Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan

The antibacterial AgNPs@PVA/MC composite films were prepared by using methyl cellulose (MC) and polyvinyl alcohol (PVA) as composite substrate, nanosilver (AgNPs) as antibacterial agent, and glycerin as plasticizer. The effects of different mass fractions (0%, 0.05%, 0.1%, 0.2%, 0.3%) of AgNPs on th...

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Main Authors: Shuaishuai DAI, Weijie WU, Xiangjun FANG, Hangjun CHEN, Jun HUANG, Ruiling LIU, Huizhi CHEN, Ben NIU, Haiyan GAO
Format: Article
Language:zho
Published: The editorial department of Science and Technology of Food Industry 2025-01-01
Series:Shipin gongye ke-ji
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Online Access:http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024010317
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author Shuaishuai DAI
Weijie WU
Xiangjun FANG
Hangjun CHEN
Jun HUANG
Ruiling LIU
Huizhi CHEN
Ben NIU
Haiyan GAO
author_facet Shuaishuai DAI
Weijie WU
Xiangjun FANG
Hangjun CHEN
Jun HUANG
Ruiling LIU
Huizhi CHEN
Ben NIU
Haiyan GAO
author_sort Shuaishuai DAI
collection DOAJ
description The antibacterial AgNPs@PVA/MC composite films were prepared by using methyl cellulose (MC) and polyvinyl alcohol (PVA) as composite substrate, nanosilver (AgNPs) as antibacterial agent, and glycerin as plasticizer. The effects of different mass fractions (0%, 0.05%, 0.1%, 0.2%, 0.3%) of AgNPs on the properties of the composite films were investigated, and its appearance, mechanical properties, microstructure and antibacterial properties were characterized, in order to provide theoretical support for the development of preservation materials for storing Ougan. The results showed that as the content of AgNPs increased, the inhibitory effect of the composite film on the growth of Penicillium citrinum became more significant (P<0.05). Among them, the composite film with 0.1% AgNPs content had the best comprehensive performance, its tensile strength reached 12.45 MPa, elongation at break was 6.47%, water vapor permeability was 21.03×10−6 g·mm/(m2·s·Pa), and oxygen permeability was 2.31×10−6 cm3/(cm2·s·Pa). Scanning electron microscopy (SEM) showed that composite film with 0.1% AgNPs content was regular, compact and evenly distributed in cross section. Infrared spectroscopy and thermogravimetric analysis showed that composite film with 0.1% AgNPs content had good bonding and thermal stability. 0.1%AgNPs@PVA/MC composite film could effectively reduce the weight loss rate of Ougan during storage, and reduce the consumption rate of soluble solid, titratable acid and VC, delay the maturation of Ougan and significantly inhibit the growth of Penicillium citrinum, which could better maintain the quality of Ougan during the storage period, this study provided support for the sustainable development of Ougan industry.
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spelling doaj-art-da2118d4f6cf426e99499ca33a8b898d2025-01-10T06:49:17ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062025-01-0146134935810.13386/j.issn1002-0306.20240103172024010317-1Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of OuganShuaishuai DAI0Weijie WU1Xiangjun FANG2Hangjun CHEN3Jun HUANG4Ruiling LIU5Huizhi CHEN6Ben NIU7Haiyan GAO8School of Biological & Chemical Engineering, Zhejiang University of Science & Technology,Hangzhou 310023, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaSchool of Biological & Chemical Engineering, Zhejiang University of Science & Technology,Hangzhou 310023, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaInstitute of Food Science, Zhejiang Academy of Agricultural Sciences, Key Laboratory of Post-Harvest Fruit Processing, Key Laboratory of Post-Harvest Vegetable Preservation and Processing, Ministry of Agriculture and Rural Affairs, Zhejiang Key Laboratory of Intelligent Food Logistic and Processing, Key Laboratory of Light Industry Fruit and Vegetable Preservation and Processing, Hangzhou 310021, ChinaThe antibacterial AgNPs@PVA/MC composite films were prepared by using methyl cellulose (MC) and polyvinyl alcohol (PVA) as composite substrate, nanosilver (AgNPs) as antibacterial agent, and glycerin as plasticizer. The effects of different mass fractions (0%, 0.05%, 0.1%, 0.2%, 0.3%) of AgNPs on the properties of the composite films were investigated, and its appearance, mechanical properties, microstructure and antibacterial properties were characterized, in order to provide theoretical support for the development of preservation materials for storing Ougan. The results showed that as the content of AgNPs increased, the inhibitory effect of the composite film on the growth of Penicillium citrinum became more significant (P<0.05). Among them, the composite film with 0.1% AgNPs content had the best comprehensive performance, its tensile strength reached 12.45 MPa, elongation at break was 6.47%, water vapor permeability was 21.03×10−6 g·mm/(m2·s·Pa), and oxygen permeability was 2.31×10−6 cm3/(cm2·s·Pa). Scanning electron microscopy (SEM) showed that composite film with 0.1% AgNPs content was regular, compact and evenly distributed in cross section. Infrared spectroscopy and thermogravimetric analysis showed that composite film with 0.1% AgNPs content had good bonding and thermal stability. 0.1%AgNPs@PVA/MC composite film could effectively reduce the weight loss rate of Ougan during storage, and reduce the consumption rate of soluble solid, titratable acid and VC, delay the maturation of Ougan and significantly inhibit the growth of Penicillium citrinum, which could better maintain the quality of Ougan during the storage period, this study provided support for the sustainable development of Ougan industry.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024010317ougan (citrus reticulata cv. suavissima)composite filmnanosilvermethyl cellulosepolyvinyl alcoholstoragequality
spellingShingle Shuaishuai DAI
Weijie WU
Xiangjun FANG
Hangjun CHEN
Jun HUANG
Ruiling LIU
Huizhi CHEN
Ben NIU
Haiyan GAO
Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
Shipin gongye ke-ji
ougan (citrus reticulata cv. suavissima)
composite film
nanosilver
methyl cellulose
polyvinyl alcohol
storage
quality
title Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
title_full Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
title_fullStr Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
title_full_unstemmed Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
title_short Preparation of Composite Films Based on Methyl Cellulose/Polyvinyl Alcohol-loaded Nanosilver (AgNPs@PVA/MC) and Its Effect on Storage Quality of Ougan
title_sort preparation of composite films based on methyl cellulose polyvinyl alcohol loaded nanosilver agnps pva mc and its effect on storage quality of ougan
topic ougan (citrus reticulata cv. suavissima)
composite film
nanosilver
methyl cellulose
polyvinyl alcohol
storage
quality
url http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2024010317
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