Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials
This study aims to determine the effect of adding 3 mol% yttria stabilized zirconia (3YSZ) in hydroxyapatite (HA) and sintering HA/3YSZ nanocomposites under nitrogen gas on HA decomposition. This paper presents the relationship between microstructure and mechanical properties of HA/3YSZ nanocomposit...
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2014-01-01
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Series: | Advances in Materials Science and Engineering |
Online Access: | http://dx.doi.org/10.1155/2014/367267 |
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author | C. H. Leong A. Muchtar C. Y. Tan M. Razali Noor Faeizah Amat |
author_facet | C. H. Leong A. Muchtar C. Y. Tan M. Razali Noor Faeizah Amat |
author_sort | C. H. Leong |
collection | DOAJ |
description | This study aims to determine the effect of adding 3 mol% yttria stabilized zirconia (3YSZ) in hydroxyapatite (HA) and sintering HA/3YSZ nanocomposites under nitrogen gas on HA decomposition. This paper presents the relationship between microstructure and mechanical properties of HA/3YSZ nanocomposites. Gas pressure and conventional sintering were performed on HA/3YSZ nanocomposites containing different amounts of 3YSZ (i.e., 0, 0.5, 1, and 7 wt%) at 1250°C. The phase stability, morphology, relative density, and microhardness of the HA/3YSZ nanocomposites were investigated. The phase stability of the HA/3YSZ nanocomposites was affected by adding different amounts of 3YSZ. Overall, gas pressure sintering leads to the formation of greater grain size compared with the conventional sintering method. The severe HA decomposition and the presence of the porosity in HA/7 wt% 3YSZ have led to deterioration in relative density and microhardness. In this study, HA/0.5 wt% 3YSZ with gas pressure sintering exhibited the optimum microstructure with the highest relative density (97%) and microhardness (3.93 GPa). |
format | Article |
id | doaj-art-c4da77c6e4584b9f826a6ba6aeaf4563 |
institution | Kabale University |
issn | 1687-8434 1687-8442 |
language | English |
publishDate | 2014-01-01 |
publisher | Wiley |
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series | Advances in Materials Science and Engineering |
spelling | doaj-art-c4da77c6e4584b9f826a6ba6aeaf45632025-02-03T05:47:48ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422014-01-01201410.1155/2014/367267367267Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental MaterialsC. H. Leong0A. Muchtar1C. Y. Tan2M. Razali3Noor Faeizah Amat4Department of Mechanical and Materials Engineering, Faculty of Engineering & Built Environment, Universiti Kebangsaan Malaysia (UKM), 43600 Bangi, Selangor, MalaysiaDepartment of Mechanical and Materials Engineering, Faculty of Engineering & Built Environment, Universiti Kebangsaan Malaysia (UKM), 43600 Bangi, Selangor, MalaysiaDepartment of Mechanical Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, MalaysiaPeriodontology Department, Faculty of Dentistry, Universiti Kebangsaan Malaysia, Jalan Raja Muda Abdul Aziz, 50300 Kuala Lumpur, MalaysiaDepartment of Mechanical and Materials Engineering, Faculty of Engineering & Built Environment, Universiti Kebangsaan Malaysia (UKM), 43600 Bangi, Selangor, MalaysiaThis study aims to determine the effect of adding 3 mol% yttria stabilized zirconia (3YSZ) in hydroxyapatite (HA) and sintering HA/3YSZ nanocomposites under nitrogen gas on HA decomposition. This paper presents the relationship between microstructure and mechanical properties of HA/3YSZ nanocomposites. Gas pressure and conventional sintering were performed on HA/3YSZ nanocomposites containing different amounts of 3YSZ (i.e., 0, 0.5, 1, and 7 wt%) at 1250°C. The phase stability, morphology, relative density, and microhardness of the HA/3YSZ nanocomposites were investigated. The phase stability of the HA/3YSZ nanocomposites was affected by adding different amounts of 3YSZ. Overall, gas pressure sintering leads to the formation of greater grain size compared with the conventional sintering method. The severe HA decomposition and the presence of the porosity in HA/7 wt% 3YSZ have led to deterioration in relative density and microhardness. In this study, HA/0.5 wt% 3YSZ with gas pressure sintering exhibited the optimum microstructure with the highest relative density (97%) and microhardness (3.93 GPa).http://dx.doi.org/10.1155/2014/367267 |
spellingShingle | C. H. Leong A. Muchtar C. Y. Tan M. Razali Noor Faeizah Amat Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials Advances in Materials Science and Engineering |
title | Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials |
title_full | Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials |
title_fullStr | Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials |
title_full_unstemmed | Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials |
title_short | Sintering of Hydroxyapatite/Yttria Stabilized Zirconia Nanocomposites under Nitrogen Gas for Dental Materials |
title_sort | sintering of hydroxyapatite yttria stabilized zirconia nanocomposites under nitrogen gas for dental materials |
url | http://dx.doi.org/10.1155/2014/367267 |
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