Determination of solubility of chlorides of d-elements in chloroaluminate melts

Solubility of several transition metal chlorides (NiCl2, CrCl2, MoCl3, FeCl2) was measured in KCl-AlCl3 based melts. It was found that the solubility of studied metal chlorides depends on K : Al mole ratio. MoCl3 solubility decreases with increasing AlCl3 content. Solubility of CrCl2 and FeCl2 reach...

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Bibliographic Details
Main Authors: V. V. Karpov, V. A. Volkovich, I. B. Polovov, O. I. Rebrin
Format: Article
Language:English
Published: Uralʹskij federalʹnyj universitet imeni pervogo Prezidenta Rossii B.N. Elʹcina 2014-09-01
Series:Chimica Techno Acta
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Online Access:https://chimicatechnoacta.ru/article/view/699
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Summary:Solubility of several transition metal chlorides (NiCl2, CrCl2, MoCl3, FeCl2) was measured in KCl-AlCl3 based melts. It was found that the solubility of studied metal chlorides depends on K : Al mole ratio. MoCl3 solubility decreases with increasing AlCl3 content. Solubility of CrCl2 and FeCl2 reaches maximum at K : Al ratio of 1 and decreases when this ratio either de-creases or increases. The dependence of NiCl2 solubility on K : Al mole ratio is V-shaped with the maximum near 0.9-0.95. The effect of temperature on solubility of transition metal chlorides in KCl-AlCl3 melts was also investigated. Increasing temperature does not alter the character of «solubility – K : Al mole ratio» dependences.
ISSN:2411-1414