Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process

In order to minimize the impact of oxide inclusions on the quality of Si-Mn deoxidized steel, the effects of heat treatment temperature and holding time on the inclusion composition and morphology were studied. LX82A billets were heated isothermally at 1000, 1100, and 1200°C for 8, 10, and 12 hours,...

Full description

Saved in:
Bibliographic Details
Main Authors: Nie X.-L., Xu Q., Xie X., Li J.-L.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2025-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
Subjects:
Online Access:https://doiserbia.nb.rs/img/doi/1450-5339/2025/1450-53392500009N.pdf
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849247427053223936
author Nie X.-L.
Xu Q.
Xie X.
Li J.-L.
author_facet Nie X.-L.
Xu Q.
Xie X.
Li J.-L.
author_sort Nie X.-L.
collection DOAJ
description In order to minimize the impact of oxide inclusions on the quality of Si-Mn deoxidized steel, the effects of heat treatment temperature and holding time on the inclusion composition and morphology were studied. LX82A billets were heated isothermally at 1000, 1100, and 1200°C for 8, 10, and 12 hours, respectively. The experimental results show that as the heat treatment temperature increases, calcium treatment and the reduction of the w(Al2O3 + MgO) / w(SiO2 + MnO) ratio enhance the deformability of the oxide inclusions. This causes a gradual transition in inclusion shape from oval to round. At 1200°C, the oxide inclusions are predominantly regular and round. With increasing heat treatment temperature and holding time, the oxide inclusions in Si-Mn deoxidized steel shift from the CaO-SiO2-Al2O3 system to the MnO-SiO2-Al2O3 system. At a constant temperature, the highest inclusion transformation rate and the most uniform composition occur at a 10-hour holding time. At 1200°C, an alternative calcium treatment and the steel matrix-inclusion interface reaction increase the MnO content at the interface, reducing the manganese content in the steel and forming a Mn-depleted zone. This decreases austenite stability, enhances ferrite nucleation, and improves the steel quality and performance. Therefore, controlling the heat treatment temperature around 1200°C is crucial.
format Article
id doaj-art-3c6cdea8048a4af2b10377b024c40d1c
institution Kabale University
issn 1450-5339
2217-7175
language English
publishDate 2025-01-01
publisher University of Belgrade, Technical Faculty, Bor
record_format Article
series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-3c6cdea8048a4af2b10377b024c40d1c2025-08-20T03:58:14ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392217-71752025-01-0161111112410.2298/JMMB250109009N1450-53392500009NEvolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating processNie X.-L.0Xu Q.1Xie X.2Li J.-L.3Key Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education, Wuhan University of Science and Technology, Wuhan, Hubei, ChinaKey Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education, Wuhan University of Science and Technology, Wuhan, Hubei, ChinaKey Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education, Wuhan University of Science and Technology, Wuhan, Hubei, ChinaKey Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education, Wuhan University of Science and Technology, Wuhan, Hubei, China + Hubei Provincial Key Laboratory for New Processes of Ironmaking and Steelmaking, Wuhan University of Science and Technology, Wuhan, Hubei, ChinaIn order to minimize the impact of oxide inclusions on the quality of Si-Mn deoxidized steel, the effects of heat treatment temperature and holding time on the inclusion composition and morphology were studied. LX82A billets were heated isothermally at 1000, 1100, and 1200°C for 8, 10, and 12 hours, respectively. The experimental results show that as the heat treatment temperature increases, calcium treatment and the reduction of the w(Al2O3 + MgO) / w(SiO2 + MnO) ratio enhance the deformability of the oxide inclusions. This causes a gradual transition in inclusion shape from oval to round. At 1200°C, the oxide inclusions are predominantly regular and round. With increasing heat treatment temperature and holding time, the oxide inclusions in Si-Mn deoxidized steel shift from the CaO-SiO2-Al2O3 system to the MnO-SiO2-Al2O3 system. At a constant temperature, the highest inclusion transformation rate and the most uniform composition occur at a 10-hour holding time. At 1200°C, an alternative calcium treatment and the steel matrix-inclusion interface reaction increase the MnO content at the interface, reducing the manganese content in the steel and forming a Mn-depleted zone. This decreases austenite stability, enhances ferrite nucleation, and improves the steel quality and performance. Therefore, controlling the heat treatment temperature around 1200°C is crucial.https://doiserbia.nb.rs/img/doi/1450-5339/2025/1450-53392500009N.pdfsi-mn deoxidized steeloxide inclusionheat treatmenttemperatureholding timecomposition changes
spellingShingle Nie X.-L.
Xu Q.
Xie X.
Li J.-L.
Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
Journal of Mining and Metallurgy. Section B: Metallurgy
si-mn deoxidized steel
oxide inclusion
heat treatment
temperature
holding time
composition changes
title Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
title_full Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
title_fullStr Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
title_full_unstemmed Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
title_short Evolution behavior of oxide inclusions in Si-Mn deoxidized steel during billet heating process
title_sort evolution behavior of oxide inclusions in si mn deoxidized steel during billet heating process
topic si-mn deoxidized steel
oxide inclusion
heat treatment
temperature
holding time
composition changes
url https://doiserbia.nb.rs/img/doi/1450-5339/2025/1450-53392500009N.pdf
work_keys_str_mv AT niexl evolutionbehaviorofoxideinclusionsinsimndeoxidizedsteelduringbilletheatingprocess
AT xuq evolutionbehaviorofoxideinclusionsinsimndeoxidizedsteelduringbilletheatingprocess
AT xiex evolutionbehaviorofoxideinclusionsinsimndeoxidizedsteelduringbilletheatingprocess
AT lijl evolutionbehaviorofoxideinclusionsinsimndeoxidizedsteelduringbilletheatingprocess