Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction
Abstract. Recently, Na2/3[Fe1/2Mn1/2]O2 has received attention as a potential candidate material for cathode sodium-ion batteries. However, this material was synthesized by a solid-state process, resulting in larger particle size and nonuniform morphology. The larger particle size will sluggish the...
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| Format: | Article |
| Language: | English |
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Universitas Sebelas Maret
2024-05-01
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| Series: | Equilibrium |
| Online Access: | https://jurnal.uns.ac.id/equilibrium/article/view/80464 |
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| author | Diah Agustina Puspitasari Supriyono Supriyono Christina Wahyu Kartikowati Mar’atul Fauziyah Femiana Gapsari Vania Mitha Pratiwi Devina Annora H Br Butar-Butar Ira Marisa D.N Rashieka Putri Maghfiroh Yudha Bhakti Prasetia Rivanda Adi I. R Irginata Aqil H Roihan Rajabi Umar Khalid Zaki Abdul |
| author_facet | Diah Agustina Puspitasari Supriyono Supriyono Christina Wahyu Kartikowati Mar’atul Fauziyah Femiana Gapsari Vania Mitha Pratiwi Devina Annora H Br Butar-Butar Ira Marisa D.N Rashieka Putri Maghfiroh Yudha Bhakti Prasetia Rivanda Adi I. R Irginata Aqil H Roihan Rajabi Umar Khalid Zaki Abdul |
| author_sort | Diah Agustina Puspitasari |
| collection | DOAJ |
| description | Abstract. Recently, Na2/3[Fe1/2Mn1/2]O2 has received attention as a potential candidate material for cathode sodium-ion batteries. However, this material was synthesized by a solid-state process, resulting in larger particle size and nonuniform morphology. The larger particle size will sluggish the Na ion diffusion. Here we report the synthesis of Na2/3[Fe1/2Mn1/2]O2 using a simple sol-gel process. The X-ray diffraction revealed that the sample was identified as Na2/3[Fe1/2Mn1/2]O2 with a hexagonal crystal structure. However, the impurities are formed at diffraction angles of 36.28°, 45.03°, and 51.23°. Calcination temperature affects the formation of the crystal phase, grain growth, morphology, and particle size. Our findings provide valuable insight into the development of Na2/3[Fe1/2Mn1/2]O2 material with desirable properties.
Keywords:
Sol-Gel, Solid State, Grain Growth, Calcination, Na2/3[Fe1/2Mn1/2]O2 |
| format | Article |
| id | doaj-art-2d4354070180406299371547ba06dc1f |
| institution | Kabale University |
| issn | 2622-3430 |
| language | English |
| publishDate | 2024-05-01 |
| publisher | Universitas Sebelas Maret |
| record_format | Article |
| series | Equilibrium |
| spelling | doaj-art-2d4354070180406299371547ba06dc1f2025-01-14T08:39:45ZengUniversitas Sebelas MaretEquilibrium2622-34302024-05-0181454810.20961/equilibrium.v8i1.8046441879Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel ReactionDiah Agustina Puspitasari0Supriyono SupriyonoChristina Wahyu KartikowatiMar’atul FauziyahFemiana GapsariVania Mitha PratiwiDevina Annora H Br Butar-ButarIra Marisa D.NRashieka Putri MaghfirohYudha Bhakti PrasetiaRivanda Adi I. RIrginata Aqil HRoihan RajabiUmar Khalid Zaki AbdulBrawijaya UniversityAbstract. Recently, Na2/3[Fe1/2Mn1/2]O2 has received attention as a potential candidate material for cathode sodium-ion batteries. However, this material was synthesized by a solid-state process, resulting in larger particle size and nonuniform morphology. The larger particle size will sluggish the Na ion diffusion. Here we report the synthesis of Na2/3[Fe1/2Mn1/2]O2 using a simple sol-gel process. The X-ray diffraction revealed that the sample was identified as Na2/3[Fe1/2Mn1/2]O2 with a hexagonal crystal structure. However, the impurities are formed at diffraction angles of 36.28°, 45.03°, and 51.23°. Calcination temperature affects the formation of the crystal phase, grain growth, morphology, and particle size. Our findings provide valuable insight into the development of Na2/3[Fe1/2Mn1/2]O2 material with desirable properties. Keywords: Sol-Gel, Solid State, Grain Growth, Calcination, Na2/3[Fe1/2Mn1/2]O2https://jurnal.uns.ac.id/equilibrium/article/view/80464 |
| spellingShingle | Diah Agustina Puspitasari Supriyono Supriyono Christina Wahyu Kartikowati Mar’atul Fauziyah Femiana Gapsari Vania Mitha Pratiwi Devina Annora H Br Butar-Butar Ira Marisa D.N Rashieka Putri Maghfiroh Yudha Bhakti Prasetia Rivanda Adi I. R Irginata Aqil H Roihan Rajabi Umar Khalid Zaki Abdul Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction Equilibrium |
| title | Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction |
| title_full | Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction |
| title_fullStr | Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction |
| title_full_unstemmed | Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction |
| title_short | Calcination Temperature Effect on Characteristic Properties of Na2/3[Fe1/2Mn1/2]O2 Synthesized by Sol-Gel Reaction |
| title_sort | calcination temperature effect on characteristic properties of na2 3 fe1 2mn1 2 o2 synthesized by sol gel reaction |
| url | https://jurnal.uns.ac.id/equilibrium/article/view/80464 |
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