Lithium extraction by extractant confined in Pickering emulsion

Abstract The global energy transformation towards electrification and decarbonization urgently requires a sustainable lithium supply. However, current solvent extraction technology suffers from extractant dissolution and low efficiency. Herein, we develop an oil-in-water (O/W) Pickering emulsion wit...

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Main Authors: Enze Li, Zelong Li, Qiancheng Xia, Feiyu Zhang, Zhangqi Liang, Zhaozan Xu, Guandao Gao, Hu Li, Fangqin Cheng
Format: Article
Language:English
Published: Nature Portfolio 2025-08-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-62927-z
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author Enze Li
Zelong Li
Qiancheng Xia
Feiyu Zhang
Zhangqi Liang
Zhaozan Xu
Guandao Gao
Hu Li
Fangqin Cheng
author_facet Enze Li
Zelong Li
Qiancheng Xia
Feiyu Zhang
Zhangqi Liang
Zhaozan Xu
Guandao Gao
Hu Li
Fangqin Cheng
author_sort Enze Li
collection DOAJ
description Abstract The global energy transformation towards electrification and decarbonization urgently requires a sustainable lithium supply. However, current solvent extraction technology suffers from extractant dissolution and low efficiency. Herein, we develop an oil-in-water (O/W) Pickering emulsion with high stability using amphipathic SiO2 nanoparticles to confine tributyl phosphate (TBP) extractant within the oil phase for enhancing lithium extraction from salt-lake brine. Resultantly, the Pickering emulsion achieves a lithium recovery of 91.7% with Li-Mg separation factor (β Li Mg) of 101.9 after only three-stage extraction and Li+ mass transfer rate (k) of 4.57 × 10−8 m/s, greatly outperforming the traditional TBP system (52.8% recovery, β Li Mg = 12, k = 7.50 × 10−9 m/s). We propose that the tiny gaps between SiO2 particles serve as Li+ transport channels, in which the interfacial electric field generated by surface charges of SiO2 particles and the confinement effect within these gaps synergistically enhance Li+ dehydration and diffusion.
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id doaj-art-d6d332f36dae4b16a235411c3c47fcf9
institution Kabale University
issn 2041-1723
language English
publishDate 2025-08-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-d6d332f36dae4b16a235411c3c47fcf92025-08-20T03:42:55ZengNature PortfolioNature Communications2041-17232025-08-011611910.1038/s41467-025-62927-zLithium extraction by extractant confined in Pickering emulsionEnze Li0Zelong Li1Qiancheng Xia2Feiyu Zhang3Zhangqi Liang4Zhaozan Xu5Guandao Gao6Hu Li7Fangqin Cheng8Institute of Resources and Environmental Engineering, State Environmental Protection Key Laboratory of Efficient Utilization Technology of Coal Waste Resources, Shanxi Laboratory of Yellow River, Shanxi UniversityInstitute of Resources and Environmental Engineering, State Environmental Protection Key Laboratory of Efficient Utilization Technology of Coal Waste Resources, Shanxi Laboratory of Yellow River, Shanxi UniversityState Key Laboratory of Pollution Control and Resource Reuse, School of Environment, Nanjing UniversityState Key Laboratory of Pollution Control and Resource Reuse, School of Environment, Nanjing UniversityState Key Laboratory of Pollution Control and Resource Reuse, School of Environment, Nanjing UniversityInstitute of Resources and Environmental Engineering, State Environmental Protection Key Laboratory of Efficient Utilization Technology of Coal Waste Resources, Shanxi Laboratory of Yellow River, Shanxi UniversityState Key Laboratory of Pollution Control and Resource Reuse, School of Environment, Nanjing UniversityQinghai Jintai Lithium Industry Co., LTDInstitute of Resources and Environmental Engineering, State Environmental Protection Key Laboratory of Efficient Utilization Technology of Coal Waste Resources, Shanxi Laboratory of Yellow River, Shanxi UniversityAbstract The global energy transformation towards electrification and decarbonization urgently requires a sustainable lithium supply. However, current solvent extraction technology suffers from extractant dissolution and low efficiency. Herein, we develop an oil-in-water (O/W) Pickering emulsion with high stability using amphipathic SiO2 nanoparticles to confine tributyl phosphate (TBP) extractant within the oil phase for enhancing lithium extraction from salt-lake brine. Resultantly, the Pickering emulsion achieves a lithium recovery of 91.7% with Li-Mg separation factor (β Li Mg) of 101.9 after only three-stage extraction and Li+ mass transfer rate (k) of 4.57 × 10−8 m/s, greatly outperforming the traditional TBP system (52.8% recovery, β Li Mg = 12, k = 7.50 × 10−9 m/s). We propose that the tiny gaps between SiO2 particles serve as Li+ transport channels, in which the interfacial electric field generated by surface charges of SiO2 particles and the confinement effect within these gaps synergistically enhance Li+ dehydration and diffusion.https://doi.org/10.1038/s41467-025-62927-z
spellingShingle Enze Li
Zelong Li
Qiancheng Xia
Feiyu Zhang
Zhangqi Liang
Zhaozan Xu
Guandao Gao
Hu Li
Fangqin Cheng
Lithium extraction by extractant confined in Pickering emulsion
Nature Communications
title Lithium extraction by extractant confined in Pickering emulsion
title_full Lithium extraction by extractant confined in Pickering emulsion
title_fullStr Lithium extraction by extractant confined in Pickering emulsion
title_full_unstemmed Lithium extraction by extractant confined in Pickering emulsion
title_short Lithium extraction by extractant confined in Pickering emulsion
title_sort lithium extraction by extractant confined in pickering emulsion
url https://doi.org/10.1038/s41467-025-62927-z
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AT zelongli lithiumextractionbyextractantconfinedinpickeringemulsion
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AT feiyuzhang lithiumextractionbyextractantconfinedinpickeringemulsion
AT zhangqiliang lithiumextractionbyextractantconfinedinpickeringemulsion
AT zhaozanxu lithiumextractionbyextractantconfinedinpickeringemulsion
AT guandaogao lithiumextractionbyextractantconfinedinpickeringemulsion
AT huli lithiumextractionbyextractantconfinedinpickeringemulsion
AT fangqincheng lithiumextractionbyextractantconfinedinpickeringemulsion