Synthesis, Characterization, X-Ray Crystallography, and Antileishmanial Activities of N-Linked and O-Linked Glycopyranosides by Haroon ur Rashid, Sher Wali Khan, Momin Khan, Akhtar Nadhman, Noor Rehman, Muhammad Tariq, Sammer Yousuf

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Structural Characterization of B-DNA d(CGTGAATTCACG)₂ in Complex with the Specific Minor Groove Binding Fluorescent Marker Hoechst 33342 by Hristina Sbirkova-Dimitrova, Rusi Rusew, Hristo Gerginov, Annie Heroux, Boris L. Shivachev

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Protocol for high-yield bacterial expression and purification of the voltage-dependent anion channel 1 for high-throughput biophysical assays by Stefano Conti Nibali, Andrea Magrì, Angela Messina, Armin Wagner, Ramona Duman, Vito De Pinto, Cristian Turato, Cristina Arrigoni, Marco Lolicato

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Remarkable Conversion of 2-Thioxo-2,3-dihydroquinazolin-4(1H)-ones into the Corresponding Quinazoline-2,4(1H,3H)-diones: Spectroscopic Analysis and X-Ray Crystallography by Adel S. El-Azab, Nasr Y. Khalil, Alaa A.-M. Abdel-Aziz

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Synthesis and Conformational Analysis of Sterically Congested (4R)-(−)-1-(2,4,6-Trimethylbenzenesulfonyl)-3-n-butyryl-4-tert-butyl-2-imidazolidinone: X-Ray Crystallography and Semiempirical Calculations by Ibrahim A. Al-Swaidan, Adel S. El-Azab, Amer M. Alanazi, Alaa A.-M. Abdel-Aziz

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Real-time data processing for serial crystallography experiments by Thomas White, Tim Schoof, Sergey Yakubov, Aleksandra Tolstikova, Philipp Middendorf, Mikhail Karnevskiy, Valerio Mariani, Alessandra Henkel, Bjarne Klopprogge, Juergen Hannappel, Dominik Oberthuer, Ivan De Gennaro Aquino, Dmitry Egorov, Anna Munke, Janina Sprenger, Guillaume Pompidor, Helena Taberman, Andrey Gruzinov, Jan Meyer, Johanna Hakanpää, Martin Gasthuber

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Agonistic anti-NKG2D antibody structure reveals unique stoichiometry and epitope compared to natural ligands by Daniel Fallon, Ching-Shin Huang, Jingya Ma, Christopher Morgan, Zhaohui Sunny Zhou

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Structural analysis of light chain-driven bispecific antibodies targeting CD47 and PD-L1 by Pauline Malinge, Xavier Chauchet, Jérémie Bourguignon, Nicolas Bosson, Sébastien Calloud, Tereza Bautzova, Marie Borlet, Mette Laursen, Vinardas Kelpsas, Nadia Rose, Franck Gueneau, Ulla Ravn, Giovanni Magistrelli, Nicolas Fischer

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Synthesis, Physicochemical Properties, and Ion Recognition Ability of Azulene-Based Bis-(Thio)Semicarbazone by Anamaria Hanganu, Catalin Maxim, Andreea Dogaru, Adrian E. Ion, Coralia Bleotu, Augustin M. Madalan, Daniela Bala, Simona Nica

Subjects: “…single-crystal X-ray crystallography…”
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Crystal Structures of <span style="font-variant: small-caps">d</span>-Lyxono-1,4-lactone and Its <i>O</i>-Tosyl Derivative by Anna Sosnowska, Jarosław Chojnacki, Justyna Samaszko-Fiertek, Janusz Madaj, Barbara Dmochowska

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L’école de cristallographie de Nancy : un hommage by Welter, Richard

“…They are specifically three “great” deceased teachers who marked my scientific formation and allowed me to be well prepared in the large field of X-ray crystallography.In this article, I want to pay tribute to the Professors Yves Dusausoy, Jean Protas and Niels Hansen and show, on a few easy examples, the relevance of their respective teachings.…”
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Cyclization Reactions Involving 2-Aminoarenetellurols and Derivatives of α,β-Unsaturated Carboxylic Acids by Jayna A. Patel, Aundrea M. Lee, Donna V. Franklin, Frank R. Fronczek, Thomas Junk

