Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants

The aim of this study was to compare the mechanical and physicochemical properties of Ti6Al4V alloy samples produced using 3D printing (Direct Metal Laser Sintering) and bar after plastic working. Both sets of samples were subjected to various surface-processing methods, including sandblasting, heat...

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Main Authors: Wojciech Kajzer, Gabriela Wielgus, Anita Kajzer
Format: Article
Language:English
Published: MDPI AG 2024-11-01
Series:Applied Sciences
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Online Access:https://www.mdpi.com/2076-3417/14/23/11181
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author Wojciech Kajzer
Gabriela Wielgus
Anita Kajzer
author_facet Wojciech Kajzer
Gabriela Wielgus
Anita Kajzer
author_sort Wojciech Kajzer
collection DOAJ
description The aim of this study was to compare the mechanical and physicochemical properties of Ti6Al4V alloy samples produced using 3D printing (Direct Metal Laser Sintering) and bar after plastic working. Both sets of samples were subjected to various surface-processing methods, including sandblasting, heat treatment (hardening for 120 min at 820 ± 10 °C, followed by cooling to room temperature), mechanical polishing, and steam sterilization. This research included macroscopic surface evaluation before and after pitting corrosion resistance tests, metallographic microscopic research, scanning electron microscopy, and energy-dispersive spectroscopy, as well as measurements of hardness, roughness, and surface wettability. The results showed that heat and surface treatment (grinding and mechanical polishing) significantly increased the material’s hardness and corrosion resistance. Furthermore, the steam sterilization process had a positive effect by increasing surface wettability, which is important for biomedical applications, as higher wettability promotes better integration with biological tissues. This is especially relevant in implantology, where surface properties influence osseointegration and overall biocompatibility. In summary, these findings indicate that the selection of manufacturing method and the application of subsequent treatment processes significantly affect the mechanical and physicochemical properties of Ti6Al4V alloy, thereby influencing its performance and suitability for diverse engineering and biomedical applications.
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spelling doaj-art-ff92eca34bde40508e40a9cfaae55f6f2024-12-13T16:23:05ZengMDPI AGApplied Sciences2076-34172024-11-0114231118110.3390/app142311181Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics ImplantsWojciech Kajzer0Gabriela Wielgus1Anita Kajzer2Department of Biomaterials and Medical Devices Engineering, Faculty of Biomedical Engineering, Silesian University of Technology, Roosevelta 40 Street, 41-800 Zabrze, PolandDepartment of Biomaterials and Medical Devices Engineering, Faculty of Biomedical Engineering, Silesian University of Technology, Roosevelta 40 Street, 41-800 Zabrze, PolandDepartment of Biomaterials and Medical Devices Engineering, Faculty of Biomedical Engineering, Silesian University of Technology, Roosevelta 40 Street, 41-800 Zabrze, PolandThe aim of this study was to compare the mechanical and physicochemical properties of Ti6Al4V alloy samples produced using 3D printing (Direct Metal Laser Sintering) and bar after plastic working. Both sets of samples were subjected to various surface-processing methods, including sandblasting, heat treatment (hardening for 120 min at 820 ± 10 °C, followed by cooling to room temperature), mechanical polishing, and steam sterilization. This research included macroscopic surface evaluation before and after pitting corrosion resistance tests, metallographic microscopic research, scanning electron microscopy, and energy-dispersive spectroscopy, as well as measurements of hardness, roughness, and surface wettability. The results showed that heat and surface treatment (grinding and mechanical polishing) significantly increased the material’s hardness and corrosion resistance. Furthermore, the steam sterilization process had a positive effect by increasing surface wettability, which is important for biomedical applications, as higher wettability promotes better integration with biological tissues. This is especially relevant in implantology, where surface properties influence osseointegration and overall biocompatibility. In summary, these findings indicate that the selection of manufacturing method and the application of subsequent treatment processes significantly affect the mechanical and physicochemical properties of Ti6Al4V alloy, thereby influencing its performance and suitability for diverse engineering and biomedical applications.https://www.mdpi.com/2076-3417/14/23/11181Ti6Al4V titanium alloymechanical propertiesphysicochemical propertiessteam sterilizationheat treatmentgrinding and mechanical polishing
spellingShingle Wojciech Kajzer
Gabriela Wielgus
Anita Kajzer
Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
Applied Sciences
Ti6Al4V titanium alloy
mechanical properties
physicochemical properties
steam sterilization
heat treatment
grinding and mechanical polishing
title Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
title_full Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
title_fullStr Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
title_full_unstemmed Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
title_short Mechanical and Physicochemical Properties of Ti6Al4V Alloy After Plastic Working and 3D Printing Intended for Orthopedics Implants
title_sort mechanical and physicochemical properties of ti6al4v alloy after plastic working and 3d printing intended for orthopedics implants
topic Ti6Al4V titanium alloy
mechanical properties
physicochemical properties
steam sterilization
heat treatment
grinding and mechanical polishing
url https://www.mdpi.com/2076-3417/14/23/11181
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AT gabrielawielgus mechanicalandphysicochemicalpropertiesofti6al4valloyafterplasticworkingand3dprintingintendedfororthopedicsimplants
AT anitakajzer mechanicalandphysicochemicalpropertiesofti6al4valloyafterplasticworkingand3dprintingintendedfororthopedicsimplants