Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)

<b>Background/Objectives</b>: This study evaluates the effect of Mn(II) and Co(II) ions on the production of anti-<i>Candida</i> metabolites by the endophytic fungus Aspergillus sp., isolated from <i>Dizygostemon riparius</i>. The objective was to identify metal-i...

Full description

Saved in:
Bibliographic Details
Main Authors: Anne Karoline Maiorana Santos, Bianca Araújo dos Santos, Josivan Regis Farias, Sebastião Vieira de Morais, Cleydlenne Costa Vasconcelos, Rosane Nassar Meireles Guerra, Edson Rodrigues-Filho, Alberto Jorge Oliveira Lopes, Antônio José Cantanhede Filho
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Pharmaceuticals
Subjects:
Online Access:https://www.mdpi.com/1424-8247/17/12/1678
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1846103209228107776
author Anne Karoline Maiorana Santos
Bianca Araújo dos Santos
Josivan Regis Farias
Sebastião Vieira de Morais
Cleydlenne Costa Vasconcelos
Rosane Nassar Meireles Guerra
Edson Rodrigues-Filho
Alberto Jorge Oliveira Lopes
Antônio José Cantanhede Filho
author_facet Anne Karoline Maiorana Santos
Bianca Araújo dos Santos
Josivan Regis Farias
Sebastião Vieira de Morais
Cleydlenne Costa Vasconcelos
Rosane Nassar Meireles Guerra
Edson Rodrigues-Filho
Alberto Jorge Oliveira Lopes
Antônio José Cantanhede Filho
author_sort Anne Karoline Maiorana Santos
collection DOAJ
description <b>Background/Objectives</b>: This study evaluates the effect of Mn(II) and Co(II) ions on the production of anti-<i>Candida</i> metabolites by the endophytic fungus Aspergillus sp., isolated from <i>Dizygostemon riparius</i>. The objective was to identify metal-induced secondary metabolites with antifungal potential against drug-resistant <i>Candida</i> species. <b>Methods</b>: <i>Aspergillus</i> sp. was cultivated in Czapek agar supplemented with MnCl₂ (400 µM) or CoCl₂ (200 µM). Metabolite profiles were analyzed using UHPLC-DAD and LC-ESI-HRMS, followed by structural elucidation via NMR. Antifungal and biofilm inhibition activities were tested against <i>Candida albicans</i> and <i>Candida parapsilosis</i>. Toxicity was assessed using <i>Tenebrio molitor</i> larvae. <b>Results</b>: Key metabolites, including pyrophen, penicillquei B, and fonsecinone B, demonstrated antifungal activity with MIC values of 4.37–280.61 µg/mL. Fonsecinone B exhibited superior biofilm inhibition, surpassing fluconazole in reducing biofilm biomass and viability. In vivo assays showed low toxicity, with survival rates above 80% at 2× MIC/kg. <b>Conclusions</b>: Mn(II) and Co(II) significantly modulated the production of antifungal metabolites in <i>Aspergillus</i> sp. Fonsecinone B emerged as a promising candidate for antifungal therapy due to its potent activity and low toxicity. These findings support further investigation into the therapeutic potential of metal-induced fungal metabolites for combating drug-resistant <i>Candida</i> infections.
format Article
id doaj-art-284fdcbe5a1b4db1a3e7274f4ab192f3
institution Kabale University
issn 1424-8247
language English
publishDate 2024-12-01
publisher MDPI AG
record_format Article
series Pharmaceuticals
spelling doaj-art-284fdcbe5a1b4db1a3e7274f4ab192f32024-12-27T14:46:03ZengMDPI AGPharmaceuticals1424-82472024-12-011712167810.3390/ph17121678Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)Anne Karoline Maiorana Santos0Bianca Araújo dos Santos1Josivan Regis Farias2Sebastião Vieira de Morais3Cleydlenne Costa Vasconcelos4Rosane Nassar Meireles Guerra5Edson Rodrigues-Filho6Alberto Jorge Oliveira Lopes7Antônio José Cantanhede Filho8Chemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, BrazilChemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, BrazilCenter for Biological and Health Sciences, Federal University of Maranhão, São Luís 65080-805, BrazilChemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, BrazilChemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, BrazilCenter for Biological and Health Sciences, Federal University of Maranhão, São