Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation
The combustion method to obtain for pure graphitic carbon nitride (gCN) and two binary nanocomposites, gCN-Zn - gCN-Fe have been used in the present study. The structural, morphological, thermal and optical characterizations of the syhtesized samples were characterized with X-ray diffraction, scanni...
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Sakarya University
2023-06-01
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| Series: | Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi |
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| Online Access: | https://dergipark.org.tr/tr/download/article-file/2736417 |
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| author | Hasan Eskalen Mustafa Kavgacı |
| author_facet | Hasan Eskalen Mustafa Kavgacı |
| author_sort | Hasan Eskalen |
| collection | DOAJ |
| description | The combustion method to obtain for pure graphitic carbon nitride (gCN) and two binary nanocomposites, gCN-Zn - gCN-Fe have been used in the present study. The structural, morphological, thermal and optical characterizations of the syhtesized samples were characterized with X-ray diffraction, scanning electron microscopy, thermogravimetric analysis (TGA) and UV-Vis spectroscopy. The intensity of characteristic gCN peak at (002) crystalline plane decrease with formation of binary nanocomposites was observed. The EDX spectra supports presents of Zn and Fe element in binary nanocomposites. The bandgap of pristine gCN is calculated as 2.75 eV and it decreases to 2.58 eV and 2.50 eV for Zn and Fe addition. The degradation capacity of pristine gCN and synthesized binary nanocomposites showed an enhanced photodegradation performance for binary composite relative to pristine gCN was observed. The maximum degradation performance was observed at gCN-Zn binary composite. The obtained composites with this simple synthesis method and cost effective raw materials used for the photodegradation of methylene blue dye detail. |
| format | Article |
| id | doaj-art-8c964ac40b734881ba121d3c7cc0c859 |
| institution | Kabale University |
| issn | 2147-835X |
| language | English |
| publishDate | 2023-06-01 |
| publisher | Sakarya University |
| record_format | Article |
| series | Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi |
| spelling | doaj-art-8c964ac40b734881ba121d3c7cc0c8592024-12-23T08:15:28ZengSakarya UniversitySakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi2147-835X2023-06-0127353054110.16984/saufenbilder.119593428Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue DegradationHasan Eskalen0https://orcid.org/0000-0002-4523-6573Mustafa Kavgacı1https://orcid.org/0000-0001-8747-0635Kahramanmaraş Sütçü İmam ÜniversitesiKAHRAMANMARAŞ SÜTÇÜ İMAM ÜNİVERSİTESİThe combustion method to obtain for pure graphitic carbon nitride (gCN) and two binary nanocomposites, gCN-Zn - gCN-Fe have been used in the present study. The structural, morphological, thermal and optical characterizations of the syhtesized samples were characterized with X-ray diffraction, scanning electron microscopy, thermogravimetric analysis (TGA) and UV-Vis spectroscopy. The intensity of characteristic gCN peak at (002) crystalline plane decrease with formation of binary nanocomposites was observed. The EDX spectra supports presents of Zn and Fe element in binary nanocomposites. The bandgap of pristine gCN is calculated as 2.75 eV and it decreases to 2.58 eV and 2.50 eV for Zn and Fe addition. The degradation capacity of pristine gCN and synthesized binary nanocomposites showed an enhanced photodegradation performance for binary composite relative to pristine gCN was observed. The maximum degradation performance was observed at gCN-Zn binary composite. The obtained composites with this simple synthesis method and cost effective raw materials used for the photodegradation of methylene blue dye detail.https://dergipark.org.tr/tr/download/article-file/2736417degradationznfemethylene blue (mb)graphitic carbon nitride (gcn) |
| spellingShingle | Hasan Eskalen Mustafa Kavgacı Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi degradation zn fe methylene blue (mb) graphitic carbon nitride (gcn) |
| title | Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation |
| title_full | Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation |
| title_fullStr | Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation |
| title_full_unstemmed | Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation |
| title_short | Facile Synthesis and Characterization of gCN, gCN-Zn and gCN-Fe Binary Nanocomposite and Its Application as Photocatalyst for Methylene Blue Degradation |
| title_sort | facile synthesis and characterization of gcn gcn zn and gcn fe binary nanocomposite and its application as photocatalyst for methylene blue degradation |
| topic | degradation zn fe methylene blue (mb) graphitic carbon nitride (gcn) |
| url | https://dergipark.org.tr/tr/download/article-file/2736417 |
| work_keys_str_mv | AT hasaneskalen facilesynthesisandcharacterizationofgcngcnznandgcnfebinarynanocompositeanditsapplicationasphotocatalystformethylenebluedegradation AT mustafakavgacı facilesynthesisandcharacterizationofgcngcnznandgcnfebinarynanocompositeanditsapplicationasphotocatalystformethylenebluedegradation |