Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography
In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer (50.0 mM, pH 4.0):acetonitrile (55:45 v/v) as m...
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Sakarya University
2023-10-01
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| Series: | Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi |
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| Online Access: | https://dergipark.org.tr/tr/download/article-file/3012399 |
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| author | Tuğçe Unutkan Gösterişli |
| author_facet | Tuğçe Unutkan Gösterişli |
| author_sort | Tuğçe Unutkan Gösterişli |
| collection | DOAJ |
| description | In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer (50.0 mM, pH 4.0):acetonitrile (55:45 v/v) as mobile phase. Under the optimal conditions, the limits of detection and quantification (LOD and LOQ) were found as 7.4 – 24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable % recoveries in the range of 81.4–112.9%, while the values of relative standard deviation (RSD) were below 10% showing a satisfactory applicability for cymoxanil in such complex real samples matrix. |
| format | Article |
| id | doaj-art-700cb4743a2645e0b13f1288f9021e9b |
| institution | Kabale University |
| issn | 2147-835X |
| language | English |
| publishDate | 2023-10-01 |
| publisher | Sakarya University |
| record_format | Article |
| series | Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi |
| spelling | doaj-art-700cb4743a2645e0b13f1288f9021e9b2024-12-23T08:15:40ZengSakarya UniversitySakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi2147-835X2023-10-012751002100710.16984/saufenbilder.126550728Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid ChromatographyTuğçe Unutkan Gösterişli0https://orcid.org/0000-0002-1143-4192YILDIZ TECHNICAL UNIVERSITYIn this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer (50.0 mM, pH 4.0):acetonitrile (55:45 v/v) as mobile phase. Under the optimal conditions, the limits of detection and quantification (LOD and LOQ) were found as 7.4 – 24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable % recoveries in the range of 81.4–112.9%, while the values of relative standard deviation (RSD) were below 10% showing a satisfactory applicability for cymoxanil in such complex real samples matrix.https://dergipark.org.tr/tr/download/article-file/3012399cymoxanilpotato flourhigh performance liquid chromatographyfungidice |
| spellingShingle | Tuğçe Unutkan Gösterişli Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi cymoxanil potato flour high performance liquid chromatography fungidice |
| title | Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography |
| title_full | Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography |
| title_fullStr | Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography |
| title_full_unstemmed | Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography |
| title_short | Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography |
| title_sort | development of an analytical method for the determination of cymoxanil in potato flour samples by high performance liquid chromatography |
| topic | cymoxanil potato flour high performance liquid chromatography fungidice |
| url | https://dergipark.org.tr/tr/download/article-file/3012399 |
| work_keys_str_mv | AT tugceunutkangosterisli developmentofananalyticalmethodforthedeterminationofcymoxanilinpotatofloursamplesbyhighperformanceliquidchromatography |