Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway

Non-small cell lung cancer (NSCLC) is a leading cause of cancer-related deaths worldwide. Its treatment is complicated due to the development of resistance to conventional chemotherapy and targeted therapy. Deoxybouvardin and related cyclic hexapeptides reportedly exhibit antitumor activities, but t...

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Main Authors: Na Yeong Lee, Sang Hoon Joo, A-Young Nam, Seung-On Lee, Goo Yoon, Seung-sik Cho, Yung Hyun Choi, Jin Woo Park, Jung-Hyun Shim
Format: Article
Language:English
Published: IfADo - Leibniz Research Centre for Working Environment and Human Factors, Dortmund 2024-10-01
Series:EXCLI Journal : Experimental and Clinical Sciences
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Online Access:https://www.excli.de/excli/article/view/7359
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author Na Yeong Lee
Sang Hoon Joo
A-Young Nam
Seung-On Lee
Goo Yoon
Seung-sik Cho
Yung Hyun Choi
Jin Woo Park
Jung-Hyun Shim
author_facet Na Yeong Lee
Sang Hoon Joo
A-Young Nam
Seung-On Lee
Goo Yoon
Seung-sik Cho
Yung Hyun Choi
Jin Woo Park
Jung-Hyun Shim
author_sort Na Yeong Lee
collection DOAJ
description Non-small cell lung cancer (NSCLC) is a leading cause of cancer-related deaths worldwide. Its treatment is complicated due to the development of resistance to conventional chemotherapy and targeted therapy. Deoxybouvardin and related cyclic hexapeptides reportedly exhibit antitumor activities, but their mechanisms of action remain unclear. This study aimed to investigate the anticancer mechanisms of deoxybouvardin glucoside (DBG), a glucosidic form of deoxybouvardin from Rubia species, in gefitinib (GEF)-sensitive and -resistant NSCLC HCC827 cells. The effects of DBG treatment on cell proliferation were evaluated using a viability assay. The inhibitory effects of DBG treatment on the activities and phosphorylation of the protein kinases epidermal growth factor receptor (EGFR), MET, and AKTs were assessed using in vitro kinase assay and western blot, respectively. DBG treatment inhibited the growth of HCC827 cells in a concentration- and time-dependent manner. Results of in vitro kinase assay and western blotting showed that DBG treatment significantly inhibited the activities and phosphorylation of the protein kinases EGFR, MET, and AKT. Prediction using molecular docking showed that DBG is located in the ATP-binding pockets of these kinases, supporting the kinase inhibition by DBG treatment. Moreover, DBG treatment induced reactive oxygen species (ROS) generation and cell cycle arrest in the cells. The induction of apoptosis by DBG through caspase activation was confirmed by Z-VAD-FMK treatment. In summary, DBG treatment inhibited the growth of GEF-sensitive and -resistant NSCLC cells by targeting EGFR, MET, and AKTs. Moreover, it induced apoptosis by inducing ROS generation and caspase activation. These results indicate that DBG is a potential therapeutic agent for the treatment of GEF-resistant NSCLC.
