Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins

Abstract The effects of heat-assisted vat photopolymerization (HVPP) on the physical and mechanical properties of 3D-printed dental resins, including the morphometric stability of 3D-printed crowns, were investigated. A resin tank was designed to maintain the resin at 30, 40, and 50 ℃ during the 3D...

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Main Authors: Jung-Hwa Lim, Seung-Ho Shin, Young-Eun Jung, Hongseok An, Jong-Eun Kim
Format: Article
Language:English
Published: Nature Portfolio 2025-01-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-85529-7
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author Jung-Hwa Lim
Seung-Ho Shin
Young-Eun Jung
Hongseok An
Jong-Eun Kim
author_facet Jung-Hwa Lim
Seung-Ho Shin
Young-Eun Jung
Hongseok An
Jong-Eun Kim
author_sort Jung-Hwa Lim
collection DOAJ
description Abstract The effects of heat-assisted vat photopolymerization (HVPP) on the physical and mechanical properties of 3D-printed dental resins, including the morphometric stability of 3D-printed crowns, were investigated. A resin tank was designed to maintain the resin at 30, 40, and 50 ℃ during the 3D printing process. Test specimens were fabricated using a commercial dental resin, with untreated resin serving as the control group. Key properties such as viscosity, curing kinetics, surface microhardness, flexural properties, and dimensional accuracy were evaluated. The viscosity of the resin decreased significantly (P < 0.05) with increasing temperature, thereby enhancing its flow properties. Photo-DSC analysis revealed a 17.58% increase in peak heat flow at 50 ℃, indicating accelerated polymerization. Surface microhardness improved significantly (P < 0.05) with HVPP, though a slight reduction was observed at 50 ℃ compared to that at 30 and 40 ℃. The flexural strength, modulus, and resilience were significantly enhanced (P < 0.05) at higher temperatures, with 50 ℃ yielding the best mechanical properties. However, 3D morphometric analysis showed increased root mean square deviation from the CAD design at elevated temperatures. Our results suggest that HVPP enhances the durability of dental prostheses, although careful optimization of the printing temperature is essential to balance their strength and accuracy.
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spelling doaj-art-086cbfc60d8f47558c46ccb74c73fc062025-01-12T12:22:59ZengNature PortfolioScientific Reports2045-23222025-01-0115111110.1038/s41598-025-85529-7Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resinsJung-Hwa Lim0Seung-Ho Shin1Young-Eun Jung2Hongseok An3Jong-Eun Kim4Department of Prosthodontics, Yonsei University College of DentistryDepartment of Prosthodontics, Yonsei University College of DentistryDepartment of Orthodontics, New York University College of DentistryDepartment of Oral Rehabilitation and Biosciences, Oregon Health & Science University School of DentistryDepartment of Prosthodontics, Yonsei University College of DentistryAbstract The effects of heat-assisted vat photopolymerization (HVPP) on the physical and mechanical properties of 3D-printed dental resins, including the morphometric stability of 3D-printed crowns, were investigated. A resin tank was designed to maintain the resin at 30, 40, and 50 ℃ during the 3D printing process. Test specimens were fabricated using a commercial dental resin, with untreated resin serving as the control group. Key properties such as viscosity, curing kinetics, surface microhardness, flexural properties, and dimensional accuracy were evaluated. The viscosity of the resin decreased significantly (P < 0.05) with increasing temperature, thereby enhancing its flow properties. Photo-DSC analysis revealed a 17.58% increase in peak heat flow at 50 ℃, indicating accelerated polymerization. Surface microhardness improved significantly (P < 0.05) with HVPP, though a slight reduction was observed at 50 ℃ compared to that at 30 and 40 ℃. The flexural strength, modulus, and resilience were significantly enhanced (P < 0.05) at higher temperatures, with 50 ℃ yielding the best mechanical properties. However, 3D morphometric analysis showed increased root mean square deviation from the CAD design at elevated temperatures. Our results suggest that HVPP enhances the durability of dental prostheses, although careful optimization of the printing temperature is essential to balance their strength and accuracy.https://doi.org/10.1038/s41598-025-85529-7Vat photopolymerization3D-printed crownHot lithographyMechanical propertiesBiomedical resins
spellingShingle Jung-Hwa Lim
Seung-Ho Shin
Young-Eun Jung
Hongseok An
Jong-Eun Kim
Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
Scientific Reports
Vat photopolymerization
3D-printed crown
Hot lithography
Mechanical properties
Biomedical resins
title Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
title_full Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
title_fullStr Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
title_full_unstemmed Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
title_short Influence of heat-assisted vat photopolymerization on the physical and mechanical characteristics of dental 3D printing resins
title_sort influence of heat assisted vat photopolymerization on the physical and mechanical characteristics of dental 3d printing resins
topic Vat photopolymerization
3D-printed crown
Hot lithography
Mechanical properties
Biomedical resins
url https://doi.org/10.1038/s41598-025-85529-7
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