Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics

Cellulose nanocrystals (CNC) are rod-shaped, nanoscale colloidal particles. Their strong hydrophilicity and the single functional group structure seriously have limited potential utilization in stabilizing Pickering emulsions. This study aimed to improve the emulsification ability of CNC to prepare...

Full description

Saved in:
Bibliographic Details
Main Authors: Lin LIU, Dan WANG, Qian ZHANG, Yuxian LONG, Jie TANG, Xingzhong ZHANG
Format: Article
Language:zho
Published: The editorial department of Science and Technology of Food Industry 2025-08-01
Series:Shipin gongye ke-ji
Subjects:
Online Access:http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024060395
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849330159020146688
author Lin LIU
Dan WANG
Qian ZHANG
Yuxian LONG
Jie TANG
Xingzhong ZHANG
author_facet Lin LIU
Dan WANG
Qian ZHANG
Yuxian LONG
Jie TANG
Xingzhong ZHANG
author_sort Lin LIU
collection DOAJ
description Cellulose nanocrystals (CNC) are rod-shaped, nanoscale colloidal particles. Their strong hydrophilicity and the single functional group structure seriously have limited potential utilization in stabilizing Pickering emulsions. This study aimed to improve the emulsification ability of CNC to prepare more stable emulsions. CNC and gelatin protein (GE) were combined to form complex colloidal particles, and subsequently stabilizing oil phase to fabricate stable O/W Pickering emulsions. The effects of different pH and compound ratios on the properties of CNC/GE complexes were characterized and analyzed using Zeta potential, turbidity, and Fourier transform infrared spectroscopy (FTIR). The characteristics of the obtained Pickering emulsions were investigated by morphology observation, particle size and distribution experiments. The results indicated that the CNC/GE complex colloidal particles were formed by electrostatic interaction at pH4.2, which presented excellent emulsification performance and thermal stability. With the increasing content of GE in the CNC/GE complexes, the particle size of obtained complex particles gradually decreased. When the ratio of CNC to GE in the complex was 1:5, the particle size was 305.3 nm, and when the ratio was 1:9, the particle size reduced to 258.3 nm. And their thermal stability were improved. Meanwhile, the resultant Pickering emulsions had the smaller and more uniform droplet sizes, and exhibited the enhanced storage stability. This research provides a theoretical basis for expanding the applications of cellulose/protein complexes in food-grade Pickering emulsions.
format Article
id doaj-art-0c3d93f7b5054abfa9e2a0e69a829ab0
institution Kabale University
issn 1002-0306
language zho
publishDate 2025-08-01
publisher The editorial department of Science and Technology of Food Industry
record_format Article
series Shipin gongye ke-ji
spelling doaj-art-0c3d93f7b5054abfa9e2a0e69a829ab02025-08-20T03:47:03ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062025-08-014615687510.13386/j.issn1002-0306.20240603952024060395-15Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification CharacteristicsLin LIU0Dan WANG1Qian ZHANG2Yuxian LONG3Jie TANG4Xingzhong ZHANG5School of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaSchool of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaSchool of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaSchool of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaSchool of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaSchool of Food and Bioengineering, Xihua University, Chengdu 610039, ChinaCellulose nanocrystals (CNC) are rod-shaped, nanoscale colloidal particles. Their strong hydrophilicity and the single functional group structure seriously have limited potential utilization in stabilizing Pickering emulsions. This study aimed to improve the emulsification ability of CNC to prepare more stable emulsions. CNC and gelatin protein (GE) were combined to form complex colloidal particles, and subsequently stabilizing oil phase to fabricate stable O/W Pickering emulsions. The effects of different pH and compound ratios on the properties of CNC/GE complexes were characterized and analyzed using Zeta potential, turbidity, and Fourier transform infrared spectroscopy (FTIR). The characteristics of the obtained Pickering emulsions were investigated by morphology observation, particle size and distribution experiments. The results indicated that the CNC/GE complex colloidal particles were formed by electrostatic interaction at pH4.2, which presented excellent emulsification performance and thermal stability. With the increasing content of GE in the CNC/GE complexes, the particle size of obtained complex particles gradually decreased. When the ratio of CNC to GE in the complex was 1:5, the particle size was 305.3 nm, and when the ratio was 1:9, the particle size reduced to 258.3 nm. And their thermal stability were improved. Meanwhile, the resultant Pickering emulsions had the smaller and more uniform droplet sizes, and exhibited the enhanced storage stability. This research provides a theoretical basis for expanding the applications of cellulose/protein complexes in food-grade Pickering emulsions.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024060395cellulose nanocrystalsgelatinpickering emulsionemulsification characteristics
spellingShingle Lin LIU
Dan WANG
Qian ZHANG
Yuxian LONG
Jie TANG
Xingzhong ZHANG
Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
Shipin gongye ke-ji
cellulose nanocrystals
gelatin
pickering emulsion
emulsification characteristics
title Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
title_full Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
title_fullStr Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
title_full_unstemmed Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
title_short Preparation of Pickering Emulsion Stabilized by Cellulose Nanocrystals and Gelatin and Their Emulsification Characteristics
title_sort preparation of pickering emulsion stabilized by cellulose nanocrystals and gelatin and their emulsification characteristics
topic cellulose nanocrystals
gelatin
pickering emulsion
emulsification characteristics
url http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024060395
work_keys_str_mv AT linliu preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics
AT danwang preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics
AT qianzhang preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics
AT yuxianlong preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics
AT jietang preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics
AT xingzhongzhang preparationofpickeringemulsionstabilizedbycellulosenanocrystalsandgelatinandtheiremulsificationcharacteristics