Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications

Abstract The effect of W and WO3 electrodes on the ferroelectric characteristics of HZO (Zr-doped HfO2)-based MFM (metal-ferroelectric-metal) capacitors was investigated. During the deposition of tungsten, the W electrode was formed using only Ar gas, while the WO3 electrode was formed using a mixtu...

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Main Authors: Yejoo Choi, Jaemin Shin, Jinhong Min, Seungjun Moon, Daeyoung Chu, Donghwan Han, Changhwan Shin
Format: Article
Language:English
Published: Nature Portfolio 2024-11-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-024-80523-x
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author Yejoo Choi
Jaemin Shin
Jinhong Min
Seungjun Moon
Daeyoung Chu
Donghwan Han
Changhwan Shin
author_facet Yejoo Choi
Jaemin Shin
Jinhong Min
Seungjun Moon
Daeyoung Chu
Donghwan Han
Changhwan Shin
author_sort Yejoo Choi
collection DOAJ
description Abstract The effect of W and WO3 electrodes on the ferroelectric characteristics of HZO (Zr-doped HfO2)-based MFM (metal-ferroelectric-metal) capacitors was investigated. During the deposition of tungsten, the W electrode was formed using only Ar gas, while the WO3 electrode was formed using a mixture of Ar and O2 gases. The W-based MFM capacitors exhibited superior remnant polarization (2Pr of 107.9 µC/cm2 at 700 oC) compared to the WO3-based capacitors; however, their endurance performance was degraded. In contrast, the WO3-based capacitors showed endurance performance enhanced by three orders of magnitude due to the oxygen-rich reservoir effect. The oxygen introduced during the deposition of WO3 prevented the oxygen scavenging effect of tungsten. Consequently, excessive generation of oxygen vacancies in the HZO layer was suppressed, resulting in improved endurance performance. These results were quantitatively confirmed through TEM, XPS, and XRD analyses.
format Article
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institution Kabale University
issn 2045-2322
language English
publishDate 2024-11-01
publisher Nature Portfolio
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series Scientific Reports
spelling doaj-art-02df6876f15347f4bb2e01541ac0fe8d2024-11-24T12:24:32ZengNature PortfolioScientific Reports2045-23222024-11-011411810.1038/s41598-024-80523-xOxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applicationsYejoo Choi0Jaemin Shin1Jinhong Min2Seungjun Moon3Daeyoung Chu4Donghwan Han5Changhwan Shin6Department of Electrical and Computer Engineering, Sungkyunkwan UniversityDepartment of Electrical Engineering, University of Notre DameDepartment of Materials Science and Engineering, University of MichiganSemiconductor R&D Center, Samsung ElectronicsSemiconductor R&D Center, Samsung ElectronicsSemiconductor R&D Center, Samsung ElectronicsSchool of Electrical Engineering, Korea UniversityAbstract The effect of W and WO3 electrodes on the ferroelectric characteristics of HZO (Zr-doped HfO2)-based MFM (metal-ferroelectric-metal) capacitors was investigated. During the deposition of tungsten, the W electrode was formed using only Ar gas, while the WO3 electrode was formed using a mixture of Ar and O2 gases. The W-based MFM capacitors exhibited superior remnant polarization (2Pr of 107.9 µC/cm2 at 700 oC) compared to the WO3-based capacitors; however, their endurance performance was degraded. In contrast, the WO3-based capacitors showed endurance performance enhanced by three orders of magnitude due to the oxygen-rich reservoir effect. The oxygen introduced during the deposition of WO3 prevented the oxygen scavenging effect of tungsten. Consequently, excessive generation of oxygen vacancies in the HZO layer was suppressed, resulting in improved endurance performance. These results were quantitatively confirmed through TEM, XPS, and XRD analyses.https://doi.org/10.1038/s41598-024-80523-x
spellingShingle Yejoo Choi
Jaemin Shin
Jinhong Min
Seungjun Moon
Daeyoung Chu
Donghwan Han
Changhwan Shin
Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
Scientific Reports
title Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
title_full Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
title_fullStr Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
title_full_unstemmed Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
title_short Oxygen reservoir effect of Tungsten trioxide electrode on endurance performance of ferroelectric capacitors for FeRAM applications
title_sort oxygen reservoir effect of tungsten trioxide electrode on endurance performance of ferroelectric capacitors for feram applications
url https://doi.org/10.1038/s41598-024-80523-x
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AT jinhongmin oxygenreservoireffectoftungstentrioxideelectrodeonenduranceperformanceofferroelectriccapacitorsforferamapplications
AT seungjunmoon oxygenreservoireffectoftungstentrioxideelectrodeonenduranceperformanceofferroelectriccapacitorsforferamapplications
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