In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions
The hydrogen evolution reaction is important in energy conversion and storage. This has led to the design of different types of catalysts and production setups. Understanding the status of the catalysts and reaction mechanisms motivated researchers to adopt the operando/in situ techniques. Herein,...
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International Association of Physical Chemists (IAPC)
2024-12-01
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| Series: | Journal of Electrochemical Science and Engineering |
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| Online Access: | https://pub.iapchem.org/ojs/index.php/JESE/article/view/2526 |
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| author | Anaclet Nsabimana Yiran Guan Guobao Xu |
| author_facet | Anaclet Nsabimana Yiran Guan Guobao Xu |
| author_sort | Anaclet Nsabimana |
| collection | DOAJ |
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The hydrogen evolution reaction is important in energy conversion and storage. This has led to the design of different types of catalysts and production setups. Understanding the status of the catalysts and reaction mechanisms motivated researchers to adopt the operando/in situ techniques. Herein, we present a brief overview of the recent (from 2020) advances in the use of in situ and operando characterization techniques, such as in situ X-ray absorption spectroscopy, X-ray photoelectron spectroscopy, X-ray diffraction analysis, IR spectroscopy, electrochemical Raman spectroscopy, online inductively coupled plasma - mass spectroscopy, differential electrochemical mass spectroscopy, optical microscopy, electron microscopy, electrochemical atomic microscopy, electrochemical scanning tunneling microscopy, and scanning electrochemical microscopy, in the electrochemical hydrogen evolution reaction. Representative examples of the applications of these techniques are also provided. Challenges in this field and future perspectives are discussed.
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| format | Article |
| id | doaj-art-c7f9ab3e446743cea49519742a680925 |
| institution | Kabale University |
| issn | 1847-9286 |
| language | English |
| publishDate | 2024-12-01 |
| publisher | International Association of Physical Chemists (IAPC) |
| record_format | Article |
| series | Journal of Electrochemical Science and Engineering |
| spelling | doaj-art-c7f9ab3e446743cea49519742a6809252025-01-10T07:35:57ZengInternational Association of Physical Chemists (IAPC)Journal of Electrochemical Science and Engineering1847-92862024-12-0110.5599/jese.2526In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactionsAnaclet Nsabimana0Yiran Guan1Guobao Xu2Chemistry Department, College of Science and Technology, University of Rwanda, P.O. Box: 3900, Kigali, RwandaState Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Jilin 130022, ChinaState Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Jilin 130022, China and School of Chemistry and Applied Engineering, University of Science and Technology of China, Hefei, Anhui 230026, China The hydrogen evolution reaction is important in energy conversion and storage. This has led to the design of different types of catalysts and production setups. Understanding the status of the catalysts and reaction mechanisms motivated researchers to adopt the operando/in situ techniques. Herein, we present a brief overview of the recent (from 2020) advances in the use of in situ and operando characterization techniques, such as in situ X-ray absorption spectroscopy, X-ray photoelectron spectroscopy, X-ray diffraction analysis, IR spectroscopy, electrochemical Raman spectroscopy, online inductively coupled plasma - mass spectroscopy, differential electrochemical mass spectroscopy, optical microscopy, electron microscopy, electrochemical atomic microscopy, electrochemical scanning tunneling microscopy, and scanning electrochemical microscopy, in the electrochemical hydrogen evolution reaction. Representative examples of the applications of these techniques are also provided. Challenges in this field and future perspectives are discussed. https://pub.iapchem.org/ojs/index.php/JESE/article/view/2526Electrocatalystoperando techniquein situ characterization techniqueshydrogen evolution reaction |
| spellingShingle | Anaclet Nsabimana Yiran Guan Guobao Xu In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions Journal of Electrochemical Science and Engineering Electrocatalyst operando technique in situ characterization techniques hydrogen evolution reaction |
| title | In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions |
| title_full | In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions |
| title_fullStr | In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions |
| title_full_unstemmed | In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions |
| title_short | In situ and operando characterization techniques for nanocatalyst-based electrochemical hydrogen evolution reactions |
| title_sort | in situ and operando characterization techniques for nanocatalyst based electrochemical hydrogen evolution reactions |
| topic | Electrocatalyst operando technique in situ characterization techniques hydrogen evolution reaction |
| url | https://pub.iapchem.org/ojs/index.php/JESE/article/view/2526 |
| work_keys_str_mv | AT anacletnsabimana insituandoperandocharacterizationtechniquesfornanocatalystbasedelectrochemicalhydrogenevolutionreactions AT yiranguan insituandoperandocharacterizationtechniquesfornanocatalystbasedelectrochemicalhydrogenevolutionreactions AT guobaoxu insituandoperandocharacterizationtechniquesfornanocatalystbasedelectrochemicalhydrogenevolutionreactions |