Luís 65080-805, BrazilLaBioMMi, Federal University of São Carlos, CP 676, São Carlos 13565-905, BrazilChemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, BrazilChemistry Postgraduate Program, Federal Institute of Science Education and Technology of Maranhão, São Luís 65030-005, Brazil<b>Background/Objectives</b>: This study evaluates the effect of Mn(II) and Co(II) ions on the production of anti-<i>Candida</i> metabolites by the endophytic fungus Aspergillus sp., isolated from <i>Dizygostemon riparius</i>. The objective was to identify metal-induced secondary metabolites with antifungal potential against drug-resistant <i>Candida</i> species. <b>Methods</b>: <i>Aspergillus</i> sp. was cultivated in Czapek agar supplemented with MnCl₂ (400 µM) or CoCl₂ (200 µM). Metabolite profiles were analyzed using UHPLC-DAD and LC-ESI-HRMS, followed by structural elucidation via NMR. Antifungal and biofilm inhibition activities were tested against <i>Candida albicans</i> and <i>Candida parapsilosis</i>. Toxicity was assessed using <i>Tenebrio molitor</i> larvae. <b>Results</b>: Key metabolites, including pyrophen, penicillquei B, and fonsecinone B, demonstrated antifungal activity with MIC values of 4.37–280.61 µg/mL. Fonsecinone B exhibited superior biofilm inhibition, surpassing fluconazole in reducing biofilm biomass and viability. In vivo assays showed low toxicity, with survival rates above 80% at 2× MIC/kg. <b>Conclusions</b>: Mn(II) and Co(II) significantly modulated the production of antifungal metabolites in <i>Aspergillus</i> sp. Fonsecinone B emerged as a promising candidate for antifungal therapy due to its potent activity and low toxicity. These findings support further investigation into the therapeutic potential of metal-induced fungal metabolites for combating drug-resistant <i>Candida</i> infections.https://www.mdpi.com/1424-8247/17/12/1678anti-<i>Candida</i> metabolitesendophytic fungimetal-induced secondary metabolismnatural products biotechnology
spellingShingle Anne Karoline Maiorana Santos
Bianca Araújo dos Santos
Josivan Regis Farias
Sebastião Vieira de Morais
Cleydlenne Costa Vasconcelos
Rosane Nassar Meireles Guerra
Edson Rodrigues-Filho
Alberto Jorge Oliveira Lopes
Antônio José Cantanhede Filho
Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
Pharmaceuticals
anti-<i>Candida</i> metabolites
endophytic fungi
metal-induced secondary metabolism
natural products biotechnology
title Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
title_full Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
title_fullStr Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
title_full_unstemmed Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
title_short Effect of Mn(II) and Co(II) on Anti-<i>Candida</i> Metabolite Production by <i>Aspergillus</i> sp. an Endophyte Isolated from <i>Dizygostemon riparius</i> (Plantaginaceae)
title_sort effect of mn ii and co ii on anti i candida i metabolite production by i aspergillus i sp an endophyte isolated from i dizygostemon riparius i plantaginaceae
topic anti-<i>Candida</i> metabolites
endophytic fungi
metal-induced secondary metabolism
natural products biotechnology
url https://www.mdpi.com/1424-8247/17/12/1678
work_keys_str_mv AT annekarolinemaioranasantos effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT biancaaraujodossantos effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT josivanregisfarias effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT sebastiaovieirademorais effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT cleydlennecostavasconcelos effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT rosanenassarmeirelesguerra effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT edsonrodriguesfilho effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT albertojorgeoliveiralopes effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae
AT antoniojosecantanhedefilho effectofmniiandcoiionantiicandidaimetaboliteproductionbyiaspergillusispanendophyteisolatedfromidizygostemonripariusiplantaginaceae