Theoretical and experimental analysis of the modulated phase grating X-ray interferometer

Abstract X-ray grating interferometry allows for the simultaneous acquisition of attenuation, differential-phase contrast, and dark-field images, resulting from X-ray attenuation, refraction, and small-angle scattering, respectively. The modulated phase grating (MPG) interferometer is a recently dev...

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Main Authors: Hunter Meyer, Joyoni Dey, Sydney Carr, Kyungmin Ham, Leslie G. Butler, Kerry M. Dooley, Ivan Hidrovo, Markus Bleuel, Tamas Varga, Joachim Schulz, Thomas Beckenbach, Konradin Kaiser
Format: Article
Language:English
Published: Nature Portfolio 2024-11-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-024-78133-8
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author Hunter Meyer
Joyoni Dey
Sydney Carr
Kyungmin Ham
Leslie G. Butler
Kerry M. Dooley
Ivan Hidrovo
Markus Bleuel
Tamas Varga
Joachim Schulz
Thomas Beckenbach
Konradin Kaiser
author_facet Hunter Meyer
Joyoni Dey
Sydney Carr
Kyungmin Ham
Leslie G. Butler
Kerry M. Dooley
Ivan Hidrovo
Markus Bleuel
Tamas Varga
Joachim Schulz
Thomas Beckenbach
Konradin Kaiser
author_sort Hunter Meyer
collection DOAJ
description Abstract X-ray grating interferometry allows for the simultaneous acquisition of attenuation, differential-phase contrast, and dark-field images, resulting from X-ray attenuation, refraction, and small-angle scattering, respectively. The modulated phase grating (MPG) interferometer is a recently developed grating interferometry system capable of generating a directly resolvable interference pattern using a relatively large period grating envelope function that is sampled at a pitch that is small enough that X-ray spatial coherence can be achieved by using a microfocus X-ray source or G0 grating. We present the theory of the MPG interferometry system for a 2-dimensional staggered grating, derived using Fourier optics, and we compare the theoretical predictions with experiments we have performed with a microfocus X-ray system at Pennington Biomedical Research Center, LSU. The theoretical and experimental fringe visibility is evaluated as a function of grating-to-detector distance. Additionally, quantitative experiments are performed with porous carbon and alumina compounds, and the mean normalized dark-field signal is compared with independent porosimetry measurements. Qualitative analysis of attenuation and dark-field images of a dried anchovy are shown.
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spelling doaj-art-047e614befbc4c25bd68d1cb236774f02024-11-10T12:15:34ZengNature PortfolioScientific Reports2045-23222024-11-0114111510.1038/s41598-024-78133-8Theoretical and experimental analysis of the modulated phase grating X-ray interferometerHunter Meyer0Joyoni Dey1Sydney Carr2Kyungmin Ham3Leslie G. Butler4Kerry M. Dooley5Ivan Hidrovo6Markus Bleuel7Tamas Varga8Joachim Schulz9Thomas Beckenbach10Konradin Kaiser11Department of Physics and Astronomy, Louisiana State UniversityDepartment of Physics and Astronomy, Louisiana State UniversityDepartment of Physics and Astronomy, Louisiana State UniversityCenter for Advanced Microstructures and Devices, Louisiana State UniversityDepartment of Chemistry, Louisiana State UniversityCain Department of Chemical Engineering, Louisiana State UniversityDepartment of Physics and Astronomy, Louisiana State UniversityAdelphi Technology, Inc.The Environmental Molecular Sciences Laboratory, Pacific Northwest National LaboratoryMicroworks GmbHMicroworks GmbHMicroworks GmbHAbstract X-ray grating interferometry allows for the simultaneous acquisition of attenuation, differential-phase contrast, and dark-field images, resulting from X-ray attenuation, refraction, and small-angle scattering, respectively. The modulated phase grating (MPG) interferometer is a recently developed grating interferometry system capable of generating a directly resolvable interference pattern using a relatively large period grating envelope function that is sampled at a pitch that is small enough that X-ray spatial coherence can be achieved by using a microfocus X-ray source or G0 grating. We present the theory of the MPG interferometry system for a 2-dimensional staggered grating, derived using Fourier optics, and we compare the theoretical predictions with experiments we have performed with a microfocus X-ray system at Pennington Biomedical Research Center, LSU. The theoretical and experimental fringe visibility is evaluated as a function of grating-to-detector distance. Additionally, quantitative experiments are performed with porous carbon and alumina compounds, and the mean normalized dark-field signal is compared with independent porosimetry measurements. Qualitative analysis of attenuation and dark-field images of a dried anchovy are shown.https://doi.org/10.1038/s41598-024-78133-8X-ray interferometryModulated phase gratingDiffraction gratingDark-fieldPorosity
spellingShingle Hunter Meyer
Joyoni Dey
Sydney Carr
Kyungmin Ham
Leslie G. Butler
Kerry M. Dooley
Ivan Hidrovo
Markus Bleuel
Tamas Varga
Joachim Schulz
Thomas Beckenbach
Konradin Kaiser
Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
Scientific Reports
X-ray interferometry
Modulated phase grating
Diffraction grating
Dark-field
Porosity
title Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
title_full Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
title_fullStr Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
title_full_unstemmed Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
title_short Theoretical and experimental analysis of the modulated phase grating X-ray interferometer
title_sort theoretical and experimental analysis of the modulated phase grating x ray interferometer
topic X-ray interferometry
Modulated phase grating
Diffraction grating
Dark-field
Porosity
url https://doi.org/10.1038/s41598-024-78133-8
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