β-Tricalcium Phosphate Interferes with the Assessment of Crystallinity in Burned Skeletal Remains by Giampaolo Piga, Ana Amarante, Calil Makhoul, Eugénia Cunha, Assumpció Malgosa, Stefano Enzo, David Gonçalves

“…The main goal of this paper is to apply X-ray diffraction, partially supported by infrared attenuated total reflectance spectroscopy to determine changes in burned human bones and teeth in terms of mineral phase transformations. …”
Get full text

Branched polyethyleneimine functionalized tin(IV)-porphyrinic complex: Synthesis, characterization and application towards acid blue 25 adsorption from water by Raoudha Soury, Mahjoub Jabli, Mabrouka El Oudi, Ashanul Haque, Khalaf M. Alenezi, Ahmed Al Otaibi, Fahad Abdulaziz, Amor Bchetnia

“…The adsorbent [Sn(TPP)(Cl2)]-PEI was prepared via a swift protocol and characterized extensively using multi-nuclear spectroscopic techniques including the 1H NMR, FT-IR and UV–Vis spectroscopic techniques. X-ray diffraction (XRD) data confirmed that the addition of PEI to the Sn-porphyrin complex did not affect its crystallinity. …”
Get full text

Corrosion Mitigation with Chemical Injection in Welded Carbon Steel Pipe for Offshore Water Treatment Plant by Henry Ekene Mgbemere, Johnson Olumuyiwa Agunsoye, Kenechi Ijeoma Ojemeni, Obianuju Vivian Izuegbu

“…Biocide introduction lowered the redox potential, while oxygen scavenger made the redox potential unstable. X-ray diffraction analysis of the steel surface exposed to the seawater indicated the presence of various compounds, suggesting ongoing corrosion processes and the existence of organic and inorganic contaminants. …”
Get full text

Coconut Shell Activated Carbon/CoFe2O4 Composite for the Removal of Rhodamine B from Aqueous Solution by Le Phuong Hoang, Huu Tap Van, Thi Thuy Hang Nguyen, Van Quang Nguyen, Phan Quang Thang

“…The properties of coconut shell activated carbon (CAC) and CAC/CoFe2O4 were investigated through the usage of electron microscopic methods (SEM: Scanning Electron Microscopy, EDS: Energy Dispersive X-ray), powder X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). …”
Get full text

Comparison of CaO-NPs and Chicken Eggshell-Derived CaO in the Production of Biodiesel from Schinziophyton rautanenii (Mongongo) Nut Oil by Keene Carlvin Mmusi, Sebusi Odisitse, Florence Nareetsile

“…The catalysts were calcined at a temperature of 800°C for 3 h and characterized by scanning electron microscope-energy dispersive X-ray (SEM-EDX) where both catalysts showed agglomerated particles and high elemental composition of Ca and O. Powder X-ray diffraction (XRD) showed that CaO was present in both catalysts, and the average crystalline size obtained was 42 and 50 nm for CaO-NPs and eggshell ash, respectively. …”
Get full text

Investigation of the structure of CaO-Al2O3-SiO2 melts as a basis for the development of new agglomerated welding fluxes and industrial refractories by Sokol’skii V.E., Pruttskov D.V., Busko V.M., Kazimirov V.P., Roik O.S., Chyrkin A.D., Galinich V.I., Goncharov I.A.

“…Three samples of ternary CaO-Al2O3-SiO2 system were studied by means of high-temperature X-ray diffraction above the melting point: 23.3CaO- 14.7Al2O3-62.0SiO2 wt. % (sample 1, eutectic), 9.8CaO-19.8Al2O3-70.4SiO2 wt. % (sample 2, eutectic), 15.6 CaO- 36.5Al2O3-47.9SiO2 wt. % (sample 3). …”
Get full text

Photodegradation process for the removal of acid orange 10 using titanium dioxide and bismuth vanadate from aqueous solution by B. Rahimi, A. Ebrahimi, N. Mansouri, N. Hosseini

