Influence of hydrophilicity on adsorption of caffeine onto montmorillonite

Some types of montmorillonite containing different interlayer ions were prepared and the changes in the interlayer spacings, the hydrophilicity, and the characteristics of adsorption of caffeine in solution were observed. Ion exchange treatments were performed using Li, Na, K, Rb, Cs, Mg, Ca, Sr, or...

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Main Authors: Kenichiro Yamamoto, Takashi Shiono, Ryoto Yoshimura, Yasuto Matsui, Minoru Yoneda
Format: Article
Language:English
Published: SAGE Publishing 2018-05-01
Series:Adsorption Science & Technology
Online Access:https://doi.org/10.1177/0263617417735480
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author Kenichiro Yamamoto
Takashi Shiono
Ryoto Yoshimura
Yasuto Matsui
Minoru Yoneda
author_facet Kenichiro Yamamoto
Takashi Shiono
Ryoto Yoshimura
Yasuto Matsui
Minoru Yoneda
author_sort Kenichiro Yamamoto
collection DOAJ
description Some types of montmorillonite containing different interlayer ions were prepared and the changes in the interlayer spacings, the hydrophilicity, and the characteristics of adsorption of caffeine in solution were observed. Ion exchange treatments were performed using Li, Na, K, Rb, Cs, Mg, Ca, Sr, or Ba. As a result, Li- and Na-type montmorillonite showed larger interlayer distance (1.31–1.53 nm), than K, Rb, and Cs-type montmorillonite (1.23–1.26 nm). In the measurement of hydrophilicity using a pulse NMR-based particle interface analyzer, Li- and Na-type montmorillonite showed higher hydrophilicity. In addition, K Lang , which indicates the interaction with caffeine, was 0.25–0.32 l/mmol, which is lower than K-, Rb-, and Cs-type montmorillonite (1.14–1.60 l/mmol). It is possible that adsorption of water molecules inhibits caffeine from adsorbing. Because of the difficulty of exchange between caffeine and water molecules in interlayer of the Li- and Na-type montmorillonite, the interaction with caffeine decreased. Alternatively, another possibility is that when highly hydrophilic montmorillonite retains many water molecules, the caffeine adsorption sites are blocked by water molecules. In either case, hydrophilicity has a large influence on the adsorption of caffeine onto montmorillonite.
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publishDate 2018-05-01
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series Adsorption Science & Technology
spelling doaj-art-2941d187664e4492afed6cd46a3c8eea2025-01-02T02:57:59ZengSAGE PublishingAdsorption Science & Technology0263-61742048-40382018-05-013610.1177/0263617417735480Influence of hydrophilicity on adsorption of caffeine onto montmorilloniteKenichiro YamamotoTakashi ShionoRyoto YoshimuraYasuto MatsuiMinoru YonedaSome types of montmorillonite containing different interlayer ions were prepared and the changes in the interlayer spacings, the hydrophilicity, and the characteristics of adsorption of caffeine in solution were observed. Ion exchange treatments were performed using Li, Na, K, Rb, Cs, Mg, Ca, Sr, or Ba. As a result, Li- and Na-type montmorillonite showed larger interlayer distance (1.31–1.53 nm), than K, Rb, and Cs-type montmorillonite (1.23–1.26 nm). In the measurement of hydrophilicity using a pulse NMR-based particle interface analyzer, Li- and Na-type montmorillonite showed higher hydrophilicity. In addition, K Lang , which indicates the interaction with caffeine, was 0.25–0.32 l/mmol, which is lower than K-, Rb-, and Cs-type montmorillonite (1.14–1.60 l/mmol). It is possible that adsorption of water molecules inhibits caffeine from adsorbing. Because of the difficulty of exchange between caffeine and water molecules in interlayer of the Li- and Na-type montmorillonite, the interaction with caffeine decreased. Alternatively, another possibility is that when highly hydrophilic montmorillonite retains many water molecules, the caffeine adsorption sites are blocked by water molecules. In either case, hydrophilicity has a large influence on the adsorption of caffeine onto montmorillonite.https://doi.org/10.1177/0263617417735480
spellingShingle Kenichiro Yamamoto
Takashi Shiono
Ryoto Yoshimura
Yasuto Matsui
Minoru Yoneda
Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
Adsorption Science & Technology
title Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
title_full Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
title_fullStr Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
title_full_unstemmed Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
title_short Influence of hydrophilicity on adsorption of caffeine onto montmorillonite
title_sort influence of hydrophilicity on adsorption of caffeine onto montmorillonite
url https://doi.org/10.1177/0263617417735480
work_keys_str_mv AT kenichiroyamamoto influenceofhydrophilicityonadsorptionofcaffeineontomontmorillonite
AT takashishiono influenceofhydrophilicityonadsorptionofcaffeineontomontmorillonite
AT ryotoyoshimura influenceofhydrophilicityonadsorptionofcaffeineontomontmorillonite
AT yasutomatsui influenceofhydrophilicityonadsorptionofcaffeineontomontmorillonite
AT minoruyoneda influenceofhydrophilicityonadsorptionofcaffeineontomontmorillonite