Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties

The synthesis, characterization, and application of mixed oxide nanocomposites (NCs) are gaining recognition for their superior functional properties compared with simple metal oxides. In this study, we synthesized magnesium oxide (MgO)–copper oxide (CuO)–iron oxide (Fe2O3) mixed oxide NCs using a s...

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Main Authors: Adnan Alnehia, Annas Al-Sharabi, Hisham Alnahari, Muhammad Hadi
Format: Article
Language:English
Published: Wiley 2024-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/joch/8129748
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author Adnan Alnehia
Annas Al-Sharabi
Hisham Alnahari
Muhammad Hadi
author_facet Adnan Alnehia
Annas Al-Sharabi
Hisham Alnahari
Muhammad Hadi
author_sort Adnan Alnehia
collection DOAJ
description The synthesis, characterization, and application of mixed oxide nanocomposites (NCs) are gaining recognition for their superior functional properties compared with simple metal oxides. In this study, we synthesized magnesium oxide (MgO)–copper oxide (CuO)–iron oxide (Fe2O3) mixed oxide NCs using a simple coprecipitation method and investigated several of their physical properties. X-ray diffraction (XRD) analyses revealed distinct phases, including monoclinic CuO, cubic MgO, cubic Fe2O3, and tetragonal CuFe2O4, with crystallite sizes ranging from 51 to 100 nm. Notably, the crystallite dimensions increased upon annealing at 800°C. UV-vis spectral analysis indicated two distinct energy bandgaps for the first sample at 3.10 eV and 4.18 eV and for the second sample at 3.44 eV and 2.67 eV, demonstrating a reduction in the optical energy bandgap with increasing temperature. Importantly, antibacterial assays revealed that the NCs exhibited a zone of inhibition of 24 mm against Gram-positive S. aureus; however, no significant antibacterial effect was observed against Gram-negative bacteria. These findings suggest that the MgO–CuO–Fe2O3 NC holds promise for healthcare and biotechnological applications, emphasizing the necessity for further exploration of its antibacterial properties for potential practical applications.
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spelling doaj-art-3be7e4b0fd744fdf9611c906967727b72025-01-08T00:00:07ZengWileyJournal of Chemistry2090-90712024-01-01202410.1155/joch/8129748Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial PropertiesAdnan Alnehia0Annas Al-Sharabi1Hisham Alnahari2Muhammad Hadi3Department of PhysicsDepartment of PhysicsDepartment of PhysicsDepartment of PhysicsThe synthesis, characterization, and application of mixed oxide nanocomposites (NCs) are gaining recognition for their superior functional properties compared with simple metal oxides. In this study, we synthesized magnesium oxide (MgO)–copper oxide (CuO)–iron oxide (Fe2O3) mixed oxide NCs using a simple coprecipitation method and investigated several of their physical properties. X-ray diffraction (XRD) analyses revealed distinct phases, including monoclinic CuO, cubic MgO, cubic Fe2O3, and tetragonal CuFe2O4, with crystallite sizes ranging from 51 to 100 nm. Notably, the crystallite dimensions increased upon annealing at 800°C. UV-vis spectral analysis indicated two distinct energy bandgaps for the first sample at 3.10 eV and 4.18 eV and for the second sample at 3.44 eV and 2.67 eV, demonstrating a reduction in the optical energy bandgap with increasing temperature. Importantly, antibacterial assays revealed that the NCs exhibited a zone of inhibition of 24 mm against Gram-positive S. aureus; however, no significant antibacterial effect was observed against Gram-negative bacteria. These findings suggest that the MgO–CuO–Fe2O3 NC holds promise for healthcare and biotechnological applications, emphasizing the necessity for further exploration of its antibacterial properties for potential practical applications.http://dx.doi.org/10.1155/joch/8129748
spellingShingle Adnan Alnehia
Annas Al-Sharabi
Hisham Alnahari
Muhammad Hadi
Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
Journal of Chemistry
title Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
title_full Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
title_fullStr Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
title_full_unstemmed Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
title_short Synthesis and Characterization of MgO–CuO–Fe2O3 Nanocomposite: A Study of Its Structural, Optical, and Antibacterial Properties
title_sort synthesis and characterization of mgo cuo fe2o3 nanocomposite a study of its structural optical and antibacterial properties
url http://dx.doi.org/10.1155/joch/8129748
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AT annasalsharabi synthesisandcharacterizationofmgocuofe2o3nanocompositeastudyofitsstructuralopticalandantibacterialproperties
AT hishamalnahari synthesisandcharacterizationofmgocuofe2o3nanocompositeastudyofitsstructuralopticalandantibacterialproperties
AT muhammadhadi synthesisandcharacterizationofmgocuofe2o3nanocompositeastudyofitsstructuralopticalandantibacterialproperties