Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract

Astragalus glycyphyllos L. is widely used in Bulgarian folk medicine. Extracts from this plant have antiproliferative, antitumor and immune stimulating effects in vitro and in vivo. The aim of this study was to examine the potential antiviral activity of a standardized extract from the aerial parts...

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Main Authors: Aleksandar Shkondrov, Anton Hinkov, Venelin Cvetkov, Kalina Shishkova, Daniel Todorov, Stoyan Shishkov, Ivan Stambolov, Krassimira Yoncheva, Ilina Krasteva
Format: Article
Language:English
Published: Taylor & Francis Group 2023-03-01
Series:Biotechnology & Biotechnological Equipment
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Online Access:https://www.tandfonline.com/doi/10.1080/13102818.2023.2221752
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author Aleksandar Shkondrov
Anton Hinkov
Venelin Cvetkov
Kalina Shishkova
Daniel Todorov
Stoyan Shishkov
Ivan Stambolov
Krassimira Yoncheva
Ilina Krasteva
author_facet Aleksandar Shkondrov
Anton Hinkov
Venelin Cvetkov
Kalina Shishkova
Daniel Todorov
Stoyan Shishkov
Ivan Stambolov
Krassimira Yoncheva
Ilina Krasteva
author_sort Aleksandar Shkondrov
collection DOAJ
description Astragalus glycyphyllos L. is widely used in Bulgarian folk medicine. Extracts from this plant have antiproliferative, antitumor and immune stimulating effects in vitro and in vivo. The aim of this study was to examine the potential antiviral activity of a standardized extract from the aerial parts of the plant and to formulate it in a suitable dosage form. A dry extract was obtained, and its phytochemical composition was determined by ultra-high-performance liquid chromatography–high resolution electrospray ionization mass spectrometry (UHPLC-HRESIMS). The extract contained flavonoids and predominantly saponins. 17(R),20(R)-3β,6α,16β-trihydroxycycloartanyl-23-carboxylic acid 16-lactone 3-O-β-D-glucopyranoside was used as a reference for quantitation. The extract had 3% saponins. The antiviral activity of the extract was tested against Simplexvirus humanalpha type 1 (acyclovir sensitive) and 2 (acyclovir resistant) in vitro. Between 60% and 70% of protection was reached against both virus strains when the extract (at the maximal non-toxic concentration of 0.6 mg/mL) was added simultaneously with and 1 h after Madine and Darby bovine kidney cell inoculation. The extract was also tested in combination with acyclovir only against Simplexvirus humanalpha type 1, in vitro. Further, the lyophilized extract was mixed with appropriate excipients aiming to prepare tablets via direct compaction. The optimized tablets fulfilled the requirements of the pharmacopoeia for disintegration and friability. Thus, the study demonstrated the possibility to formulate a standardized extract of A. glycyphyllos in tablets and their potential for adjuvant antiviral application in further trials.
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publishDate 2023-03-01
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series Biotechnology & Biotechnological Equipment
spelling doaj-art-cc78a47e98c74bd9aecd8d9f0c2439ea2024-11-25T09:24:35ZengTaylor & Francis GroupBiotechnology & Biotechnological Equipment1310-28181314-35302023-03-0137110.1080/13102818.2023.2221752Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extractAleksandar Shkondrov0Anton Hinkov1Venelin Cvetkov2Kalina Shishkova3Daniel Todorov4Stoyan Shishkov5Ivan Stambolov6Krassimira Yoncheva7Ilina Krasteva8Department of Pharmacognosy, Faculty of Pharmacy, Medical University of Sofia, Sofia, BulgariaLaboratory of Virology, Faculty of Biology, University of Sofia “St. Kl. Ohridski”, Sofia, BulgariaLaboratory of Virology, Faculty of Biology, University of Sofia “St. Kl. Ohridski”, Sofia, BulgariaLaboratory of Virology, Faculty of Biology, University of Sofia “St. Kl. Ohridski”, Sofia, BulgariaLaboratory of Virology, Faculty of Biology, University of Sofia “St. Kl. Ohridski”, Sofia, BulgariaLaboratory of Virology, Faculty of Biology, University of Sofia “St. Kl. Ohridski”, Sofia, BulgariaDepartment of Pharmacognosy, Faculty of Pharmacy, Medical University of Sofia, Sofia, BulgariaDepartment of Pharmaceutical Technology and Biopharmaceutics, Faculty of Pharmacy, Medical University of Sofia, Sofia, BulgariaDepartment of Pharmacognosy, Faculty of Pharmacy, Medical University of Sofia, Sofia, BulgariaAstragalus glycyphyllos L. is widely used in Bulgarian folk medicine. Extracts from this plant have antiproliferative, antitumor and immune stimulating effects in vitro and in vivo. The aim of this study was to examine the potential antiviral activity of a standardized extract from the aerial parts of the plant and to formulate it in a suitable dosage form. A dry extract was obtained, and its phytochemical composition was determined by ultra-high-performance liquid chromatography–high resolution electrospray ionization mass spectrometry (UHPLC-HRESIMS). The extract contained flavonoids and predominantly saponins. 17(R),20(R)-3β,6α,16β-trihydroxycycloartanyl-23-carboxylic acid 16-lactone 3-O-β-D-glucopyranoside was used as a reference for quantitation. The extract had 3% saponins. The antiviral activity of the extract was tested against Simplexvirus humanalpha type 1 (acyclovir sensitive) and 2 (acyclovir resistant) in vitro. Between 60% and 70% of protection was reached against both virus strains when the extract (at the maximal non-toxic concentration of 0.6 mg/mL) was added simultaneously with and 1 h after Madine and Darby bovine kidney cell inoculation. The extract was also tested in combination with acyclovir only against Simplexvirus humanalpha type 1, in vitro. Further, the lyophilized extract was mixed with appropriate excipients aiming to prepare tablets via direct compaction. The optimized tablets fulfilled the requirements of the pharmacopoeia for disintegration and friability. Thus, the study demonstrated the possibility to formulate a standardized extract of A. glycyphyllos in tablets and their potential for adjuvant antiviral application in further trials.https://www.tandfonline.com/doi/10.1080/13102818.2023.2221752Tablet formulationantiviral activitysaponinsAstragalus glycyphyllosstandardizationSimplexvirus humanalpha type 1 and 2
spellingShingle Aleksandar Shkondrov
Anton Hinkov
Venelin Cvetkov
Kalina Shishkova
Daniel Todorov
Stoyan Shishkov
Ivan Stambolov
Krassimira Yoncheva
Ilina Krasteva
Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
Biotechnology & Biotechnological Equipment
Tablet formulation
antiviral activity
saponins
Astragalus glycyphyllos
standardization
Simplexvirus humanalpha type 1 and 2
title Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
title_full Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
title_fullStr Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
title_full_unstemmed Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
title_short Astragalus glycyphyllos L.: antiviral activity and tablet dosage formulation of a standardized dry extract
title_sort astragalus glycyphyllos l antiviral activity and tablet dosage formulation of a standardized dry extract
topic Tablet formulation
antiviral activity
saponins
Astragalus glycyphyllos
standardization
Simplexvirus humanalpha type 1 and 2
url https://www.tandfonline.com/doi/10.1080/13102818.2023.2221752
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