and characterization of new hybrid microspheres with amide functionalization |
| title_fullStr | Synthesis and characterization of new hybrid microspheres with amide functionalization |
| title_full_unstemmed | Synthesis and characterization of new hybrid microspheres with amide functionalization |
| title_short | Synthesis and characterization of new hybrid microspheres with amide functionalization |
| title_sort | synthesis and characterization of new hybrid microspheres with amide functionalization |
| url | https://doi.org/10.1177/0263617417694364 |
| work_keys_str_mv | AT beatapodkoscielna synthesisandcharacterizationofnewhybridmicrosphereswithamidefunctionalization AT karolinafila synthesisandcharacterizationofnewhybridmicrosphereswithamidefunctionalization AT małgorzatagil synthesisandcharacterizationofnewhybridmicrosphereswithamidefunctionalization AT janinanowak synthesisandcharacterizationofnewhybridmicrosphereswithamidefunctionalization |