“…The characteristics of catalysts were determined by field emission scanning electron microscopes, X-ray diffraction and Fourier transform infrared spectroscopy. …”
Get full text

Sc-doped GeTe thin films prepared by radio-frequency magnetron sputtering by Marek Bouška, Jan Gutwirth, Kamil Bečvář, Vladimír Kucek, Stanislav Šlang, Petr Janíček, Lubomír Prokeš, Josef Havel, Virginie Nazabal, Petr Němec

“…Different characterization techniques (scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction, atomic force microscopy, sheet resistance temperature-dependent measurements, variable angle spectroscopic ellipsometry, and laser ablation time-of-flight mass spectrometry) were used to evaluate the properties of as-deposited (amorphous) and annealed (crystalline) Ge-Te-Sc thin films. …”
Get full text

Eco-friendly alkali-activated nano concrete: Impact of nano-GGBFS on mechanical and microstructural properties by Samuvel Raj R, G. Prince Arulraj, N. Anand, Balamurali Kanagaraj, Eva Lubloy

“…Microstructural studies, including Field Emission Scanning Electron Microscopy (FESEM), X-ray Diffraction (XRD), Energy Dispersive X-ray analysis (EDAX), Fourier Transform Infrared (FTIR), and Thermogravimetric Analysis (TGA), demonstrated superior geopolymerization at this optimal nGS content. …”
Get full text

Removal of Sodium Dodecylbenzenesulphonate and Cetyltrimethylammonium Bromide Using a Carbon Composite Derived from Modified Zn–Al-Layered Double Hydroxide by Rodrigo Morais Menezes dos Santos, Rosembergue Gabriel Lima Gonçalves, Marina de Carvalho Eufrásio Pinto, Roberta Gomes Prado, Vera Regina Leopoldo Constantino, Liovando Marciano da Costa, Frederico Garcia Pinto, Jairo Tronto

“…The material was characterized by powder X-ray diffraction, Fourier transform infrared/attenuated total reflectance spectroscopy, thermogravimetric analysis–differential scanning calorimetry–mass spectrometry, measurement of BET specific surface area, zeta-potential analysis and scanning electron microscopy. …”
Get full text

Electrochemical Performance of Hybrid Cationic Aqueous-Based Rechargeable Battery with Different Current Collectors and Electrolytes by Shang Chen, Fang Tang, Ting He, Huanhuan Zhang, Shanshan Deng, Yukang Li, Xianwen Wu, Qiaobao Zhang, Yanhong Xiang, Wenbin Yan

“…Different zinc foils as anode current collectors by electrowinning in various electrolytes with additives were prepared, which were evaluated through X-ray diffraction (XRD), scanning electron microscopy (SEM), float charge, and Tafel curve tests. …”
Get full text

Preparation and Photocatalytic Characterization of Modified Nano TiO2/Nd/Rice Husk Ash Material for Rifampicin Removal in Aqueous Solution by Thuy Dang Thi Ngoc, Ha Nguyen Thi, Dung Nguyen Duc, Sen Nguyen Thi, Toan Nguyen Duc, Nam Nguyen Hoang

“…The structural characteristics and photocatalytic properties of the materials were analyzed by X-ray diffraction, energy dispersive X-ray, transmission electron microscopy, scanning electron microscopy, forbidden zone energy, and specific surface area. …”
Get full text

Influence of graphene nanoplatelets (GNPs) and aluminum-carbon layered double hydroxides (Al-C LDH) in polypropylene matrix of hybrid composite structures on the microstructure and... by R. Daulath Banu, R. Karunanithi, S. Sivasankaran, B. Subramanian, Abdullah A. Alhomidan

“…The developed hybrid composites were characterized using high-resolution scanning electron microscopy (HRSEM) for microstructural analysis, X-ray diffraction (XRD) for phase identification, X-ray photoelectron spectroscopy (XPS) for compositional analysis, and Fourier-transform infrared spectroscopy (FTIR) for functional group identification. …”
Get full text

