Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions

S355NL structural steel is extensively employed in bridges, ships, and power station equipment owing to its excellent tensile strength, weldability, and low-temperature toughness. However, pronounced fluctuations in its Charpy impact energy at low temperatures significantly compromise the reliabilit...

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Main Authors: Jiandong Yang, Bijun Xie, Mingyue Sun
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/15/7/802
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author Jiandong Yang
Bijun Xie
Mingyue Sun
author_facet Jiandong Yang
Bijun Xie
Mingyue Sun
author_sort Jiandong Yang
collection DOAJ
description S355NL structural steel is extensively employed in bridges, ships, and power station equipment owing to its excellent tensile strength, weldability, and low-temperature toughness. However, pronounced fluctuations in its Charpy impact energy at low temperatures significantly compromise the reliability and service life of critical components. In this study, vacuum-induction-melted ingots of S355NL steel containing 0–0.086 wt.% rare earth cerium were prepared. The effects of Ce on microstructures, inclusions, and impact toughness were systematically investigated using optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and Charpy V-notch testing. The results indicate that appropriate Ce additions (0.0011–0.0049 wt.%) refine the average grain size from 5.27 μm to 4.88 μm, reduce the pearlite interlamellar spacing from 204 nm to 169 nm, and promote the transformation of large-size Al<sub>2</sub>O<sub>3</sub>-MnS composite inclusions into fine, spherical, Ce-rich oxysulfides. Charpy V-notch tests at –50 °C reveal that 0.0011 wt.% Ce enhances both longitudinal (269.7 J) and transverse (257.4 J) absorbed energies while minimizing anisotropy (E_t/E_l  =  1.01). Conversely, excessive Ce addition (0.086 wt.%) leads to coarse inclusions and deteriorates impact performance. These findings establish an optimal Ce window (0.0011–0.0049 wt.%) for microstructural and inclusion engineering to enhance the low-temperature impact toughness of S355NL steel.
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spelling doaj-art-81d337a8fd6a4aee8366b8d17d708e6f2025-08-20T03:58:31ZengMDPI AGMetals2075-47012025-07-0115780210.3390/met15070802Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and InclusionsJiandong Yang0Bijun Xie1Mingyue Sun2Shenyang National Research Center for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShenyang National Research Center for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShenyang National Research Center for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaS355NL structural steel is extensively employed in bridges, ships, and power station equipment owing to its excellent tensile strength, weldability, and low-temperature toughness. However, pronounced fluctuations in its Charpy impact energy at low temperatures significantly compromise the reliability and service life of critical components. In this study, vacuum-induction-melted ingots of S355NL steel containing 0–0.086 wt.% rare earth cerium were prepared. The effects of Ce on microstructures, inclusions, and impact toughness were systematically investigated using optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and Charpy V-notch testing. The results indicate that appropriate Ce additions (0.0011–0.0049 wt.%) refine the average grain size from 5.27 μm to 4.88 μm, reduce the pearlite interlamellar spacing from 204 nm to 169 nm, and promote the transformation of large-size Al<sub>2</sub>O<sub>3</sub>-MnS composite inclusions into fine, spherical, Ce-rich oxysulfides. Charpy V-notch tests at –50 °C reveal that 0.0011 wt.% Ce enhances both longitudinal (269.7 J) and transverse (257.4 J) absorbed energies while minimizing anisotropy (E_t/E_l  =  1.01). Conversely, excessive Ce addition (0.086 wt.%) leads to coarse inclusions and deteriorates impact performance. These findings establish an optimal Ce window (0.0011–0.0049 wt.%) for microstructural and inclusion engineering to enhance the low-temperature impact toughness of S355NL steel.https://www.mdpi.com/2075-4701/15/7/802S355NL steelrare earth microalloyinggrain refinementinclusion modificationimpact toughness
spellingShingle Jiandong Yang
Bijun Xie
Mingyue Sun
Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
Metals
S355NL steel
rare earth microalloying
grain refinement
inclusion modification
impact toughness
title Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
title_full Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
title_fullStr Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
title_full_unstemmed Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
title_short Cerium Addition Enhances Impact Energy Stability in S355NL Steel by Tailoring Microstructure and Inclusions
title_sort cerium addition enhances impact energy stability in s355nl steel by tailoring microstructure and inclusions
topic S355NL steel
rare earth microalloying
grain refinement
inclusion modification
impact toughness
url https://www.mdpi.com/2075-4701/15/7/802
work_keys_str_mv AT jiandongyang ceriumadditionenhancesimpactenergystabilityins355nlsteelbytailoringmicrostructureandinclusions
AT bijunxie ceriumadditionenhancesimpactenergystabilityins355nlsteelbytailoringmicrostructureandinclusions
AT mingyuesun ceriumadditionenhancesimpactenergystabilityins355nlsteelbytailoringmicrostructureandinclusions