High-throughput screening of multimetallic catalysts for three-way catalysis

Multimetallic nanoparticles (MNPs) have appeared as promising catalysts for important catalytic reactions such as three-way catalysis (TWC) due to their synergistic effects. Herein, a comprehensive process of preparing and evaluating MNPs and supported catalysts using high-throughput experimentation...

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Main Authors: Son Dinh Le, Nhan Nu Thanh Ton, Kalaivani Seenivasan, Patchanee Chammingkwan, Koichi Higashimine, Supareak Praserthdam, Toshiaki Taniike
Format: Article
Language:English
Published: Taylor & Francis Group 2024-12-01
Series:Science and Technology of Advanced Materials: Methods
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Online Access:https://www.tandfonline.com/doi/10.1080/27660400.2023.2284130
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author Son Dinh Le
Nhan Nu Thanh Ton
Kalaivani Seenivasan
Patchanee Chammingkwan
Koichi Higashimine
Supareak Praserthdam
Toshiaki Taniike
author_facet Son Dinh Le
Nhan Nu Thanh Ton
Kalaivani Seenivasan
Patchanee Chammingkwan
Koichi Higashimine
Supareak Praserthdam
Toshiaki Taniike
author_sort Son Dinh Le
collection DOAJ
description Multimetallic nanoparticles (MNPs) have appeared as promising catalysts for important catalytic reactions such as three-way catalysis (TWC) due to their synergistic effects. Herein, a comprehensive process of preparing and evaluating MNPs and supported catalysts using high-throughput experimentation (HTE) for TWC is demonstrated. The synthesis of MNPs via a hot-injection method is performed using a homemade parallel reactor. The prepared MNPs are impregnated in parallel on alumina and examined for TWC. An in-house fixed-bed reactor equipped with a quadrupole mass spectrometer was employed for catalyst evaluation, taking advantage of the rapid screening of 20 catalysts and multiple reaction conditions. The overall HTE system can facilitate the synthesis and evaluation of 51 multimetallic catalysts for TWC in less than 2 weeks, and also appear to be a flexible and versatile system for other applications.
format Article
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institution Kabale University
issn 2766-0400
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publishDate 2024-12-01
publisher Taylor & Francis Group
record_format Article
series Science and Technology of Advanced Materials: Methods
spelling doaj-art-404f1580a7b542e6bdc73bcf8c1f7edc2024-12-10T09:58:05ZengTaylor & Francis GroupScience and Technology of Advanced Materials: Methods2766-04002024-12-014110.1080/27660400.2023.2284130High-throughput screening of multimetallic catalysts for three-way catalysisSon Dinh Le0Nhan Nu Thanh Ton1Kalaivani Seenivasan2Patchanee Chammingkwan3Koichi Higashimine4Supareak Praserthdam5Toshiaki Taniike6Graduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanGraduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanGraduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanGraduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanGraduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanHigh-Performance Computing Unit (CECC-HCU), Center of Excellence on Catalysis and Catalytic Reaction Engineering (CECC), Chulalongkorn University, Bangkok, ThailandGraduate School of Advanced Science and Technology, Japan Advanced Institute of Science and Technology (JAIST), Nomi, JapanMultimetallic nanoparticles (MNPs) have appeared as promising catalysts for important catalytic reactions such as three-way catalysis (TWC) due to their synergistic effects. Herein, a comprehensive process of preparing and evaluating MNPs and supported catalysts using high-throughput experimentation (HTE) for TWC is demonstrated. The synthesis of MNPs via a hot-injection method is performed using a homemade parallel reactor. The prepared MNPs are impregnated in parallel on alumina and examined for TWC. An in-house fixed-bed reactor equipped with a quadrupole mass spectrometer was employed for catalyst evaluation, taking advantage of the rapid screening of 20 catalysts and multiple reaction conditions. The overall HTE system can facilitate the synthesis and evaluation of 51 multimetallic catalysts for TWC in less than 2 weeks, and also appear to be a flexible and versatile system for other applications.https://www.tandfonline.com/doi/10.1080/27660400.2023.2284130High-throughputmultimetallicthree-way catalystautomotive catalystCO oxidation, NO reduction
spellingShingle Son Dinh Le
Nhan Nu Thanh Ton
Kalaivani Seenivasan
Patchanee Chammingkwan
Koichi Higashimine
Supareak Praserthdam
Toshiaki Taniike
High-throughput screening of multimetallic catalysts for three-way catalysis
Science and Technology of Advanced Materials: Methods
High-throughput
multimetallic
three-way catalyst
automotive catalyst
CO oxidation, NO reduction
title High-throughput screening of multimetallic catalysts for three-way catalysis
title_full High-throughput screening of multimetallic catalysts for three-way catalysis
title_fullStr High-throughput screening of multimetallic catalysts for three-way catalysis
title_full_unstemmed High-throughput screening of multimetallic catalysts for three-way catalysis
title_short High-throughput screening of multimetallic catalysts for three-way catalysis
title_sort high throughput screening of multimetallic catalysts for three way catalysis
topic High-throughput
multimetallic
three-way catalyst
automotive catalyst
CO oxidation, NO reduction
url https://www.tandfonline.com/doi/10.1080/27660400.2023.2284130
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