Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors

Zinc oxide nanoparticles (ZnO NPs), copper oxide nanoparticles (CuO NPs) and CuO@ZnO NPs as a colloidal core-shell solution were synthesized by laser ablation. A Nd:YAG laser with an energy of 700 mJ, a wavelength of 1064 nm and 200 pulses was used for the ablation process. The colloidal solution wa...

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Main Authors: Salah Abdul Aziz, Uday Nayef, Mohammed Rasheed
Format: Article
Language:English
Published: University of Technology, Baghdad 2024-12-01
Series:Journal of Applied Sciences and Nanotechnology
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Online Access:https://jasn.uotechnology.edu.iq/article_24386_bc525d9cfbc441061c3abe7846001ae9.pdf
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author Salah Abdul Aziz
Uday Nayef
Mohammed Rasheed
author_facet Salah Abdul Aziz
Uday Nayef
Mohammed Rasheed
author_sort Salah Abdul Aziz
collection DOAJ
description Zinc oxide nanoparticles (ZnO NPs), copper oxide nanoparticles (CuO NPs) and CuO@ZnO NPs as a colloidal core-shell solution were synthesized by laser ablation. A Nd:YAG laser with an energy of 700 mJ, a wavelength of 1064 nm and 200 pulses was used for the ablation process. The colloidal solution was deposited on porous silicon (PSi) using the drop-casting method. The PSi substrates were prepared by photoelectrochemical etching (PECE) on n-type (111) silicon wafers. The study investigated the influence on the electrical, optical, morphological and structural properties of the CuO NPs and ZnO NPs samples when they were converted into a core-shell, specifically for their use in photodetector applications. XRD analysis revealed the presence of CuO, ZnO and CuO@ZnO by diffraction peaks at different angles. According to the SEM images, the nanoparticles show randomly distributed spherical grains, while PSi exhibits a sponge-like structure. The core-shell shape is confirmed by TEM images, which show a dark inner region consisting of CuO NPs and a much lighter outer region consisting of the ZnO nanoshell. The optical properties of the CuO@ZnO NPs were investigated and a minimum energy gap of 2.8 eV was found. The CuO@ZnO NPs/PSi/n-Si photodetector showed improved current-voltage (J-V) characteristics, rectifying properties and remarkable sensitivity in the visible to near-infrared region compared to other photodetector samples. The fabricated photodetector confirmed improved quantum performance, especially in the visible spectrum. The work aims to synthesize CuO@ZnO core-shell nanoparticles by a laser ablation technique to improve the electrical properties and spectral response of photodetectors.
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spelling doaj-art-8071bcd08a8d4cdaa3e4120913df97b42024-12-10T07:31:53ZengUniversity of Technology, BaghdadJournal of Applied Sciences and Nanotechnology2788-68672024-12-0144627610.53293/jasn.2024.7496.132024386Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of PhotodetectorsSalah Abdul Aziz0Uday Nayef1Mohammed Rasheed2Sumer University-Department of Science, Dhi Qar, IraqDepartment of Applied Sciences, University of Technology - Iraq, IraqDepartment of Applied Sciences, University of Technology - Iraq, IraqZinc oxide nanoparticles (ZnO NPs), copper oxide nanoparticles (CuO NPs) and CuO@ZnO NPs as a colloidal core-shell solution were synthesized by laser ablation. A Nd:YAG laser with an energy of 700 mJ, a wavelength of 1064 nm and 200 pulses was used for the ablation process. The colloidal solution was deposited on porous silicon (PSi) using the drop-casting method. The PSi substrates were prepared by photoelectrochemical etching (PECE) on n-type (111) silicon wafers. The study investigated the influence on the electrical, optical, morphological and structural properties of the CuO NPs and ZnO NPs samples when they were converted into a core-shell, specifically for their use in photodetector applications. XRD analysis revealed the presence of CuO, ZnO and CuO@ZnO by diffraction peaks at different angles. According to the SEM images, the nanoparticles show randomly distributed spherical grains, while PSi exhibits a sponge-like structure. The core-shell shape is confirmed by TEM images, which show a dark inner region consisting of CuO NPs and a much lighter outer region consisting of the ZnO nanoshell. The optical properties of the CuO@ZnO NPs were investigated and a minimum energy gap of 2.8 eV was found. The CuO@ZnO NPs/PSi/n-Si photodetector showed improved current-voltage (J-V) characteristics, rectifying properties and remarkable sensitivity in the visible to near-infrared region compared to other photodetector samples. The fabricated photodetector confirmed improved quantum performance, especially in the visible spectrum. The work aims to synthesize CuO@ZnO core-shell nanoparticles by a laser ablation technique to improve the electrical properties and spectral response of photodetectors.https://jasn.uotechnology.edu.iq/article_24386_bc525d9cfbc441061c3abe7846001ae9.pdfcuo@zno core-shelllaser ablationporous siliconcolloidal solutionphotodetectors
spellingShingle Salah Abdul Aziz
Uday Nayef
Mohammed Rasheed
Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
Journal of Applied Sciences and Nanotechnology
cuo@zno core-shell
laser ablation
porous silicon
colloidal solution
photodetectors
title Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
title_full Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
title_fullStr Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
title_full_unstemmed Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
title_short Manufacturing of CuO@ZnO Nanoparticles Core-Shell for Enhancing Electrical Properties and Spectral Responsivity of Photodetectors
title_sort manufacturing of cuo zno nanoparticles core shell for enhancing electrical properties and spectral responsivity of photodetectors
topic cuo@zno core-shell
laser ablation
porous silicon
colloidal solution
photodetectors
url https://jasn.uotechnology.edu.iq/article_24386_bc525d9cfbc441061c3abe7846001ae9.pdf
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AT udaynayef manufacturingofcuoznonanoparticlescoreshellforenhancingelectricalpropertiesandspectralresponsivityofphotodetectors
AT mohammedrasheed manufacturingofcuoznonanoparticlescoreshellforenhancingelectricalpropertiesandspectralresponsivityofphotodetectors