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spelling doaj-art-a2f044b6fa1446ff9c60f27c29629e5c2024-12-02T10:14:54ZengIfADo - Leibniz Research Centre for Working Environment and Human Factors, DortmundEXCLI Journal : Experimental and Clinical Sciences1611-21562024-10-01231287130210.17179/excli2024-73596798Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathwayNa Yeong Lee0https://orcid.org/0000-0003-2681-3344Sang Hoon Joo1https://orcid.org/0000-0001-8660-884XA-Young Nam2https://orcid.org/0000-0003-0162-108XSeung-On Lee3https://orcid.org/0000-0003-1293-4604Goo Yoon4https://orcid.org/0000-0001-7998-4708Seung-sik Cho5https://orcid.org/0000-0003-1497-0529Yung Hyun Choi6https://orcid.org/0000-0002-1454-3124Jin Woo Park7https://orcid.org/0000-0002-0001-7043Jung-Hyun Shim8https://orcid.org/0000-0002-4062-4016Department of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of KoreaCollege of Pharmacy, Daegu Catholic University, Gyeongsan 38430, Republic of KoreaDepartment of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of KoreaDepartment of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of KoreaDepartment of Pharmacy, College of Pharmacy, Mokpo National University, Muan 58554, Republic of KoreaDepartment of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of Korea; Department of Pharmacy, College of Pharmacy, Mokpo National University, Muan 58554, Republic of KoreaDepartment of Biochemistry, College of Korean Medicine, Dong-Eui University, Busan 47227, Republic of KoreaDepartment of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of Korea, Tel: +82-61-450-2704, E-mail: jwpark@mokpo.ac.krDepartment of Biomedicine, Health & Life Convergence Sciences, BK21 Four, College of Pharmacy, Mokpo National University, Muan 58554, Republic of Korea, Tel: +82-61-450-2684, E-mail: s1004jh@gmail.comNon-small cell lung cancer (NSCLC) is a leading cause of cancer-related deaths worldwide. Its treatment is complicated due to the development of resistance to conventional chemotherapy and targeted therapy. Deoxybouvardin and related cyclic hexapeptides reportedly exhibit antitumor activities, but their mechanisms of action remain unclear. This study aimed to investigate the anticancer mechanisms of deoxybouvardin glucoside (DBG), a glucosidic form of deoxybouvardin from Rubia species, in gefitinib (GEF)-sensitive and -resistant NSCLC HCC827 cells. The effects of DBG treatment on cell proliferation were evaluated using a viability assay. The inhibitory effects of DBG treatment on the activities and phosphorylation of the protein kinases epidermal growth factor receptor (EGFR), MET, and AKTs were assessed using in vitro kinase assay and western blot, respectively. DBG treatment inhibited the growth of HCC827 cells in a concentration- and time-dependent manner. Results of in vitro kinase assay and western blotting showed that DBG treatment significantly inhibited the activities and phosphorylation of the protein kinases EGFR, MET, and AKT. Prediction using molecular docking showed that DBG is located in the ATP-binding pockets of these kinases, supporting the kinase inhibition by DBG treatment. Moreover, DBG treatment induced reactive oxygen species (ROS) generation and cell cycle arrest in the cells. The induction of apoptosis by DBG through caspase activation was confirmed by Z-VAD-FMK treatment. In summary, DBG treatment inhibited the growth of GEF-sensitive and -resistant NSCLC cells by targeting EGFR, MET, and AKTs. Moreover, it induced apoptosis by inducing ROS generation and caspase activation. These results indicate that DBG is a potential therapeutic agent for the treatment of GEF-resistant NSCLC.https://www.excli.de/excli/article/view/7359deoxybouvardin glucosidenon-small cell lung canceregfr/met/aktcell cyclereactive oxygen speciesapoptosis
spellingShingle Na Yeong Lee
Sang Hoon Joo
A-Young Nam
Seung-On Lee
Goo Yoon
Seung-sik Cho
Yung Hyun Choi
Jin Woo Park
Jung-Hyun Shim
Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
EXCLI Journal : Experimental and Clinical Sciences
deoxybouvardin glucoside
non-small cell lung cancer
egfr/met/akt
cell cycle
reactive oxygen species
apoptosis
title Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
title_full Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
title_fullStr Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
title_full_unstemmed Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
title_short Deoxybouvardin-glucoside induces apoptosis in non-small cell lung cancer cells by targeting EGFR/MET and AKT signaling pathway
title_sort deoxybouvardin glucoside induces apoptosis in non small cell lung cancer cells by targeting egfr met and akt signaling pathway
topic deoxybouvardin glucoside
non-small cell lung cancer
egfr/met/akt
cell cycle
reactive oxygen species
apoptosis
url https://www.excli.de/excli/article/view/7359
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