Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth

Water, a vital resource for ecosystems and human populations, is facing increasing nitrate contamination due to agricultural runoff, industrial discharge and improper waste disposal. The present study focuses on the efficacy of nitrate removal through adsorption using fuller’s earth (FE) and modifie...

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Main Authors: Bhagyeshwari D Chalageri, Rajeswari M Kulkarni, Archna Narula
Format: Article
Language:English
Published: Taylor & Francis Group 2024-12-01
Series:International Journal of Sustainable Engineering
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Online Access:https://www.tandfonline.com/doi/10.1080/19397038.2024.2387434
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author Bhagyeshwari D Chalageri
Rajeswari M Kulkarni
Archna Narula
author_facet Bhagyeshwari D Chalageri
Rajeswari M Kulkarni
Archna Narula
author_sort Bhagyeshwari D Chalageri
collection DOAJ
description Water, a vital resource for ecosystems and human populations, is facing increasing nitrate contamination due to agricultural runoff, industrial discharge and improper waste disposal. The present study focuses on the efficacy of nitrate removal through adsorption using fuller’s earth (FE) and modified fuller’s earth (acid-treated) (MFE) as adsorbents. The impact of initial pH (2.0–7.0), contact time (5–240 min), adsorbent dosage (1–30 g/L), initial nitrate concentration (50–250 mg/L) and temperature (30–50°C) on nitrate removal using fuller’s earth were studied. The maximum nitrate removal was observed at pH 2.0, and equilibrium was reached in 120 min at 30℃. The Freundlich isotherm best fit the equilibrium data. The maximum nitrate uptake of fuller’s earth and modified fuller’s earth were 84.75 mg/g and 85.47 mg/g, respectively. Nitrate removal by FE and MFE followed a second-order kinetic equation. Thermodynamic studies showed spontaneity and the exothermic nature of the nitrate adsorption process. ∆H° values were −44.96 and −42.63 kJmol−1 for FE and MFE and ΔS° was −85.11 and −74.52 Jk−1mol−1 for FE and MFE, respectively. FE, known for its exceptional adsorption capacity owing to its porous structure and high ion-exchange capacity, has demonstrated a remarkable affinity for nitrate ions in batch studies.
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spelling doaj-art-465e384dc33e4b7ca4f767a9635527dd2024-12-12T09:12:39ZengTaylor & Francis GroupInternational Journal of Sustainable Engineering1939-70381939-70462024-12-0117160161210.1080/19397038.2024.2387434Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earthBhagyeshwari D Chalageri0Rajeswari M Kulkarni1Archna Narula2Department of Chemical Engineering, Ramaiah Institute of Technology, Bengaluru, IndiaDepartment of Chemical Engineering, Ramaiah Institute of Technology, Bengaluru, IndiaDepartment of Chemical Engineering, Ramaiah Institute of Technology, Bengaluru, IndiaWater, a vital resource for ecosystems and human populations, is facing increasing nitrate contamination due to agricultural runoff, industrial discharge and improper waste disposal. The present study focuses on the efficacy of nitrate removal through adsorption using fuller’s earth (FE) and modified fuller’s earth (acid-treated) (MFE) as adsorbents. The impact of initial pH (2.0–7.0), contact time (5–240 min), adsorbent dosage (1–30 g/L), initial nitrate concentration (50–250 mg/L) and temperature (30–50°C) on nitrate removal using fuller’s earth were studied. The maximum nitrate removal was observed at pH 2.0, and equilibrium was reached in 120 min at 30℃. The Freundlich isotherm best fit the equilibrium data. The maximum nitrate uptake of fuller’s earth and modified fuller’s earth were 84.75 mg/g and 85.47 mg/g, respectively. Nitrate removal by FE and MFE followed a second-order kinetic equation. Thermodynamic studies showed spontaneity and the exothermic nature of the nitrate adsorption process. ∆H° values were −44.96 and −42.63 kJmol−1 for FE and MFE and ΔS° was −85.11 and −74.52 Jk−1mol−1 for FE and MFE, respectively. FE, known for its exceptional adsorption capacity owing to its porous structure and high ion-exchange capacity, has demonstrated a remarkable affinity for nitrate ions in batch studies.https://www.tandfonline.com/doi/10.1080/19397038.2024.2387434Nitrate removalmodified fuller’s earthadsorption isothermskinetic models
spellingShingle Bhagyeshwari D Chalageri
Rajeswari M Kulkarni
Archna Narula
Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
International Journal of Sustainable Engineering
Nitrate removal
modified fuller’s earth
adsorption isotherms
kinetic models
title Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
title_full Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
title_fullStr Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
title_full_unstemmed Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
title_short Nitrate removal from aqueous solution using fuller’s earth and modified fuller’s earth
title_sort nitrate removal from aqueous solution using fuller s earth and modified fuller s earth
topic Nitrate removal
modified fuller’s earth
adsorption isotherms
kinetic models
url https://www.tandfonline.com/doi/10.1080/19397038.2024.2387434
work_keys_str_mv AT bhagyeshwaridchalageri nitrateremovalfromaqueoussolutionusingfullersearthandmodifiedfullersearth
AT rajeswarimkulkarni nitrateremovalfromaqueoussolutionusingfullersearthandmodifiedfullersearth
AT archnanarula nitrateremovalfromaqueoussolutionusingfullersearthandmodifiedfullersearth