Hydroxyapatite composites with multiwalled carbon nanotubes

The structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotube...

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Main Authors: Ewa Skwarek, Yuliia Bolbukh, Władysław Janusz, Valentyn Tertykh
Format: Article
Language:English
Published: SAGE Publishing 2017-06-01
Series:Adsorption Science & Technology
Online Access:https://doi.org/10.1177/0263617417700637
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author Ewa Skwarek
Yuliia Bolbukh
Władysław Janusz
Valentyn Tertykh
author_facet Ewa Skwarek
Yuliia Bolbukh
Władysław Janusz
Valentyn Tertykh
author_sort Ewa Skwarek
collection DOAJ
description The structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotubes. An influence of nature of functional groups of the nanotubes boundary layer on a crystallinity of the inorganic part was evaluated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Morphology of composites obtained was studied by nitrogen adsorption/desorption technique and scanning electron microscopy. The hydroxyapatite/nanotubes interface was characterised using electrochemical methods. The parameters of the electrical double layer: A density of surface charge versus pH, zeta potential versus pH were described. The study has shown that the synthesis of hydroxyapatite/nanotube composites by formation of inorganic part in the presence of carbon filler significantly affect the microstructure, phase composition, crystallinity, hydroxyl content, chemical composition of the mineral part, as well as thermal properties and electrokinetic properties of composite.
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id doaj-art-f4f5e467853e446c98fd5c4a5aaf8e0c
institution Kabale University
issn 0263-6174
2048-4038
language English
publishDate 2017-06-01
publisher SAGE Publishing
record_format Article
series Adsorption Science & Technology
spelling doaj-art-f4f5e467853e446c98fd5c4a5aaf8e0c2025-01-02T22:37:25ZengSAGE PublishingAdsorption Science & Technology0263-61742048-40382017-06-013510.1177/0263617417700637Hydroxyapatite composites with multiwalled carbon nanotubesEwa SkwarekYuliia BolbukhWładysław JanuszValentyn TertykhThe structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotubes. An influence of nature of functional groups of the nanotubes boundary layer on a crystallinity of the inorganic part was evaluated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Morphology of composites obtained was studied by nitrogen adsorption/desorption technique and scanning electron microscopy. The hydroxyapatite/nanotubes interface was characterised using electrochemical methods. The parameters of the electrical double layer: A density of surface charge versus pH, zeta potential versus pH were described. The study has shown that the synthesis of hydroxyapatite/nanotube composites by formation of inorganic part in the presence of carbon filler significantly affect the microstructure, phase composition, crystallinity, hydroxyl content, chemical composition of the mineral part, as well as thermal properties and electrokinetic properties of composite.https://doi.org/10.1177/0263617417700637
spellingShingle Ewa Skwarek
Yuliia Bolbukh
Władysław Janusz
Valentyn Tertykh
Hydroxyapatite composites with multiwalled carbon nanotubes
Adsorption Science & Technology
title Hydroxyapatite composites with multiwalled carbon nanotubes
title_full Hydroxyapatite composites with multiwalled carbon nanotubes
title_fullStr Hydroxyapatite composites with multiwalled carbon nanotubes
title_full_unstemmed Hydroxyapatite composites with multiwalled carbon nanotubes
title_short Hydroxyapatite composites with multiwalled carbon nanotubes
title_sort hydroxyapatite composites with multiwalled carbon nanotubes
url https://doi.org/10.1177/0263617417700637
work_keys_str_mv AT ewaskwarek hydroxyapatitecompositeswithmultiwalledcarbonnanotubes
AT yuliiabolbukh hydroxyapatitecompositeswithmultiwalledcarbonnanotubes
AT władysławjanusz hydroxyapatitecompositeswithmultiwalledcarbonnanotubes
AT valentyntertykh hydroxyapatitecompositeswithmultiwalledcarbonnanotubes