Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries

Lithium–sulfur batteries (LSBs) are gaining much attention because they offer a much higher theoretical energy density compared to traditional lithium-ion batteries. However, the cycling performance of LSBs with high sulfur mass loading is poor due to the shuttle effect, limiting the practical appli...

Full description

Saved in:
Bibliographic Details
Main Authors: Yupu Shi, Jianbin Xu, Xian Du, Yi Zhang, Fan Zhao, Ziwei Tang, Le Kang, Huiling Du
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Batteries
Subjects:
Online Access:https://www.mdpi.com/2313-0105/10/12/430
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1846105859344564224
author Yupu Shi
Jianbin Xu
Xian Du
Yi Zhang
Fan Zhao
Ziwei Tang
Le Kang
Huiling Du
author_facet Yupu Shi
Jianbin Xu
Xian Du
Yi Zhang
Fan Zhao
Ziwei Tang
Le Kang
Huiling Du
author_sort Yupu Shi
collection DOAJ
description Lithium–sulfur batteries (LSBs) are gaining much attention because they offer a much higher theoretical energy density compared to traditional lithium-ion batteries. However, the cycling performance of LSBs with high sulfur mass loading is poor due to the shuttle effect, limiting the practical application of LSBs. In this work, a unique porous sulfur/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@selenium (S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>@Se) cathode of a LSB is synthesized by a simple hydrothermal method to address these challenges. In this composite, Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> forms a conductive framework and Se is tightly anchored on the framework. The Se inhibits the agglomeration of Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> and prevents the collapse of Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>. The S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>@Se composite can adsorb lithium polysulfides (LiPSs) and suppresses the shuttle effect and volume changes during cycling, improving the cycling stability of LSBs with high S loading. A high capacity of 812.2 mAh g<sup>−1</sup> at 0.1 C with 5.0 mg cm<sup>−2</sup> sulfur mass loading after 100 cycles is obtained. This work could inspire further research into high-performance S host materials for high-S-loading LSBs.
format Article
id doaj-art-81c467cdadf54503b3a33df3f2ffb2ec
institution Kabale University
issn 2313-0105
language English
publishDate 2024-12-01
publisher MDPI AG
record_format Article
series Batteries
spelling doaj-art-81c467cdadf54503b3a33df3f2ffb2ec2024-12-27T14:10:39ZengMDPI AGBatteries2313-01052024-12-01101243010.3390/batteries10120430Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur BatteriesYupu Shi0Jianbin Xu1Xian Du2Yi Zhang3Fan Zhao4Ziwei Tang5Le Kang6Huiling Du7College of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaTianjin Sanyuan Electric Power Group Co., Ltd., Tianjin 300010, ChinaCollege of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Energy Sciences and Engineering, Nanjing Tech University, Nanjing 211816, ChinaCollege of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaCollege of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaCollege of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaCollege of Materials Science and Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaLithium–sulfur batteries (LSBs) are gaining much attention because they offer a much higher theoretical energy density compared to traditional lithium-ion batteries. However, the cycling performance of LSBs with high sulfur mass loading is poor due to the shuttle effect, limiting the practical application of LSBs. In this work, a unique porous sulfur/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@selenium (S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>@Se) cathode of a LSB is synthesized by a simple hydrothermal method to address these challenges. In this composite, Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> forms a conductive framework and Se is tightly anchored on the framework. The Se inhibits the agglomeration of Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> and prevents the collapse of Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>. The S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>@Se composite can adsorb lithium polysulfides (LiPSs) and suppresses the shuttle effect and volume changes during cycling, improving the cycling stability of LSBs with high S loading. A high capacity of 812.2 mAh g<sup>−1</sup> at 0.1 C with 5.0 mg cm<sup>−2</sup> sulfur mass loading after 100 cycles is obtained. This work could inspire further research into high-performance S host materials for high-S-loading LSBs.https://www.mdpi.com/2313-0105/10/12/430seleniumTi<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxenecathodelithium–sulfur batterieshigh loading
spellingShingle Yupu Shi
Jianbin Xu
Xian Du
Yi Zhang
Fan Zhao
Ziwei Tang
Le Kang
Huiling Du
Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
Batteries
selenium
Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene
cathode
lithium–sulfur batteries
high loading
title Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
title_full Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
title_fullStr Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
title_full_unstemmed Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
title_short Facile Synthesis of S/Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene@Se Cathode for High-Sulfur-Loading Lithium–Sulfur Batteries
title_sort facile synthesis of s ti sub 3 sub c sub 2 sub t sub x sub mxene se cathode for high sulfur loading lithium sulfur batteries
topic selenium
Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub> Mxene
cathode
lithium–sulfur batteries
high loading
url https://www.mdpi.com/2313-0105/10/12/430
work_keys_str_mv AT yupushi facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT jianbinxu facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT xiandu facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT yizhang facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT fanzhao facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT ziweitang facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT lekang facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries
AT huilingdu facilesynthesisofstisub3subcsub2subtsubxsubmxenesecathodeforhighsulfurloadinglithiumsulfurbatteries