Green synthesis of metal nanoparticles, characterization, and biosensing applications by Chiravoot Pechyen, Benchamaporn Tangnorawich, Surachet Toommee, Robert Marks, Yardnapar Parcharoen

“…The importance of thorough characterization of nanoparticles is also discussed, highlighting techniques such as transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and UV–Vis spectroscopy to analyze the size, shape, surface properties, structural integrity, and optical behavior of the NPs. …”
Get full text

Construction of All Solid State Bi2MoO6/Bi2WO6@Ti3C2 MXene Heterostructure System and the Mechanism Study of the Z-scheme Photocatalysis by Dongfang Zhang, Junkun Liu, Qiang Liu, Jiaxun Wang, Yang Qu

“…The structure and properties of the as-prepared catalytic materials were analyzed by X‑ray powder diffraction (XRD), transmission electron microscope (TEM) and high-resolution TEM (HRTEM), ultraviolet‑visible diffuse reflection spectroscopy (UV‑Vis DRS), fluorescence spectroscopy (PL), X-ray photoelectron spectroscopy (XPS), N2 adsorption–desorption measurements and photoelectrochemical tests, which were performed to analyze the phase composition, microstructure, morphology, optical properties, and recombination rate of photogenerated charge of the as-prepared samples. …”
Get full text

Monodispersed AgNPs Synthesized from the Nanofactories of Theobroma cacao (Cocoa) Leaves and Pod Husk and Their Antimicrobial Activity by Johnson Kwame Efavi, Emmanuel Nyankson, Kwaku Kyeremeh, Gloria Pokuaa Manu, Kingsford Asare, Nathaniel Yeboah

“…Scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), dynamic light scattering (DLS), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR) were used to further characterize the nanoparticles. …”
Get full text

Heteronuclear Fe-Mn Cyclopentadienyl Complexes Supported on Boehmite. Thermochemistry and Thermodynamics of their Decomposition by A.I. Rustamova, R.M. Muradxanov, S.N. Osmanova, F.K. Pashayeva, A.N. Mammadov, D.B. Tagiyev, E.H. Ismailov

“…The XRD data show that when calcining at 873 K the boehmite samples with the applied compounds of the above composition and containing these compounds less than 10 wt.%, the diffraction patterns show only reflections characteristic of poorly crystallized aluminum oxide. …”
Get full text

Influence of Y–Bi–Co oxide doping on electrical performance of ZnO varistors based on simulation analysis by Zhengzheng Fu, Zongxi Zhang, Songhai Fan, Tao Cui, Donghui Luo, Yue Yin, Pengfei Meng, Jingke Guo

“…Abstract ZnO varistors doped with Y2O3, Bi2O3, and Co2O3 were analyzed for electrical performance, microstructure, phase composition, and elemental distribution using electrical performance testing, scanning electron microscopy, X‐ray diffraction, and energy dispersive spectroscopy tests. …”
Get full text

Characterization of a thermally stable red-light-emitting phosphor: synthesis, photoluminescence, and thermoluminescence studies of CsCaF3 compound doped with Eu3+ for solid-state... by N. Hema, B. Chandrasekaran, R. Kameshwaran, M. Ammal Dhanalakshmi, V. Rathina Mala, G. Annadurai, K. Ganesh Kumar, M. Vimalan, Mohammed F. Albeshr

“…To analyze the crystal structure of the synthesized phosphors, X-ray diffraction analysis was employed. Additionally, the doped sample underwent examination of surface morphology and elemental composition through Field Emission Scanning Electron Microscopy and EDAX mapping. …”
Get full text

Structural and Electrochemical Characterization of Pure LiFePO4 and Nanocomposite C-LiFePO4 Cathodes for Lithium Ion Rechargeable Batteries by Arun Kumar, R. Thomas, N. K. Karan, J. J. Saavedra-Arias, M. K. Singh, S. B. Majumder, M. S. Tomar, R. S. Katiyar

“…Structural and electrochemical properties of these materials were compared. X-ray diffraction revealed orthorhombic olivine structure. …”
Get full text