“…Selected compounds were characterized by X-ray crystallography. The present work offers access to previously unexplored organotellurium heterocycles.…”
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Synthesis, structure and π-expansion of tris(4,5-dehydro-2,3:6,7-dibenzotropone) by Yongming Xiong, Xue Lin Ma, Shilong Su, Qian Miao

“…This report presents a new synthesis of this compound using a Ni-mediated Yamamoto coupling reaction and structural analysis of it with X-ray crystallography. Interestingly, it is observed that tris(4,5-dehydro-2,3:6,7-dibenzotropone) crystallized from its solution in hexane resulting in colorless and yellow crystal polymorphs, where it adopts conformations of approximate Cs and C2 symmetry, respectively. …”
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Structure-based insights into fluorogenic RNA aptamers by Song Qianqian, Tai Xiaoqing, Ren Qianyu, Ren Aiming

“…To date, a variety of tertiary structures of fluorogenic RNA aptamers have been determined using X-ray crystallography or NMR spectroscopy. …”
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DIMETHYL N-CYANODITHIOIMINOCARBONATE AND TRIPHENYLPHOSPHINE OXIDE METAL HALIDE COMPLEXES: MOLECULAR CRYSTAL ELUCIDATION by MOUHAMADOU BIRAME DIOP, MODOU SARR, LIBASSE DIOP, ALLEN G. OLIVER, DAVID HUGHES

“… Two MX2 (M = Ni, Zn; X = Cl, Br) dimethyl N-cyanodithioiminocarbonate compounds and one CrCl2 triphenylphosphine oxide complex were isolated and elucidated by single crystal X-ray crystallography. NiCl2[(CH3S)2C═NC≡N]2 (1) features inversion-related hydrogen bonded dimers linked into chains interacting through C-H···Cl growing layers along [110] whose junction into a 3D structure is enabled by H-bonds. …”
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Scalable fabrication of an array-type fixed-target device for automated room temperature X-ray protein crystallography by Sarthak Saha, Yaozu Chen, Silvia Russi, Darya Marchany-Rivera, Aina Cohen, Sarah L. Perry

“…Abstract X-ray crystallography is one of the leading tools to analyze the 3-D structure, and therefore, function of proteins and other biological macromolecules. …”
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The S-Layer Glycome—Adding to the Sugar Coat of Bacteria by Robin Ristl, Kerstin Steiner, Kristof Zarschler, Sonja Zayni, Paul Messner, Christina Schäffer

“…As the S-layer glycome of several bacteria is unravelling, a picture of how S-layer glycoproteins are biosynthesized is evolving. X-ray crystallography experiments allowed first insights into the catalysis mechanism of selected enzymes. …”
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Insights into the Structures of DNA Damaged by Hydroxyl Radical: Crystal Structures of DNA Duplexes Containing 5-Formyluracil by Masaru Tsunoda, Takeshi Sakaue, Satoko Naito, Tomoko Sunami, Naoko Abe, Yoshihito Ueno, Akira Matsuda, Akio Takénaka

“…In order to establish the structural basis for such mutagenesis, the crystal structures of two kinds of DNA d(CGCGRATfUCGCG) with R = A/G have been determined by X-ray crystallography. The fU residues form a Watson-Crick-type pair with A and two types of pairs (wobble and reversed wobble) with G, the latter being a new type of base pair between ionized thymine base and guanine base. …”
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Proteomics and Its Current Application in Biomedical Area: Concise Review by Semira Gobena, Bemrew Admassu, Mebrie Zemene Kinde, Abebe Tesfaye Gessese

“…Various sophisticated techniques are employed in proteomics, including polyacrylamide gel electrophoresis, mass spectrometry analysis, NMR spectroscopy, protein microarray, X-ray crystallography, and Edman sequencing. These methods collectively contribute to the comprehensive understanding of proteins and their roles in health and disease. …”
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Concise Synthesis of Naphthalene-Based 14-Aza-12-Oxasteroids by Smriti Srivastava, Jun Luo, Daniel Whalen, Katherine N. Robertson, Amitabh Jha

“…A series of 14-aza-12-oxasteroids were synthesized using our developed synthetic strategy in moderate yields, and the structure of one of the final products, 12a-Methyl-11-phenyl-11,12a-dihydro-1<i>H</i>-naphtho[2,1-d]pyrrolo[2,1-b][1,3]oxazin-3(2<i>H</i>)-one, was further confirmed by single crystal X-ray crystallography.…”
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