Hydroxyapatite composites with multiwalled carbon nanotubes
The structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotube...
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Format: | Article |
Language: | English |
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SAGE Publishing
2017-06-01
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Series: | Adsorption Science & Technology |
Online Access: | https://doi.org/10.1177/0263617417700637 |
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author | Ewa Skwarek Yuliia Bolbukh Władysław Janusz Valentyn Tertykh |
author_facet | Ewa Skwarek Yuliia Bolbukh Władysław Janusz Valentyn Tertykh |
author_sort | Ewa Skwarek |
collection | DOAJ |
description | The structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotubes. An influence of nature of functional groups of the nanotubes boundary layer on a crystallinity of the inorganic part was evaluated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Morphology of composites obtained was studied by nitrogen adsorption/desorption technique and scanning electron microscopy. The hydroxyapatite/nanotubes interface was characterised using electrochemical methods. The parameters of the electrical double layer: A density of surface charge versus pH, zeta potential versus pH were described. The study has shown that the synthesis of hydroxyapatite/nanotube composites by formation of inorganic part in the presence of carbon filler significantly affect the microstructure, phase composition, crystallinity, hydroxyl content, chemical composition of the mineral part, as well as thermal properties and electrokinetic properties of composite. |
format | Article |
id | doaj-art-f4f5e467853e446c98fd5c4a5aaf8e0c |
institution | Kabale University |
issn | 0263-6174 2048-4038 |
language | English |
publishDate | 2017-06-01 |
publisher | SAGE Publishing |
record_format | Article |
series | Adsorption Science & Technology |
spelling | doaj-art-f4f5e467853e446c98fd5c4a5aaf8e0c2025-01-02T22:37:25ZengSAGE PublishingAdsorption Science & Technology0263-61742048-40382017-06-013510.1177/0263617417700637Hydroxyapatite composites with multiwalled carbon nanotubesEwa SkwarekYuliia BolbukhWładysław JanuszValentyn TertykhThe structure of composites based on hydroxyapatite filled with multiwalled carbon nanotubes was investigated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Hydroxyapatite was prepared by the wet synthesis in the presence of pristine and oxidised carbon nanotubes. An influence of nature of functional groups of the nanotubes boundary layer on a crystallinity of the inorganic part was evaluated using differential scanning calorimetry analysis and X-ray diffraction spectroscopy. Morphology of composites obtained was studied by nitrogen adsorption/desorption technique and scanning electron microscopy. The hydroxyapatite/nanotubes interface was characterised using electrochemical methods. The parameters of the electrical double layer: A density of surface charge versus pH, zeta potential versus pH were described. The study has shown that the synthesis of hydroxyapatite/nanotube composites by formation of inorganic part in the presence of carbon filler significantly affect the microstructure, phase composition, crystallinity, hydroxyl content, chemical composition of the mineral part, as well as thermal properties and electrokinetic properties of composite.https://doi.org/10.1177/0263617417700637 |
spellingShingle | Ewa Skwarek Yuliia Bolbukh Władysław Janusz Valentyn Tertykh Hydroxyapatite composites with multiwalled carbon nanotubes Adsorption Science & Technology |
title | Hydroxyapatite composites with multiwalled carbon nanotubes |
title_full | Hydroxyapatite composites with multiwalled carbon nanotubes |
title_fullStr | Hydroxyapatite composites with multiwalled carbon nanotubes |
title_full_unstemmed | Hydroxyapatite composites with multiwalled carbon nanotubes |
title_short | Hydroxyapatite composites with multiwalled carbon nanotubes |
title_sort | hydroxyapatite composites with multiwalled carbon nanotubes |
url | https://doi.org/10.1177/0263617417700637 |
work_keys_str_mv | AT ewaskwarek hydroxyapatitecompositeswithmultiwalledcarbonnanotubes AT yuliiabolbukh hydroxyapatitecompositeswithmultiwalledcarbonnanotubes AT władysławjanusz hydroxyapatitecompositeswithmultiwalledcarbonnanotubes AT valentyntertykh hydroxyapatitecompositeswithmultiwalledcarbonnanotubes |