Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution

Transition metal phosphides (TMPs) show great potential as catalysts for the hydrogen evolution reaction (HER). FeP stands out as an efficient and cost-effective non-noble metal-based HER catalyst. However, FeP tends to aggregate and suffer from instability during the reaction. To tackle these chall...

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Main Authors: Jianguo Zhong, Ting Zhang, Jianqiang Tian, Wei Gao, Yuxin Wang
Format: Article
Language:English
Published: MDPI AG 2024-11-01
Series:Inorganics
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Online Access:https://www.mdpi.com/2304-6740/12/11/291
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author Jianguo Zhong
Ting Zhang
Jianqiang Tian
Wei Gao
Yuxin Wang
author_facet Jianguo Zhong
Ting Zhang
Jianqiang Tian
Wei Gao
Yuxin Wang
author_sort Jianguo Zhong
collection DOAJ
description Transition metal phosphides (TMPs) show great potential as catalysts for the hydrogen evolution reaction (HER). FeP stands out as an efficient and cost-effective non-noble metal-based HER catalyst. However, FeP tends to aggregate and suffer from instability during the reaction. To tackle these challenges, we developed an efficient and straightforward approach to load metal-organic framework-derived N/P co-doped carbon-encapsulated FeP nanoparticles onto a nickel foam substrate (FeP@NPC/NF-450). This catalyst exhibits exceptional HER activity in 0.5 M H<sub>2</sub>SO<sub>4</sub> and 1.0 M KOH solutions, with overpotentials of 68.3 mV and 106.1 mV at a current density of 10 mA cm<sup>−2</sup>, respectively. Furthermore, it demonstrates excellent stability with negligible decay over 48 h in both acidic and alkaline solutions. The outstanding hydrogen evolution catalytic performance of FeP@NPC/NF-450 is mainly due to the N, P co-doped carbon matrix, which safeguards the FeP nanoparticles from aggregation and surface oxidation. Consequently, this enhances the availability of active sites during the hydrogen evolution reaction (HER), leading to improved stability. Moreover, introducing nickel foam offers a larger specific surface area and enhances charge transfer rates. This study provides a reference method for preparing stable and highly active electrocatalysts for hydrogen evolution.
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publishDate 2024-11-01
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spelling doaj-art-c6132ff8fc60408d97f7b818d3ee60462024-11-26T18:06:57ZengMDPI AGInorganics2304-67402024-11-01121129110.3390/inorganics12110291Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen EvolutionJianguo Zhong0Ting Zhang1Jianqiang Tian2Wei Gao3Yuxin Wang4School of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang 212114, ChinaSchool of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang 212114, ChinaSchool of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang 212114, ChinaDepartment of Chemical and Materials Engineering, Faculty of Engineering, The University of Auckland, Auckland 1142, New ZealandSchool of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang 212114, ChinaTransition metal phosphides (TMPs) show great potential as catalysts for the hydrogen evolution reaction (HER). FeP stands out as an efficient and cost-effective non-noble metal-based HER catalyst. However, FeP tends to aggregate and suffer from instability during the reaction. To tackle these challenges, we developed an efficient and straightforward approach to load metal-organic framework-derived N/P co-doped carbon-encapsulated FeP nanoparticles onto a nickel foam substrate (FeP@NPC/NF-450). This catalyst exhibits exceptional HER activity in 0.5 M H<sub>2</sub>SO<sub>4</sub> and 1.0 M KOH solutions, with overpotentials of 68.3 mV and 106.1 mV at a current density of 10 mA cm<sup>−2</sup>, respectively. Furthermore, it demonstrates excellent stability with negligible decay over 48 h in both acidic and alkaline solutions. The outstanding hydrogen evolution catalytic performance of FeP@NPC/NF-450 is mainly due to the N, P co-doped carbon matrix, which safeguards the FeP nanoparticles from aggregation and surface oxidation. Consequently, this enhances the availability of active sites during the hydrogen evolution reaction (HER), leading to improved stability. Moreover, introducing nickel foam offers a larger specific surface area and enhances charge transfer rates. This study provides a reference method for preparing stable and highly active electrocatalysts for hydrogen evolution.https://www.mdpi.com/2304-6740/12/11/291metal-organic frameworktransition-metal phosphides (TMPs)N/P co-doped carbonelectrocatalysthydrogen evolution reaction
spellingShingle Jianguo Zhong
Ting Zhang
Jianqiang Tian
Wei Gao
Yuxin Wang
Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
Inorganics
metal-organic framework
transition-metal phosphides (TMPs)
N/P co-doped carbon
electrocatalyst
hydrogen evolution reaction
title Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
title_full Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
title_fullStr Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
title_full_unstemmed Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
title_short Nickel Foam-Supported FeP Encapsulated in N, P Co-Doped Carbon Matrix for Efficient Electrocatalytic Hydrogen Evolution
title_sort nickel foam supported fep encapsulated in n p co doped carbon matrix for efficient electrocatalytic hydrogen evolution
topic metal-organic framework
transition-metal phosphides (TMPs)
N/P co-doped carbon
electrocatalyst
hydrogen evolution reaction
url https://www.mdpi.com/2304-6740/12/11/291
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