2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction

Highlights Highly crystalline 2D metal hydrogen-bonded organic frameworks (2D-M-HOFs) including 2D-Cu-HOF and 2D-Ni-HOF were designed and synthesized. The 2D-M-HOF with flexible ligands leads to the formation of the self-adaption interlayered sites, which facilitate the C–C couple and overcome the l...

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Main Authors: Jianning Lv, Wenrui Li, Shuai Li, Shuo Xu, Zunhang Lv, Zhejiaji Zhu, Lu Dai, Bo Wang, Pengfei Li
Format: Article
Language:English
Published: SpringerOpen 2025-02-01
Series:Nano-Micro Letters
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Online Access:https://doi.org/10.1007/s40820-025-01679-3
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author Jianning Lv
Wenrui Li
Shuai Li
Shuo Xu
Zunhang Lv
Zhejiaji Zhu
Lu Dai
Bo Wang
Pengfei Li
author_facet Jianning Lv
Wenrui Li
Shuai Li
Shuo Xu
Zunhang Lv
Zhejiaji Zhu
Lu Dai
Bo Wang
Pengfei Li
author_sort Jianning Lv
collection DOAJ
description Highlights Highly crystalline 2D metal hydrogen-bonded organic frameworks (2D-M-HOFs) including 2D-Cu-HOF and 2D-Ni-HOF were designed and synthesized. The 2D-M-HOF with flexible ligands leads to the formation of the self-adaption interlayered sites, which facilitate the C–C couple and overcome the limitations of the coadsorption of multiple intermediates in the electrocatalytic CO2 reduction reaction. The undulated 2D-Cu-HOF exhibits outstanding activity and selectivity for electrocatalytic reduction of CO2 to C2 products with a total Faradaic efficiency of 82.1% (48.2% for C2H5OH and 33.9% for C2H4) at −1.2 V vs. RHE.
format Article
id doaj-art-b6a1fdb5ce4d4e8a8bcfc0b6cd73bbe3
institution Kabale University
issn 2311-6706
2150-5551
language English
publishDate 2025-02-01
publisher SpringerOpen
record_format Article
series Nano-Micro Letters
spelling doaj-art-b6a1fdb5ce4d4e8a8bcfc0b6cd73bbe32025-08-20T03:46:21ZengSpringerOpenNano-Micro Letters2311-67062150-55512025-02-0117111110.1007/s40820-025-01679-32D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 ReductionJianning Lv0Wenrui Li1Shuai Li2Shuo Xu3Zunhang Lv4Zhejiaji Zhu5Lu Dai6Bo Wang7Pengfei Li8Key Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyKey Laboratory of Cluster Science Ministry of Education, Beijing Key Laboratory of Photoelectronic/Electrophotonic, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyHighlights Highly crystalline 2D metal hydrogen-bonded organic frameworks (2D-M-HOFs) including 2D-Cu-HOF and 2D-Ni-HOF were designed and synthesized. The 2D-M-HOF with flexible ligands leads to the formation of the self-adaption interlayered sites, which facilitate the C–C couple and overcome the limitations of the coadsorption of multiple intermediates in the electrocatalytic CO2 reduction reaction. The undulated 2D-Cu-HOF exhibits outstanding activity and selectivity for electrocatalytic reduction of CO2 to C2 products with a total Faradaic efficiency of 82.1% (48.2% for C2H5OH and 33.9% for C2H4) at −1.2 V vs. RHE.https://doi.org/10.1007/s40820-025-01679-3Hydrogen-bonded organic frameworksFlexible structureSelf-adaption interlayered sitesElectrocatalytic CO2 reduction
spellingShingle Jianning Lv
Wenrui Li
Shuai Li
Shuo Xu
Zunhang Lv
Zhejiaji Zhu
Lu Dai
Bo Wang
Pengfei Li
2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
Nano-Micro Letters
Hydrogen-bonded organic frameworks
Flexible structure
Self-adaption interlayered sites
Electrocatalytic CO2 reduction
title 2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
title_full 2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
title_fullStr 2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
title_full_unstemmed 2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
title_short 2D Undulated Metal Hydrogen-Bonded Organic Frameworks with Self-Adaption Interlayered Sites for Highly Efficient C–C Coupling in the Electrocatalytic CO2 Reduction
title_sort 2d undulated metal hydrogen bonded organic frameworks with self adaption interlayered sites for highly efficient c c coupling in the electrocatalytic co2 reduction
topic Hydrogen-bonded organic frameworks
Flexible structure
Self-adaption interlayered sites
Electrocatalytic CO2 reduction
url https://doi.org/10.1007/s40820-025-01679-3
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