Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair

<b>Background:</b> The combination of macroporous cryogels with synthetic peptide factors represents a promising but poorly explored strategy for the development of extracellular matrix (ECM)-mimicking scaffolds for peripheral nerve (PN) repair. <b>Methods:</b> In this study,...

Full description

Saved in:
Bibliographic Details
Main Authors: Abdulla Yergeshov, Mohamed Zoughaib, Kenana Dayob, Marat Kamalov, Duong Luong, Albina Zakirova, Ruslan Mullin, Diana Salakhieva, Timur I. Abdullin
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Pharmaceutics
Subjects:
Online Access:https://www.mdpi.com/1999-4923/16/12/1569
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1846103194783973376
author Abdulla Yergeshov
Mohamed Zoughaib
Kenana Dayob
Marat Kamalov
Duong Luong
Albina Zakirova
Ruslan Mullin
Diana Salakhieva
Timur I. Abdullin
author_facet Abdulla Yergeshov
Mohamed Zoughaib
Kenana Dayob
Marat Kamalov
Duong Luong
Albina Zakirova
Ruslan Mullin
Diana Salakhieva
Timur I. Abdullin
author_sort Abdulla Yergeshov
collection DOAJ
description <b>Background:</b> The combination of macroporous cryogels with synthetic peptide factors represents a promising but poorly explored strategy for the development of extracellular matrix (ECM)-mimicking scaffolds for peripheral nerve (PN) repair. <b>Methods:</b> In this study, IKVAV peptide was functionalized with terminal lysine residues to allow its in situ cross-linking with gelatin macromer, resulting in the formation of IKVAV-containing proteinaceous cryogels. The controllable inclusion and distribution of the peptide molecules within the scaffold was verified using a fluorescently labelled peptide counterpart. The optimized cryogel scaffold was combined with polycaprolactone (PCL)-based shell tube to form a suturable nerve conduit (NC) to be implanted into sciatic nerve diastasis in rats. <b>Results:</b> The NC constituents did not impair the viability of primary skin fibroblasts. Concentration-dependent effects of the peptide component on interrelated viscoelastic and swelling properties of the cryogels as well as on proliferation and morphological differentiation of neurogenic PC-12 cells were established, also indicating the existence of an optimal-density range of the introduced peptide. The in vivo implanted NC sustained the connection of the nerve stumps with partial degradation of the PCL tube over eight weeks, whereas the core-filling cryogel profoundly improved local electromyographic recovery and morphological repair of the nerve tissues, confirming the regenerative activity of the developed scaffold. <b>Conclusions:</b> These results provide proof-of-concept for the development of a newly designed PN conduit prototype based on IKVAV-activated cryogel, and they can be exploited to create other ECM-mimicking scaffolds.
format Article
id doaj-art-a92d37a5cd124475a99023f8ec95ac4d
institution Kabale University
issn 1999-4923
language English
publishDate 2024-12-01
publisher MDPI AG
record_format Article
series Pharmaceutics
spelling doaj-art-a92d37a5cd124475a99023f8ec95ac4d2024-12-27T14:46:32ZengMDPI AGPharmaceutics1999-49232024-12-011612156910.3390/pharmaceutics16121569Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve RepairAbdulla Yergeshov0Mohamed Zoughaib1Kenana Dayob2Marat Kamalov3Duong Luong4Albina Zakirova5Ruslan Mullin6Diana Salakhieva7Timur I. Abdullin8Scientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaScientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaScientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaScientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaInstitute for Molecular Bioscience, The University of Queensland, St. Lucia, QLD 4072, AustraliaAcademy of Postgraduate Education under FSBU FSCC of FMBA of Russia, Department of Oncology and Plastic Surgery, 91 Volokolamsk Highway, 125371 Moscow, RussiaInstitute of Fundamental Medicine and Biology, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaScientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, RussiaScientific and Educational Center of Pharmaceutics, Kazan (Volga Region) Federal University, 18 Kremlyovskaya St., 420008 Kazan, Russia<b>Background:</b> The combination of macroporous cryogels with synthetic peptide factors represents a promising but poorly explored strategy for the development of extracellular matrix (ECM)-mimicking scaffolds for peripheral nerve (PN) repair. <b>Methods:</b> In this study, IKVAV peptide was functionalized with terminal lysine residues to allow its in situ cross-linking with gelatin macromer, resulting in the formation of IKVAV-containing proteinaceous cryogels. The controllable inclusion and distribution of the peptide molecules within the scaffold was verified using a fluorescently labelled peptide counterpart. The optimized cryogel scaffold was combined with polycaprolactone (PCL)-based shell tube to form a suturable nerve conduit (NC) to be implanted into sciatic nerve diastasis in rats. <b>Results:</b> The NC constituents did not impair the viability of primary skin fibroblasts. Concentration-dependent effects of the peptide component on interrelated viscoelastic and swelling properties of the cryogels as well as on proliferation and morphological differentiation of neurogenic PC-12 cells were established, also indicating the existence of an optimal-density range of the introduced peptide. The in vivo implanted NC sustained the connection of the nerve stumps with partial degradation of the PCL tube over eight weeks, whereas the core-filling cryogel profoundly improved local electromyographic recovery and morphological repair of the nerve tissues, confirming the regenerative activity of the developed scaffold. <b>Conclusions:</b> These results provide proof-of-concept for the development of a newly designed PN conduit prototype based on IKVAV-activated cryogel, and they can be exploited to create other ECM-mimicking scaffolds.https://www.mdpi.com/1999-4923/16/12/1569peripheral nerve repairnerve conduitscryogelsECM proteinssynthetic peptidesIKVAV derivatives
spellingShingle Abdulla Yergeshov
Mohamed Zoughaib
Kenana Dayob
Marat Kamalov
Duong Luong
Albina Zakirova
Ruslan Mullin
Diana Salakhieva
Timur I. Abdullin
Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
Pharmaceutics
peripheral nerve repair
nerve conduits
cryogels
ECM proteins
synthetic peptides
IKVAV derivatives
title Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
title_full Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
title_fullStr Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
title_full_unstemmed Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
title_short Newly Designed PCL-Wrapped Cryogel-Based Conduit Activated with IKVAV Peptide Derivative for Peripheral Nerve Repair
title_sort newly designed pcl wrapped cryogel based conduit activated with ikvav peptide derivative for peripheral nerve repair
topic peripheral nerve repair
nerve conduits
cryogels
ECM proteins
synthetic peptides
IKVAV derivatives
url https://www.mdpi.com/1999-4923/16/12/1569
work_keys_str_mv AT abdullayergeshov newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT mohamedzoughaib newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT kenanadayob newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT maratkamalov newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT duongluong newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT albinazakirova newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT ruslanmullin newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT dianasalakhieva newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair
AT timuriabdullin newlydesignedpclwrappedcryogelbasedconduitactivatedwithikvavpeptidederivativeforperipheralnerverepair