Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal

A chopper amplification technique has been developed to correct zero drift when measuring the magnitude of the piezoelectric response using the PFM method under conditions of continuous temperature change. Employing this technique, the temperatures of the antiferroelectric – ferroelectric phase tran...

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Main Authors: Vakulenko Aleksandr, Vanina Polina, Filimonov Alexey, Vakhrushev Sergey
Format: Article
Language:English
Published: Peter the Great St.Petersburg Polytechnic University 2024-12-01
Series:St. Petersburg Polytechnical University Journal: Physics and Mathematics
Subjects:
Online Access:https://physmath.spbstu.ru/article/2024.77.08/
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author Vakulenko Aleksandr
Vanina Polina
Filimonov Alexey
Vakhrushev Sergey
author_facet Vakulenko Aleksandr
Vanina Polina
Filimonov Alexey
Vakhrushev Sergey
author_sort Vakulenko Aleksandr
collection DOAJ
description A chopper amplification technique has been developed to correct zero drift when measuring the magnitude of the piezoelectric response using the PFM method under conditions of continuous temperature change. Employing this technique, the temperatures of the antiferroelectric – ferroelectric phase transition of a PZT 4% single crystal were obtained. A qualitative agreement with the results of measuring the saturation polarization obtained by the Sawyer – Tower method makes it possible to assert that the technical assumptions made are quite reasonable and the developed method is worthy of widespread use in such measurements.
format Article
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institution Kabale University
issn 2405-7223
language English
publishDate 2024-12-01
publisher Peter the Great St.Petersburg Polytechnic University
record_format Article
series St. Petersburg Polytechnical University Journal: Physics and Mathematics
spelling doaj-art-26f5b6fea7d94200a13a0be6444eb2d62025-01-16T13:35:28ZengPeter the Great St.Petersburg Polytechnic UniversitySt. Petersburg Polytechnical University Journal: Physics and Mathematics2405-72232024-12-0117410.18721/JPM.1740820714726Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystalVakulenko Aleksandr0https://orcid.org/0000-0001-5541-3409Vanina Polina1https://orcid.org/0000-0002-4113-0405Filimonov Alexey2https://orcid.org/0000-0002-2793-5717Vakhrushev Sergey3https://orcid.org/0000-0003-4867-1404Peter the Great St. Petersburg Polytechnic UniversityPeter the Great St. Petersburg Polytechnic UniversityPeter the Great St. Petersburg Polytechnic UniversityIoffe InstituteA chopper amplification technique has been developed to correct zero drift when measuring the magnitude of the piezoelectric response using the PFM method under conditions of continuous temperature change. Employing this technique, the temperatures of the antiferroelectric – ferroelectric phase transition of a PZT 4% single crystal were obtained. A qualitative agreement with the results of measuring the saturation polarization obtained by the Sawyer – Tower method makes it possible to assert that the technical assumptions made are quite reasonable and the developed method is worthy of widespread use in such measurements.https://physmath.spbstu.ru/article/2024.77.08/ferroelectriclead zirconate titanatepiezoresponseatomic force microscopyphase transitionsawyer – tower method
spellingShingle Vakulenko Aleksandr
Vanina Polina
Filimonov Alexey
Vakhrushev Sergey
Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
St. Petersburg Polytechnical University Journal: Physics and Mathematics
ferroelectric
lead zirconate titanate
piezoresponse
atomic force microscopy
phase transition
sawyer – tower method
title Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
title_full Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
title_fullStr Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
title_full_unstemmed Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
title_short Modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the PZT single crystal
title_sort modernization of the methodology for obtaining phase transition temperatures using the piezoresponse force microscopy exemplified by study of a phase transition in the pzt single crystal
topic ferroelectric
lead zirconate titanate
piezoresponse
atomic force microscopy
phase transition
sawyer – tower method
url https://physmath.spbstu.ru/article/2024.77.08/
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AT vaninapolina modernizationofthemethodologyforobtainingphasetransitiontemperaturesusingthepiezoresponseforcemicroscopyexemplifiedbystudyofaphasetransitioninthepztsinglecrystal
AT filimonovalexey modernizationofthemethodologyforobtainingphasetransitiontemperaturesusingthepiezoresponseforcemicroscopyexemplifiedbystudyofaphasetransitioninthepztsinglecrystal
AT vakhrushevsergey modernizationofthemethodologyforobtainingphasetransitiontemperaturesusingthepiezoresponseforcemicroscopyexemplifiedbystudyofaphasetransitioninthepztsinglecrystal