Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties

In order to investigate the effect of ion magnetron sputtering parameters on the scanning electron microscopy (SEM) images of nonconductive materials with different surface properties, the advantages and limitations of various ion magnetron sputtering conditions, including target material, sputterin...

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Main Author: ZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying
Format: Article
Language:zho
Published: Editorial Department of Materials Protection 2024-12-01
Series:Cailiao Baohu
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Online Access:http://www.mat-pro.com/fileup/1001-1560/PDF/20241212.pdf
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author ZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying
author_facet ZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying
author_sort ZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying
collection DOAJ
description In order to investigate the effect of ion magnetron sputtering parameters on the scanning electron microscopy (SEM) images of nonconductive materials with different surface properties, the advantages and limitations of various ion magnetron sputtering conditions, including target material, sputtering time and sputtering cycles were studied, along with their applicable ranges.Results showed that the gold target exhibited good continuity with large grain nucleation of gold.Due to its high sputtering energy, it easily caused thermal loss on the sample surface, and the gold grains adhered to the surface.Therefore, gold targets were found to be suitable for low -magnification SEM imaging(<10 000) and materials with a certain surface hardness.In contrast, the platinum target showed poor continuity with small platinum grain nucleation and lower sputtering energy.It was more likely to embed into the sample surface, forming a morphological framework, making it suitable for high-magnification SEM imaging (>30 000) and most non-conductive materials.Using a method of fewer, multiple ion magnetron sputtering cycles, reducing the sputtering cycles appropriately not only weakened the effect of the gold film on the material’s morphology and structure but also helped conserve resources and protect the environment.This result provides experimental guidance for researchers to scientifically and accurately analyze SEM images of samples.
format Article
id doaj-art-9c69d8fa1197418d8cac5261a716b902
institution Kabale University
issn 1001-1560
language zho
publishDate 2024-12-01
publisher Editorial Department of Materials Protection
record_format Article
series Cailiao Baohu
spelling doaj-art-9c69d8fa1197418d8cac5261a716b9022025-01-14T07:51:35ZzhoEditorial Department of Materials ProtectionCailiao Baohu1001-15602024-12-01571210711310.16577/j.issn.1001-1560.2024.0275Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface PropertiesZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying0(School of Materials and Energy, Guangdong University of Technology, Guangzhou 510006, China)In order to investigate the effect of ion magnetron sputtering parameters on the scanning electron microscopy (SEM) images of nonconductive materials with different surface properties, the advantages and limitations of various ion magnetron sputtering conditions, including target material, sputtering time and sputtering cycles were studied, along with their applicable ranges.Results showed that the gold target exhibited good continuity with large grain nucleation of gold.Due to its high sputtering energy, it easily caused thermal loss on the sample surface, and the gold grains adhered to the surface.Therefore, gold targets were found to be suitable for low -magnification SEM imaging(<10 000) and materials with a certain surface hardness.In contrast, the platinum target showed poor continuity with small platinum grain nucleation and lower sputtering energy.It was more likely to embed into the sample surface, forming a morphological framework, making it suitable for high-magnification SEM imaging (>30 000) and most non-conductive materials.Using a method of fewer, multiple ion magnetron sputtering cycles, reducing the sputtering cycles appropriately not only weakened the effect of the gold film on the material’s morphology and structure but also helped conserve resources and protect the environment.This result provides experimental guidance for researchers to scientifically and accurately analyze SEM images of samples.http://www.mat-pro.com/fileup/1001-1560/PDF/20241212.pdfscanning electron microscope; ion beam magnetron sputtering; non-conductive materials; surface properties; image
spellingShingle ZHANG Jie, ZOU Junwen, LIU Xueguang, LI Xiaoying
Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
Cailiao Baohu
scanning electron microscope; ion beam magnetron sputtering; non-conductive materials; surface properties; image
title Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
title_full Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
title_fullStr Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
title_full_unstemmed Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
title_short Effect of Ion Magnetron Sputtering Method on Scanning Electron Microscopy (SEM)Images of Materials with Different Surface Properties
title_sort effect of ion magnetron sputtering method on scanning electron microscopy sem images of materials with different surface properties
topic scanning electron microscope; ion beam magnetron sputtering; non-conductive materials; surface properties; image
url http://www.mat-pro.com/fileup/1001-1560/PDF/20241212.pdf
work_keys_str_mv AT zhangjiezoujunwenliuxueguanglixiaoying effectofionmagnetronsputteringmethodonscanningelectronmicroscopysemimagesofmaterialswithdifferentsurfaceproperties