Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma

This work aims to deposit silica (SiO2) on polyamide 6,6 fabrics by hybrid corona-dielectric barrier discharge plasma at atmospheric pressure. The reactor used, developed at the Laboratory of Plasma and Processes of the Aeronautics Institute of Technology (LPP/ITA), allows the treatment of fabric su...

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Main Authors: Isabella Grinberg Francelino, Felipe de Souza Miranda, Fernando Gasi, Marcia Cristina Silva, Sérgio Ricardo Lourenço, Gilberto Petraconi Filho
Format: Article
Language:English
Published: Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol) 2025-01-01
Series:Materials Research
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Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392025000100201&lng=en&tlng=en
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author Isabella Grinberg Francelino
Felipe de Souza Miranda
Fernando Gasi
Marcia Cristina Silva
Sérgio Ricardo Lourenço
Gilberto Petraconi Filho
author_facet Isabella Grinberg Francelino
Felipe de Souza Miranda
Fernando Gasi
Marcia Cristina Silva
Sérgio Ricardo Lourenço
Gilberto Petraconi Filho
author_sort Isabella Grinberg Francelino
collection DOAJ
description This work aims to deposit silica (SiO2) on polyamide 6,6 fabrics by hybrid corona-dielectric barrier discharge plasma at atmospheric pressure. The reactor used, developed at the Laboratory of Plasma and Processes of the Aeronautics Institute of Technology (LPP/ITA), allows the treatment of fabric surfaces by activation and plasma deposition processes, aiming, in this order, the alteration of wettability and the deposition of silica on its surface, using a silicic acid solution (Si(OH)4) as a silica precursor. The morphology of the deposited films was evaluated by scanning electron microscopy (SEM). To identify the chemical modifications generated by the plasma treatment, the untreated and treated samples were analyzed by Fourier transform infrared spectroscopy with attenuated reflectance (FTIR-ATR) and Energy Dispersive Spectroscopy (EDS). The thermal behavior of the treated and untreated samples was evaluated by Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Additionally, X-ray diffraction (XRD) was also used to identify crystalline phases in the film. The results showed that plasma processing proved to be an effective technique for modifying the surface characteristics of polyamide 6,6.
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institution Kabale University
issn 1516-1439
language English
publishDate 2025-01-01
publisher Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)
record_format Article
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spelling doaj-art-a2da77767d3e4f30a35bb76de1ac7cf22025-01-14T07:40:21ZengAssociação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)Materials Research1516-14392025-01-012810.1590/1980-5373-mr-2024-0257Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge PlasmaIsabella Grinberg FrancelinoFelipe de Souza MirandaFernando Gasihttps://orcid.org/0000-0001-7383-2762Marcia Cristina Silvahttps://orcid.org/0000-0001-7840-7116Sérgio Ricardo LourençoGilberto Petraconi FilhoThis work aims to deposit silica (SiO2) on polyamide 6,6 fabrics by hybrid corona-dielectric barrier discharge plasma at atmospheric pressure. The reactor used, developed at the Laboratory of Plasma and Processes of the Aeronautics Institute of Technology (LPP/ITA), allows the treatment of fabric surfaces by activation and plasma deposition processes, aiming, in this order, the alteration of wettability and the deposition of silica on its surface, using a silicic acid solution (Si(OH)4) as a silica precursor. The morphology of the deposited films was evaluated by scanning electron microscopy (SEM). To identify the chemical modifications generated by the plasma treatment, the untreated and treated samples were analyzed by Fourier transform infrared spectroscopy with attenuated reflectance (FTIR-ATR) and Energy Dispersive Spectroscopy (EDS). The thermal behavior of the treated and untreated samples was evaluated by Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Additionally, X-ray diffraction (XRD) was also used to identify crystalline phases in the film. The results showed that plasma processing proved to be an effective technique for modifying the surface characteristics of polyamide 6,6.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392025000100201&lng=en&tlng=enSilicapolyamide 6,6depositioncorona-dielectric barrier dischargesilicic acid
spellingShingle Isabella Grinberg Francelino
Felipe de Souza Miranda
Fernando Gasi
Marcia Cristina Silva
Sérgio Ricardo Lourenço
Gilberto Petraconi Filho
Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
Materials Research
Silica
polyamide 6,6
deposition
corona-dielectric barrier discharge
silicic acid
title Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
title_full Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
title_fullStr Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
title_full_unstemmed Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
title_short Silica Deposition on Polyamide 6,6 Fabrics by Hybrid Corona-Dielectric Barrier Discharge Plasma
title_sort silica deposition on polyamide 6 6 fabrics by hybrid corona dielectric barrier discharge plasma
topic Silica
polyamide 6,6
deposition
corona-dielectric barrier discharge
silicic acid
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392025000100201&lng=en&tlng=en
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