To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing

Abstract This study examined a room temperature operative, highly sensitive, stable, and selective PANI ammonia (NH3) gas sensor using multiwalled carbon nanotubes (MWCNTs) and copper nanocomposites (Cu). The silicon substrate was coated with the sensing materials using the drop casting technique. T...

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Main Authors: Shah Masheerul Aalam, Aaliyah Farooq, Mohd Sarvar, Mohd Nadeem Bhat, Monika Tomar, Mohammad Moeen Hasan Raza, Javid Ali
Format: Article
Language:English
Published: Nature Portfolio 2025-07-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-01055-6
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author Shah Masheerul Aalam
Aaliyah Farooq
Mohd Sarvar
Mohd Nadeem Bhat
Monika Tomar
Mohammad Moeen Hasan Raza
Javid Ali
author_facet Shah Masheerul Aalam
Aaliyah Farooq
Mohd Sarvar
Mohd Nadeem Bhat
Monika Tomar
Mohammad Moeen Hasan Raza
Javid Ali
author_sort Shah Masheerul Aalam
collection DOAJ
description Abstract This study examined a room temperature operative, highly sensitive, stable, and selective PANI ammonia (NH3) gas sensor using multiwalled carbon nanotubes (MWCNTs) and copper nanocomposites (Cu). The silicon substrate was coated with the sensing materials using the drop casting technique. To synthesize PANI, PANI@Cu@MWCNT nanocomposites chemical polymerisation method and ultrasonication techniques were used. In comparison to three PANI nano-composite sensor, which demonstrated sensing responses of 18%, 28%, and 43%, respectively, the PANI@Cu3@MWCNT3-based sensor demonstrated a greater sensing response of 116% under the room temperature conditions of NH3 (100 ppm). The resistance variation of all the sensors is 62 kΩ, 78 kΩ, 89 kΩ, and 90 kΩ respectively. The PANI@Cu3@MWCNT3 based sensor exhibited excellent results in term of resistance (90 kΩ). The stability, response time (10 s), and recovery time (13 s) of PANI@Cu2@MWCNT2 is measured and has better results in terms of time than all other sensors. Pure PANI nano-composite sensor has shown the sensing response of 18%, resistance variation of 62 kΩ, response time (45 s), recovery time (48 s) respectively. The sensing materials were characterized using FTIR, XRD, EDX, and FESEM techniques. PANI and PANI@Cu@MWCNT nanocomposites’ gas sensing capabilities were examined using a Keithley 6514 multimeter.
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spelling doaj-art-1d319b5a2c864c00baa5f5168e7b5ec22025-08-20T03:43:21ZengNature PortfolioScientific Reports2045-23222025-07-0115111610.1038/s41598-025-01055-6To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensingShah Masheerul Aalam0Aaliyah Farooq1Mohd Sarvar2Mohd Nadeem Bhat3Monika Tomar4Mohammad Moeen Hasan Raza5Javid Ali6Department of Physics, Jamia Millia IslamiaDepartment of Chemistry, Jamia Millia IslamiaDepartment of Physics, Jamia Millia IslamiaNational Institute of TechnologyDepartment of Physics, Miranda House , University of DelhiKing Fahd University of Petroleum & MineralsDepartment of Physics, Jamia Millia IslamiaAbstract This study examined a room temperature operative, highly sensitive, stable, and selective PANI ammonia (NH3) gas sensor using multiwalled carbon nanotubes (MWCNTs) and copper nanocomposites (Cu). The silicon substrate was coated with the sensing materials using the drop casting technique. To synthesize PANI, PANI@Cu@MWCNT nanocomposites chemical polymerisation method and ultrasonication techniques were used. In comparison to three PANI nano-composite sensor, which demonstrated sensing responses of 18%, 28%, and 43%, respectively, the PANI@Cu3@MWCNT3-based sensor demonstrated a greater sensing response of 116% under the room temperature conditions of NH3 (100 ppm). The resistance variation of all the sensors is 62 kΩ, 78 kΩ, 89 kΩ, and 90 kΩ respectively. The PANI@Cu3@MWCNT3 based sensor exhibited excellent results in term of resistance (90 kΩ). The stability, response time (10 s), and recovery time (13 s) of PANI@Cu2@MWCNT2 is measured and has better results in terms of time than all other sensors. Pure PANI nano-composite sensor has shown the sensing response of 18%, resistance variation of 62 kΩ, response time (45 s), recovery time (48 s) respectively. The sensing materials were characterized using FTIR, XRD, EDX, and FESEM techniques. PANI and PANI@Cu@MWCNT nanocomposites’ gas sensing capabilities were examined using a Keithley 6514 multimeter.https://doi.org/10.1038/s41598-025-01055-6PolyanilineCarbon nanotubesCopper nitrateGas sensingResponse
spellingShingle Shah Masheerul Aalam
Aaliyah Farooq
Mohd Sarvar
Mohd Nadeem Bhat
Monika Tomar
Mohammad Moeen Hasan Raza
Javid Ali
To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
Scientific Reports
Polyaniline
Carbon nanotubes
Copper nitrate
Gas sensing
Response
title To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
title_full To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
title_fullStr To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
title_full_unstemmed To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
title_short To study the performance of polyaniline-based copper and carbon-nanotube (PANI@Cu@CNT) nanocomposite for harmful NH3 gas sensing
title_sort to study the performance of polyaniline based copper and carbon nanotube pani cu cnt nanocomposite for harmful nh3 gas sensing
topic Polyaniline
Carbon nanotubes
Copper nitrate
Gas sensing
Response
url https://doi.org/10.1038/s41598-025-01055-6
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