A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater

In the past 20 years, sulfur hexafluoride (SF6) has been considered a highly reliable tracer for assessing modern water (< 65 yrs old) in groundwater. However, modern-air contamination may introduce complications in interpreting data obtained using current sampling methods. A new airtight methodo...

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Main Authors: Raka Sunderland, Dan Larsen, Scott Schoefernacker, Deborah Leslie
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:MethodsX
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Online Access:http://www.sciencedirect.com/science/article/pii/S2215016124005715
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author Raka Sunderland
Dan Larsen
Scott Schoefernacker
Deborah Leslie
author_facet Raka Sunderland
Dan Larsen
Scott Schoefernacker
Deborah Leslie
author_sort Raka Sunderland
collection DOAJ
description In the past 20 years, sulfur hexafluoride (SF6) has been considered a highly reliable tracer for assessing modern water (< 65 yrs old) in groundwater. However, modern-air contamination may introduce complications in interpreting data obtained using current sampling methods. A new airtight methodology isolates the sample from modern ambient air; thus, returning more reproducible and reliable results when compared to two traditional (air-sensitive and non-airtight) methods. The new airtight method returned results within 0.03–0.05 fmol/L SF6 of expected SF6 concentration for pre-modern waters (0.02–0.09±0.01 fmol/L). In contrast, the air-sensitive and non-airtight traditional methods returned results within 0.00–0.90 fmol/L and 0.02–1.21 fmol/L of the expected value, respectively. It is suspected that transformers in proximity to wells leak SF6 which subsequently partitions into the samples obtained using traditional air-sensitive and non-airtight methods, thus creating erratic SF6 results. • Comparative analyses of a new airtight method with traditional methods were performed and returned lower SF6 concentrations with the new 2022 airtight method. • The new airtight method shows reproducible low-level detection of SF6 concentrations and may reduce sampling error in production wells in urban areas that are co-located with transformers which are SF6-emitting sources.
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publishDate 2025-06-01
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spelling doaj-art-b899dc11853e480592aff7f3fc0d3f4f2024-12-25T04:21:20ZengElsevierMethodsX2215-01612025-06-0114103120A new airtight sampling method for sulfur hexafluoride (SF6) in groundwaterRaka Sunderland0Dan Larsen1Scott Schoefernacker2Deborah Leslie3Corresponding authors.; University of Memphis Department of Earth Sciences 109 Johnson Hall Memphis, TN 38152, USACorresponding authors.; University of Memphis Department of Earth Sciences 109 Johnson Hall Memphis, TN 38152, USACorresponding authors.; University of Memphis Department of Earth Sciences 109 Johnson Hall Memphis, TN 38152, USACorresponding authors.; University of Memphis Department of Earth Sciences 109 Johnson Hall Memphis, TN 38152, USAIn the past 20 years, sulfur hexafluoride (SF6) has been considered a highly reliable tracer for assessing modern water (< 65 yrs old) in groundwater. However, modern-air contamination may introduce complications in interpreting data obtained using current sampling methods. A new airtight methodology isolates the sample from modern ambient air; thus, returning more reproducible and reliable results when compared to two traditional (air-sensitive and non-airtight) methods. The new airtight method returned results within 0.03–0.05 fmol/L SF6 of expected SF6 concentration for pre-modern waters (0.02–0.09±0.01 fmol/L). In contrast, the air-sensitive and non-airtight traditional methods returned results within 0.00–0.90 fmol/L and 0.02–1.21 fmol/L of the expected value, respectively. It is suspected that transformers in proximity to wells leak SF6 which subsequently partitions into the samples obtained using traditional air-sensitive and non-airtight methods, thus creating erratic SF6 results. • Comparative analyses of a new airtight method with traditional methods were performed and returned lower SF6 concentrations with the new 2022 airtight method. • The new airtight method shows reproducible low-level detection of SF6 concentrations and may reduce sampling error in production wells in urban areas that are co-located with transformers which are SF6-emitting sources.http://www.sciencedirect.com/science/article/pii/S2215016124005715Airtight Sampling Method for SF6 in Groundwater
spellingShingle Raka Sunderland
Dan Larsen
Scott Schoefernacker
Deborah Leslie
A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
MethodsX
Airtight Sampling Method for SF6 in Groundwater
title A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
title_full A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
title_fullStr A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
title_full_unstemmed A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
title_short A new airtight sampling method for sulfur hexafluoride (SF6) in groundwater
title_sort new airtight sampling method for sulfur hexafluoride sf6 in groundwater
topic Airtight Sampling Method for SF6 in Groundwater
url http://www.sciencedirect.com/science/article/pii/S2215016124005715
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