The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)

Abstract.  Anise seeds can be processed into essential oils by steam distillation and solvent extraction. This research aims to produce a high oil yield by determining the optimum conditions of extraction, extracting anise seeds according to optimum conditions, producing anise oil with good quality...

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Main Authors: Arifah Sukasri, Wahyu Budi Utomo, Rahmiah Sjafruddin, Muhammad Nursam
Format: Article
Language:English
Published: Universitas Sebelas Maret 2023-05-01
Series:Equilibrium
Online Access:https://jurnal.uns.ac.id/equilibrium/article/view/73410
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author Arifah Sukasri
Wahyu Budi Utomo
Rahmiah Sjafruddin
Muhammad Nursam
author_facet Arifah Sukasri
Wahyu Budi Utomo
Rahmiah Sjafruddin
Muhammad Nursam
author_sort Arifah Sukasri
collection DOAJ
description Abstract.  Anise seeds can be processed into essential oils by steam distillation and solvent extraction. This research aims to produce a high oil yield by determining the optimum conditions of extraction, extracting anise seeds according to optimum conditions, producing anise oil with good quality based on 90% alcohol solubility analysis, analyzing the acid number, and conducting GC-MS analysis. The Activity Method was carried out by determining the optimum conditions of extraction on the effect of the variation in the ratio between anise seed powder and petroleum ether. Furthermore, based on optimal conditions, extraction was carried out at a temperature of 60°C, 5 hours with 5 repetitions. The results of essential oils were analyzed including solubility analysis, oil acid number, and GC-MS. The optimal extraction conditions were obtained at the ratio of anise seeds and petroleum ether 1:12.5 with an average oil yield of 4.72%. The results of the analysis showed that anise oil had good quality based on the oil solubility in 90% alcohol with a 1:7 ratio. The acid number of anise seed oil was obtained at 1.14444. GC-MS analysis showed that anise seed oil contained estragol, anethole, limonene, fenchone, and anis ketone. Keywords: Anise seeds, essential oil, soxhlet, GC-MS
format Article
id doaj-art-9150046af5f44cf2b71a195d0681a95b
institution Kabale University
issn 2622-3430
language English
publishDate 2023-05-01
publisher Universitas Sebelas Maret
record_format Article
series Equilibrium
spelling doaj-art-9150046af5f44cf2b71a195d0681a95b2024-12-03T03:06:44ZengUniversitas Sebelas MaretEquilibrium2622-34302023-05-0171596810.20961/equilibrium.v7i1.7341038366The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)Arifah Sukasri0Wahyu Budi Utomo1Rahmiah Sjafruddin2Muhammad Nursam3Politeknik Negeri Ujung PandangPoliteknik Negeri Ujung PandangPoliteknik Negeri Ujung PandangPoliteknik Negeri Ujung PandangAbstract.  Anise seeds can be processed into essential oils by steam distillation and solvent extraction. This research aims to produce a high oil yield by determining the optimum conditions of extraction, extracting anise seeds according to optimum conditions, producing anise oil with good quality based on 90% alcohol solubility analysis, analyzing the acid number, and conducting GC-MS analysis. The Activity Method was carried out by determining the optimum conditions of extraction on the effect of the variation in the ratio between anise seed powder and petroleum ether. Furthermore, based on optimal conditions, extraction was carried out at a temperature of 60°C, 5 hours with 5 repetitions. The results of essential oils were analyzed including solubility analysis, oil acid number, and GC-MS. The optimal extraction conditions were obtained at the ratio of anise seeds and petroleum ether 1:12.5 with an average oil yield of 4.72%. The results of the analysis showed that anise oil had good quality based on the oil solubility in 90% alcohol with a 1:7 ratio. The acid number of anise seed oil was obtained at 1.14444. GC-MS analysis showed that anise seed oil contained estragol, anethole, limonene, fenchone, and anis ketone. Keywords: Anise seeds, essential oil, soxhlet, GC-MShttps://jurnal.uns.ac.id/equilibrium/article/view/73410
spellingShingle Arifah Sukasri
Wahyu Budi Utomo
Rahmiah Sjafruddin
Muhammad Nursam
The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
Equilibrium
title The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
title_full The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
title_fullStr The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
title_full_unstemmed The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
title_short The Use of Soxhlet Techniques in the Essential Oil Extraction from Anise Seeds (Pimpinella anisum)
title_sort use of soxhlet techniques in the essential oil extraction from anise seeds pimpinella anisum
url https://jurnal.uns.ac.id/equilibrium/article/view/73410
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