Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing

Humidity sensors are integral to modern technology and extensively utilize Ti3C2Tx MXene for its superior sensitivity and accuracy. This material’s effectiveness stems from its abundant hydrophilic functional groups and high electrical conductivity. In this study, we enhanced the responsiveness to r...

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Main Authors: Hiroya Morotomi, Yuki Matsunaga, Lijun Liu, Hisashi Sugime, Jun Hirotani
Format: Article
Language:English
Published: AIP Publishing LLC 2024-12-01
Series:AIP Advances
Online Access:http://dx.doi.org/10.1063/5.0245810
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author Hiroya Morotomi
Yuki Matsunaga
Lijun Liu
Hisashi Sugime
Jun Hirotani
author_facet Hiroya Morotomi
Yuki Matsunaga
Lijun Liu
Hisashi Sugime
Jun Hirotani
author_sort Hiroya Morotomi
collection DOAJ
description Humidity sensors are integral to modern technology and extensively utilize Ti3C2Tx MXene for its superior sensitivity and accuracy. This material’s effectiveness stems from its abundant hydrophilic functional groups and high electrical conductivity. In this study, we enhanced the responsiveness to relative humidity changes by incorporating bentonite, a 2D clay mineral known for its robust water adsorption capacity and ionic conductivity, attributable to its distinctive structure. Our analysis of MXene/bentonite thin films through sheet resistance measurements indicated a clear inverse relationship in resistance changes above and below a specific MXene-to-bentonite ratio. Impedance analysis further revealed that the dominant conduction mechanisms within these films vary according to the mix ratio. In fabricating conductive-type humidity sensors from MXene/bentonite films, we observed a remarkable increase in humidity sensitivity. Particularly, MXene rich film (33 wt. % MXene) demonstrated a sensitivity of ∼58.1 times greater than MXene film, and bentonite rich film (10 wt. % MXene) demonstrated about 5000 times greater than MXene film. This study not only underscores the potential of MXene/bentonite composites in humidity sensing but also highlights the critical role of composition in optimizing sensor performance.
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spelling doaj-art-26f8e7bca33d4bdbae2188dc1a3a7a952025-01-02T17:23:44ZengAIP Publishing LLCAIP Advances2158-32262024-12-011412125123125123-710.1063/5.0245810Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensingHiroya Morotomi0Yuki Matsunaga1Lijun Liu2Hisashi Sugime3Jun Hirotani4Department of Micro Engineering, Graduate School of Engineering, Kyoto University, Kyotodaigaku-Katsura C3, Nishikyo-ku, Kyoto 615-8540, JapanDepartment of Chemistry, Graduate School of Science, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8602, JapanDepartment of Mechanical Engineering, Graduate School of Engineering, Osaka University, Osaka 565-0871, JapanGraduate School of Science and Engineering, Kindai University, 3-4-1, Kowakae, Higashi-Osaka, Osaka 577-8502, JapanDepartment of Micro Engineering, Graduate School of Engineering, Kyoto University, Kyotodaigaku-Katsura C3, Nishikyo-ku, Kyoto 615-8540, JapanHumidity sensors are integral to modern technology and extensively utilize Ti3C2Tx MXene for its superior sensitivity and accuracy. This material’s effectiveness stems from its abundant hydrophilic functional groups and high electrical conductivity. In this study, we enhanced the responsiveness to relative humidity changes by incorporating bentonite, a 2D clay mineral known for its robust water adsorption capacity and ionic conductivity, attributable to its distinctive structure. Our analysis of MXene/bentonite thin films through sheet resistance measurements indicated a clear inverse relationship in resistance changes above and below a specific MXene-to-bentonite ratio. Impedance analysis further revealed that the dominant conduction mechanisms within these films vary according to the mix ratio. In fabricating conductive-type humidity sensors from MXene/bentonite films, we observed a remarkable increase in humidity sensitivity. Particularly, MXene rich film (33 wt. % MXene) demonstrated a sensitivity of ∼58.1 times greater than MXene film, and bentonite rich film (10 wt. % MXene) demonstrated about 5000 times greater than MXene film. This study not only underscores the potential of MXene/bentonite composites in humidity sensing but also highlights the critical role of composition in optimizing sensor performance.http://dx.doi.org/10.1063/5.0245810
spellingShingle Hiroya Morotomi
Yuki Matsunaga
Lijun Liu
Hisashi Sugime
Jun Hirotani
Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
AIP Advances
title Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
title_full Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
title_fullStr Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
title_full_unstemmed Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
title_short Enhanced water adsorption properties of Ti3C2Tx MXene/bentonite thin films for highly sensitive humidity sensing
title_sort enhanced water adsorption properties of ti3c2tx mxene bentonite thin films for highly sensitive humidity sensing
url http://dx.doi.org/10.1063/5.0245810
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