Functionalization of Carbon and Silica Gel by Phosphoric Acid

Functionalization of polymer-based carbon (SCS-3) and silica gel (SG60) by phosphoric acid at 800°C was investigated. It was shown that heat treatment of carbon and silica gel in the presence of phosphoric acid at 800°C provides a way of functionalizing materials with phosphorus-containing surface g...

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Bibliographic Details
Main Authors: A.M. Puziy, O.I. Poddubnaya, B. Gawdzik, M. Sobiesiak, M.M. Tsyba
Format: Article
Language:English
Published: SAGE Publishing 2007-10-01
Series:Adsorption Science & Technology
Online Access:https://doi.org/10.1260/0263-6174.25.8.531
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Summary:Functionalization of polymer-based carbon (SCS-3) and silica gel (SG60) by phosphoric acid at 800°C was investigated. It was shown that heat treatment of carbon and silica gel in the presence of phosphoric acid at 800°C provides a way of functionalizing materials with phosphorus-containing surface groups. Functionalization of the finished carbon occurs as a surface reaction while destruction of the silica gel structure was observed. Functionalization with phosphoric acid creates new acid surface groups — phosphorus-containing and oxygen-containing in the case of carbon and only phosphorus-containing in the case of silica gel. Enhancement of the amount of acid surface groups by functionalization improves the metal-ion binding properties of both carbon and silica gel.
ISSN:0263-6174
2048-4038