A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography
A sensitive, economical, and miniaturized self-assembly needle tip nanocomposite Polyaniline-K10 solid-phase microextraction (NDT/PAN-K10-SPNE) coupled with high-performance liquid chromatography UV detection was developed for rapid extraction removal and determination of methoxyfenozide in environm...
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| Format: | Article |
| Language: | English |
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Iranian Chemical Society
2023-07-01
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| Series: | Nanochemistry Research |
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| Online Access: | http://www.nanochemres.org/article_171721_01c753a9f3aa1cacbed9a9b14593edce.pdf |
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| author | Marzieh Piryaei Mir Mahdi Abolghasemi Monireh Sobhi |
| author_facet | Marzieh Piryaei Mir Mahdi Abolghasemi Monireh Sobhi |
| author_sort | Marzieh Piryaei |
| collection | DOAJ |
| description | A sensitive, economical, and miniaturized self-assembly needle tip nanocomposite Polyaniline-K10 solid-phase microextraction (NDT/PAN-K10-SPNE) coupled with high-performance liquid chromatography UV detection was developed for rapid extraction removal and determination of methoxyfenozide in environmental water samples. The NDT/PAN-K10-SPE cartridge, assembled by packing 2.0 mg of PAN-K10 as sorbent into a needle tip, showed high adsorption capacity for methoxyfenozide owing to the large surface area and unique structure of PAN-K10. The factors that affected the extraction efficiency of PT-G-SPE, including sample volume, pH, sorbent amount, washing solvent and eluent solvent, were optimized. Good linearity for methoxyfenozide was obtained in a range of 0/01–100 µg mL−1 with the correlation coefficient of (R2) = 0.999. The recoveries of the methoxyfenozide at three spiked levels ranged from 84.72% to 100.03% with the relative standard deviations (RSD) of 3.78%. It is also noteworthy that the applied method is economical and has a good linear range, reproducibility, and high sensitivity. |
| format | Article |
| id | doaj-art-75d29c62700a4009accc317019e5573a |
| institution | Kabale University |
| issn | 2538-4279 2423-818X |
| language | English |
| publishDate | 2023-07-01 |
| publisher | Iranian Chemical Society |
| record_format | Article |
| series | Nanochemistry Research |
| spelling | doaj-art-75d29c62700a4009accc317019e5573a2025-01-12T10:24:45ZengIranian Chemical SocietyNanochemistry Research2538-42792423-818X2023-07-018319720410.22036/ncr.2023.03.005171721A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid ChromatographyMarzieh Piryaei0Mir Mahdi Abolghasemi1Monireh Sobhi2Department of Chemistry, Faculty of Science, University of Maragheh, Maragheh, IranDepartment of Chemistry, Faculty of Science, University of Maragheh, Maragheh, IranDepartment of Chemistry, Faculty of Science, University of Maragheh, Maragheh, IranA sensitive, economical, and miniaturized self-assembly needle tip nanocomposite Polyaniline-K10 solid-phase microextraction (NDT/PAN-K10-SPNE) coupled with high-performance liquid chromatography UV detection was developed for rapid extraction removal and determination of methoxyfenozide in environmental water samples. The NDT/PAN-K10-SPE cartridge, assembled by packing 2.0 mg of PAN-K10 as sorbent into a needle tip, showed high adsorption capacity for methoxyfenozide owing to the large surface area and unique structure of PAN-K10. The factors that affected the extraction efficiency of PT-G-SPE, including sample volume, pH, sorbent amount, washing solvent and eluent solvent, were optimized. Good linearity for methoxyfenozide was obtained in a range of 0/01–100 µg mL−1 with the correlation coefficient of (R2) = 0.999. The recoveries of the methoxyfenozide at three spiked levels ranged from 84.72% to 100.03% with the relative standard deviations (RSD) of 3.78%. It is also noteworthy that the applied method is economical and has a good linear range, reproducibility, and high sensitivity.http://www.nanochemres.org/article_171721_01c753a9f3aa1cacbed9a9b14593edce.pdfneedle tip polyaniline-k10 solid-phase microextractionmethoxyfenozidehight performance liquid chromatography uv detectionenvironmental water |
| spellingShingle | Marzieh Piryaei Mir Mahdi Abolghasemi Monireh Sobhi A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography Nanochemistry Research needle tip polyaniline-k10 solid-phase microextraction methoxyfenozide hight performance liquid chromatography uv detection environmental water |
| title | A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography |
| title_full | A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography |
| title_fullStr | A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography |
| title_full_unstemmed | A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography |
| title_short | A New Method for Extracting and Measuring Methoxyfenozide Using ND/PAN-K10 SPE Using High Performance Liquid Chromatography |
| title_sort | new method for extracting and measuring methoxyfenozide using nd pan k10 spe using high performance liquid chromatography |
| topic | needle tip polyaniline-k10 solid-phase microextraction methoxyfenozide hight performance liquid chromatography uv detection environmental water |
| url | http://www.nanochemres.org/article_171721_01c753a9f3aa1cacbed9a9b14593edce.pdf |
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