Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution
Studies on the synthesis of graphene oxide in ammonium carbonate solution by electrochemical method were conducted. During the synthesis of graphene oxide, a partial reduction of graphene oxide was observed as a result of stirring the solution. The composition of graphene oxide was analyzed using UV...
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| Format: | Article |
| Language: | English |
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Iranian Chemical Society
2024-06-01
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| Series: | Nanochemistry Research |
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| Online Access: | http://www.nanochemres.org/article_197832_b3ea91607ed38df3bf7ff0a6e077f2bb.pdf |
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| _version_ | 1841545150431494144 |
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| author | Khushnudbek Eshchanov Makhliyo Ibragimova Bazar Ibadullaev |
| author_facet | Khushnudbek Eshchanov Makhliyo Ibragimova Bazar Ibadullaev |
| author_sort | Khushnudbek Eshchanov |
| collection | DOAJ |
| description | Studies on the synthesis of graphene oxide in ammonium carbonate solution by electrochemical method were conducted. During the synthesis of graphene oxide, a partial reduction of graphene oxide was observed as a result of stirring the solution. The composition of graphene oxide was analyzed using UV- and ATR-FTIR spectroscopy and quantum chemical calculation methods. As a result of the analysis, it was found that the graphene oxide contains hydroxyl, carboxyl, methylene, methyl, and ether groups connecting aromatic rings. Absorption in the 264 nm region, according to the UV spectrum, indicates a partial reduction of graphene oxide. It is important to carry out the synthesis process in a cold solution of ammonium carbonate because when the solution is warm, the hydrolysis of the salt increases. Ammonia and carbon dioxide gases are released in the hydrolysis process. This research work demonstrates a clean separation of graphene oxide in ammonium carbonate solution. |
| format | Article |
| id | doaj-art-c145bacafd5c47b28f4891c3c3b0bec6 |
| institution | Kabale University |
| issn | 2538-4279 2423-818X |
| language | English |
| publishDate | 2024-06-01 |
| publisher | Iranian Chemical Society |
| record_format | Article |
| series | Nanochemistry Research |
| spelling | doaj-art-c145bacafd5c47b28f4891c3c3b0bec62025-01-12T10:25:14ZengIranian Chemical SocietyNanochemistry Research2538-42792423-818X2024-06-019323524110.22036/ncr.2024.03.007197832Studying the Synthesis of Graphene Oxide in Ammonium Carbonate SolutionKhushnudbek Eshchanov0Makhliyo Ibragimova1Bazar Ibadullaev2Department of Chemistry, Urganch State University, Urgench, UzbekistanDepartment of Chemistry, Urganch State University, Urgench, UzbekistanDepartment of Products and food technology, Urgench State University, Urgench, UzbekistanStudies on the synthesis of graphene oxide in ammonium carbonate solution by electrochemical method were conducted. During the synthesis of graphene oxide, a partial reduction of graphene oxide was observed as a result of stirring the solution. The composition of graphene oxide was analyzed using UV- and ATR-FTIR spectroscopy and quantum chemical calculation methods. As a result of the analysis, it was found that the graphene oxide contains hydroxyl, carboxyl, methylene, methyl, and ether groups connecting aromatic rings. Absorption in the 264 nm region, according to the UV spectrum, indicates a partial reduction of graphene oxide. It is important to carry out the synthesis process in a cold solution of ammonium carbonate because when the solution is warm, the hydrolysis of the salt increases. Ammonia and carbon dioxide gases are released in the hydrolysis process. This research work demonstrates a clean separation of graphene oxide in ammonium carbonate solution.http://www.nanochemres.org/article_197832_b3ea91607ed38df3bf7ff0a6e077f2bb.pdfgraphitegraphene oxideammonium carbonateelectrochemicalsemi-empirical |
| spellingShingle | Khushnudbek Eshchanov Makhliyo Ibragimova Bazar Ibadullaev Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution Nanochemistry Research graphite graphene oxide ammonium carbonate electrochemical semi-empirical |
| title | Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution |
| title_full | Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution |
| title_fullStr | Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution |
| title_full_unstemmed | Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution |
| title_short | Studying the Synthesis of Graphene Oxide in Ammonium Carbonate Solution |
| title_sort | studying the synthesis of graphene oxide in ammonium carbonate solution |
| topic | graphite graphene oxide ammonium carbonate electrochemical semi-empirical |
| url | http://www.nanochemres.org/article_197832_b3ea91607ed38df3bf7ff0a6e077f2bb.pdf |
| work_keys_str_mv | AT khushnudbekeshchanov studyingthesynthesisofgrapheneoxideinammoniumcarbonatesolution AT makhliyoibragimova studyingthesynthesisofgrapheneoxideinammoniumcarbonatesolution AT bazaribadullaev studyingthesynthesisofgrapheneoxideinammoniumcarbonatesolution |