Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell

Abstract The high-pressure and high-temperature structural, mechanical, and dinamical stability of rhodium has been investigated via synchrotron X-ray diffraction using a resistively heated diamond anvil cell and density functional theory. The isothermal compression data have been fitted with a Rydb...

Full description

Saved in:
Bibliographic Details
Main Authors: Jose Luis Rodrigo-Ramon, Simone Anzellini, Claudio Cazorla, Pablo Botella, Aser Garcia-Beamud, Josu Sanchez-Martin, Gaston Garbarino, Angelika D. Rosa, Samuel Gallego-Parra, Daniel Errandonea
Format: Article
Language:English
Published: Nature Portfolio 2024-11-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-024-78006-0
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1846172050086952960
author Jose Luis Rodrigo-Ramon
Simone Anzellini
Claudio Cazorla
Pablo Botella
Aser Garcia-Beamud
Josu Sanchez-Martin
Gaston Garbarino
Angelika D. Rosa
Samuel Gallego-Parra
Daniel Errandonea
author_facet Jose Luis Rodrigo-Ramon
Simone Anzellini
Claudio Cazorla
Pablo Botella
Aser Garcia-Beamud
Josu Sanchez-Martin
Gaston Garbarino
Angelika D. Rosa
Samuel Gallego-Parra
Daniel Errandonea
author_sort Jose Luis Rodrigo-Ramon
collection DOAJ
description Abstract The high-pressure and high-temperature structural, mechanical, and dinamical stability of rhodium has been investigated via synchrotron X-ray diffraction using a resistively heated diamond anvil cell and density functional theory. The isothermal compression data have been fitted with a Rydberg-Vinet equation of state (EoS) with best-fitting parameters $$V_0$$ V 0 =55.046(16) Å $$^3$$ 3 , $$K_0$$ K 0 = 251(3) GPa, and $$K'_0$$ K 0 ′ = 5.7(2). The thermal equation of state has been determined based upon the data collected following four different isotherms and has been fitted to a Holland and Powell thermal equation-of-state model with $$\alpha _0=$$ α 0 = 3.36(7)x10 $$^{-5}$$ - 5 K $$^{-1}$$ - 1 . The measured equation of state and structural parameters have been compared to the results of ab initio simulations. The agreement between theory and experiments is generally quite good. The present results solve controversies between previous studies which reported values of the bulk modulus from 240 to 300 GPa.
format Article
id doaj-art-9e1f9e9be9f04ec39b3eb548e20875e7
institution Kabale University
issn 2045-2322
language English
publishDate 2024-11-01
publisher Nature Portfolio
record_format Article
series Scientific Reports
spelling doaj-art-9e1f9e9be9f04ec39b3eb548e20875e72024-11-10T12:22:38ZengNature PortfolioScientific Reports2045-23222024-11-0114111310.1038/s41598-024-78006-0Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cellJose Luis Rodrigo-Ramon0Simone Anzellini1Claudio Cazorla2Pablo Botella3Aser Garcia-Beamud4Josu Sanchez-Martin5Gaston Garbarino6Angelika D. Rosa7Samuel Gallego-Parra8Daniel Errandonea9Department of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaDepartment of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaDepartment of Physics, Universitat Politècnica de CatalunyaDepartment of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaDepartment of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaDepartment of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaEuropean Synchrotron Radiation FacilityEuropean Synchrotron Radiation FacilityEuropean Synchrotron Radiation FacilityDepartment of Applied Physics - Institute of Materials Science, Matter at High Pressure (MALTA) Consolider Team, University of ValenciaAbstract The high-pressure and high-temperature structural, mechanical, and dinamical stability of rhodium has been investigated via synchrotron X-ray diffraction using a resistively heated diamond anvil cell and density functional theory. The isothermal compression data have been fitted with a Rydberg-Vinet equation of state (EoS) with best-fitting parameters $$V_0$$ V 0 =55.046(16) Å $$^3$$ 3 , $$K_0$$ K 0 = 251(3) GPa, and $$K'_0$$ K 0 ′ = 5.7(2). The thermal equation of state has been determined based upon the data collected following four different isotherms and has been fitted to a Holland and Powell thermal equation-of-state model with $$\alpha _0=$$ α 0 = 3.36(7)x10 $$^{-5}$$ - 5 K $$^{-1}$$ - 1 . The measured equation of state and structural parameters have been compared to the results of ab initio simulations. The agreement between theory and experiments is generally quite good. The present results solve controversies between previous studies which reported values of the bulk modulus from 240 to 300 GPa.https://doi.org/10.1038/s41598-024-78006-0
spellingShingle Jose Luis Rodrigo-Ramon
Simone Anzellini
Claudio Cazorla
Pablo Botella
Aser Garcia-Beamud
Josu Sanchez-Martin
Gaston Garbarino
Angelika D. Rosa
Samuel Gallego-Parra
Daniel Errandonea
Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
Scientific Reports
title Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
title_full Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
title_fullStr Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
title_full_unstemmed Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
title_short Thermal equation of state of rhodium characterized by XRD in a resistively heated diamond anvil cell
title_sort thermal equation of state of rhodium characterized by xrd in a resistively heated diamond anvil cell
url https://doi.org/10.1038/s41598-024-78006-0
work_keys_str_mv AT joseluisrodrigoramon thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT simoneanzellini thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT claudiocazorla thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT pablobotella thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT asergarciabeamud thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT josusanchezmartin thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT gastongarbarino thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT angelikadrosa thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT samuelgallegoparra thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell
AT danielerrandonea thermalequationofstateofrhodiumcharacterizedbyxrdinaresistivelyheateddiamondanvilcell